ITMI20090080A1 - METHOD FOR THE PRODUCTION OF PRESENTATION LENSES. - Google Patents

METHOD FOR THE PRODUCTION OF PRESENTATION LENSES. Download PDF

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Publication number
ITMI20090080A1
ITMI20090080A1 IT000080A ITMI20090080A ITMI20090080A1 IT MI20090080 A1 ITMI20090080 A1 IT MI20090080A1 IT 000080 A IT000080 A IT 000080A IT MI20090080 A ITMI20090080 A IT MI20090080A IT MI20090080 A1 ITMI20090080 A1 IT MI20090080A1
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IT
Italy
Prior art keywords
mold
lens
polyethylene terephthalate
granules
injection
Prior art date
Application number
IT000080A
Other languages
Italian (it)
Inventor
Bon Giovanni De
Sergio Sanna
Original Assignee
Plastodidattica Commerciale S R L
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Plastodidattica Commerciale S R L filed Critical Plastodidattica Commerciale S R L
Priority to ITMI2009A000080A priority Critical patent/IT1393078B1/en
Publication of ITMI20090080A1 publication Critical patent/ITMI20090080A1/en
Application granted granted Critical
Publication of IT1393078B1 publication Critical patent/IT1393078B1/en

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C45/00Injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould; Apparatus therefor
    • B29C45/0001Injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould; Apparatus therefor characterised by the choice of material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B13/00Conditioning or physical treatment of the material to be shaped
    • B29B13/06Conditioning or physical treatment of the material to be shaped by drying
    • B29B13/065Conditioning or physical treatment of the material to be shaped by drying of powder or pellets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29DPRODUCING PARTICULAR ARTICLES FROM PLASTICS OR FROM SUBSTANCES IN A PLASTIC STATE
    • B29D11/00Producing optical elements, e.g. lenses or prisms
    • B29D11/00009Production of simple or compound lenses
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C45/00Injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould; Apparatus therefor
    • B29C2045/0096Injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould; Apparatus therefor drying the moulding material before injection, e.g. by heating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C45/00Injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould; Apparatus therefor
    • B29C45/17Component parts, details or accessories; Auxiliary operations
    • B29C45/40Removing or ejecting moulded articles
    • B29C45/42Removing or ejecting moulded articles using means movable from outside the mould between mould parts, e.g. robots
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C45/00Injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould; Apparatus therefor
    • B29C45/17Component parts, details or accessories; Auxiliary operations
    • B29C45/72Heating or cooling
    • B29C45/73Heating or cooling of the mould
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29KINDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2067/00Use of polyesters or derivatives thereof, as moulding material

Description

"METODO PER LA PRODUZIONE DI LENTI DI PRESENTAZIO-NE" "METHOD FOR THE PRODUCTION OF PRESENTATION LENSES"

D E S C R I Z I O N E DESCRIPTION

Il presente trovato ha come oggetto un metodo per la produzione di lenti di presentazione. The present invention relates to a method for producing presentation lenses.

Come à ̈ noto, le lenti di presentazione, o lenti dimostrative, sono generalmente lenti stampate in materia plastica, realizzate mediante stampi multi-impronta, nei quali viene eseguita l’iniezione della materia plastica, che costituisce la lente stessa. As is known, presentation lenses, or demonstration lenses, are generally lenses molded in plastic material, made by means of multi-impression molds, in which the plastic material, which constitutes the lens itself, is injected.

La materia plastica attualmente utilizzata per la realizzazione delle lenti dimostrative à ̈ il polimetilmetacrilato. The plastic material currently used for the realization of the demonstration lenses is polymethylmethacrylate.

Compito del presente trovato à ̈ quello di mettere a punto un metodo per la produzione di lenti di presentazione che permetta di realizzare lenti dimostrative di qualità e nel contempo di ridurre i costi di produzione. The aim of the present invention is to provide a method for the production of presentation lenses which allows to produce quality demonstration lenses and at the same time to reduce production costs.

Nell’ambito di questo compito, uno scopo del trovato à ̈ quello di realizzare un'apparecchiatura in grado di produrre lenti dimostrative secondo il nuovo metodo, che risulti affidabile ed economicamente competitiva. Within the scope of this aim, an object of the invention is to provide an apparatus capable of producing demonstration lenses according to the new method, which is reliable and economically competitive.

Un ulteriore scopo à ̈ quello di realizzare una lente di presentazione di ottima qualità costituita da un materiale più economico e più vantaggioso anche dal punto di vista ambientale. A further object is to provide an excellent quality presentation lens made of a cheaper and more advantageous material also from the environmental point of view.

Questo ed altri scopi, che meglio appariranno evidenziati in seguito, sono raggiunti da un metodo per la produzione di lenti di presentazione caratterizzato dal fatto di comprendere le seguenti fasi: This and other purposes, which will be better highlighted below, are achieved by a method for the production of presentation lenses characterized by the fact that it comprises the following steps:

- deumidificazione di Polietilene Tereftalato solido in granuli; - trasformazione del Polietilene Tereftalato da solido in granuli a forma liquida tramite riscaldamento; - dehumidification of solid Polyethylene Terephthalate in granules; - transformation of Polyethylene Terephthalate from solid into liquid granules by heating;

- iniezione del Polietilene Tereftalato in forma liquida all’interno di uno stampo; - injection of polyethylene terephthalate in liquid form inside a mold;

- raffreddamento spinto dello stampo, durante la fase di iniezione; - forced cooling of the mold, during the injection phase;

- prelievo e deposito dei pezzi finiti. - picking up and depositing of finished pieces.

La fase di deumidificazione del PET in granuli à ̈ effettuata attraverso un deumidificatore, il quale elimina l'umidità in eccesso presente nel granulo di PET attraverso l'utilizzo di aria compressa filtrata attraverso filtri minerali. The dehumidification phase of PET in granules is carried out through a dehumidifier, which eliminates the excess humidity present in the PET granule through the use of compressed air filtered through mineral filters.

Vantaggiosamente, lo stampo presenta un raffreddamento molto spinto cosicché la forma amorfa del granulo, che in origine à ̈ una forma cristallina che assa alla forma amorfa attraverso il riscaldamento nella parte riscaldante della pressa, venga fissata al l'interno dello stampo freddo. Advantageously, the mold has a very intense cooling so that the amorphous form of the granule, which is originally a crystalline form which takes on the amorphous form through heating in the heating part of the press, is fixed inside the cold mold.

Ulteriori caratteristiche e vantaggi dell'oggetto del presente trovato risulteranno maggiormente evidenziati attraverso un esame della descrizione di una forma di realizzazione preferita, ma non esclusiva, del trovato. Further characteristics and advantages of the object of the present invention will become more evident through an examination of the description of a preferred, but not exclusive, embodiment of the invention.

Il metodo di produzione secondo il presente trovato permette di realizzare lenti di presentazione in Polietilene Tereftalato (PET), anziché in tradizionale polimetilmetacrilato. The production method according to the present invention allows to produce presentation lenses in Polyethylene Terephthalate (PET), instead of in traditional polymethylmethacrylate.

Il metodo comprende la trasformazione del Polietilene Tereftalato solido in granuli, tramite pressa ad iniezione, in forma liquida e la successiva iniezione all’interno di uno stampo studiato per la formazione del pezzo desiderato. The method includes the transformation of solid Polyethylene Terephthalate into granules, by injection press, in liquid form and the subsequent injection inside a mold designed for the formation of the desired piece.

Secondo il presente trovato, prima della fase di iniezione il Polietilene Tereftalato à ̈ sottoposto ad una fase di deumidificazione, effettuata tramite un deumidificatore, il quale elimina l'umidità in eccesso presente nel granulo di PET. According to the present invention, before the injection step the Polyethylene Terephthalate is subjected to a dehumidification step, carried out by means of a dehumidifier, which eliminates the excess humidity present in the PET granule.

La deumidificazione à ̈ effettuata mediante aria compressa, filtrata attraverso filtri minerali. Dehumidification is carried out by means of compressed air, filtered through mineral filters.

La fase di deumidificazione permette di eliminare l'umidità dal granulo di PET, umidità che degraderebbe il granulo stesso. The dehumidification phase allows to eliminate the humidity from the PET granule, humidity which would degrade the granule itself.

Una volta deumidificato il PET Ã ̈ pronto per essere trasformato in lente attraverso lo stampaggio. Once dehumidified, PET is ready to be transformed into a lens through molding.

La fase di stampaggio à ̈ effettuata in condizioni di raffreddamento molto s into affinché il materiale risulti tras arente mantenendo la forma amorfa ottenuta attraverso il riscaldamento nella parte riscaldante della pressa. The molding phase is carried out in very low cooling conditions so that the material is transparent while maintaining the amorphous shape obtained by heating the heating part of the press.

Infatti, il granulo in origine à ̈ cristallino e passa alla forma amorfa, necessaria per diventare trasparente, durante il riscaldamento nella parte riscaldante della pressa. In fact, the granule is originally crystalline and passes to the amorphous form, necessary to become transparent, during heating in the heating part of the press.

Il raffreddamento dello stampo permette di fissare tale forma amorfa all'interno dello stampo. The cooling of the mold allows to fix this amorphous shape inside the mold.

Preferibilmente la fase di stampaggio à ̈ effettuata mantenendo lo stampo ad una temperatura compresa tra i 10 ed i 18 gradi centigradi. Preferably the molding phase is carried out by keeping the mold at a temperature between 10 and 18 degrees centigrade.

Il metodo comprende infine una fase di prelievo e di deposito dei pezzi finiti tramite un robot cartesiano che utilizza la tecnica del vuoto, aspirando i pezzi direttamente dallo stampo e trasportandoli nell'area dedicata al deposito. Finally, the method includes a phase of picking up and depositing the finished pieces by means of a Cartesian robot that uses the vacuum technique, sucking the pieces directly from the mold and transporting them to the area dedicated to the deposit.

Il metodo oggetto del presente trovato à ̈ realizzato tramite un'apparecchiatura che comprende un deumidificatore per materie plastiche, una pressa ad iniezione, uno stampo per iniezione del materiale termoplastico, con condizionamento dedicato per PET, una centralina di refrigerazione per stampi, ed un robot cartesiano, funzionante a vuoto, per il prelievo e il deposito del pezzo finito. The method of the present invention is carried out by means of an apparatus which comprises a dehumidifier for plastic materials, an injection press, a mold for injection of thermoplastic material, with dedicated conditioning for PET, a refrigeration unit for molds, and a robot Cartesian, running empty, for picking up and depositing the finished piece.

Il deumidificatore elimina l'umidità in eccesso presente nel granulo di PET attraverso l'utilizzo di aria compressa filtrata attraverso filtri minerali. The dehumidifier eliminates the excess humidity present in the PET granule through the use of compressed air filtered through mineral filters.

Una volta deumidificato, il PET Ã ̈ pronto per essere trasformato in lente attraverso lo stampo. Once dehumidified, the PET is ready to be transformed into a lens through the mold.

Lo stampo comprende un sistema di raffreddamento molto spinto in modo da mantenere lo stampo stesso ad una temperatura compresa tra i 10 ed i 18 gradi centigradi. The mold includes a very thorough cooling system in order to keep the mold itself at a temperature between 10 and 18 degrees centigrade.

Il sistema di raffreddamento dello stampo comprende ricircoli di liquido refrigerante che arrivano a raffreddare anche il tassello che dà la forma al pezzo. The cooling system of the mold includes recirculations of coolant which also cool the piece that gives the piece its shape.

Il sistema di raffreddamento comprende inoltre una centralina refrigerante a circuito chiuso, in grado di dare al liquido refrigerante una temperatura compresa tra i 7 ed i 20 gradi centigradi. The cooling system also includes a closed-circuit refrigerating unit, capable of giving the coolant a temperature between 7 and 20 degrees centigrade.

Secondo il presente trovato l'apparecchiatura à ̈ inoltre costituita da un robot cartesiano che utilizza la tecnica del vuoto, aspirando i pezzi direttamente dallo stampo e trasportandoli nell'area dedicata al deposito. According to the present invention, the apparatus is also constituted by a Cartesian robot which uses the vacuum technique, sucking the pieces directly from the mold and transporting them to the area dedicated to storage.

Si à ̈ in pratica constatato che il trovato raggiunge il compito e gli scopi prefissati. In practice it has been found that the invention achieves the intended aim and objects.

Il metodo e l'apparecchiatura in precedenza descritti permettono infatti di produrre lenti dimostrative in Polietilene Tereftalato (PET), di qualità analoga o superiore rispetto alle lenti realizzate tradizionalmente, ma con costi di produzione sensibilmente ridotti grazie al minor costo del Polietilene Tereftalato rispetto ad altri materiali termoplastici utilizzati precedentemente quali il polimetilmetacrilato. The method and the equipment previously described allow in fact to produce demonstration lenses in Polyethylene Terephthalate (PET), of similar or superior quality compared to traditionally made lenses, but with significantly reduced production costs thanks to the lower cost of Polyethylene Terephthalate compared to others. previously used thermoplastic materials such as polymethylmethacrylate.

Naturalmente i materiali impiegati, nonché le dimensioni, potranno essere qualsiasi, secondo le esigenze. Naturally, the materials used, as well as the dimensions, may be any according to requirements.

Claims (9)

RIVENDICAZIONI 1. Metodo per la produzione di singole lenti di presentazione comprendente le fasi di: fornire granuli solidi di polietilene tereftalato; deumidificare deti granuli; riscaldare detti granuli deumidificati per fornire una massa liquida amorfa di polietilene tereftalato; iniettare la massa di polietilene tereftalato liquida amorfa all'interno di uno stampo; raffreddare in modo spinto lo stampo durante una fase di iniezione, così da fissare lo strato amorfo di detto polietilene tereftalato e fornire almeno una detta lente finita; e prelevare e depositare detta lente finita da deto stampo. CLAIMS 1. Method for manufacturing single presentation lenses comprising the steps of: providing solid polyethylene terephthalate granules; dehumidify certain granules; heating said dehumidified granules to provide an amorphous liquid mass of polyethylene terephthalate; injecting the amorphous liquid polyethylene terephthalate mass into a mold; cooling the mold in a forced manner during an injection step, so as to fix the amorphous layer of said polyethylene terephthalate and provide at least one said finished lens; And picking up and depositing said finished lens from said mold. 2. Metodo secondo la rivendicazione 1, caratterizzato dal fatto che la fase di deumidificazione à ̈ effettuata mediante aria compressa filtrata attraverso filtri minerali. 2. Method according to claim 1, characterized in that the dehumidification step is carried out by means of compressed air filtered through mineral filters. 3. Metodo secondo la rivendicazione 1, caratterizzato dal fatto che la fase di stampaggio ad iniezione à ̈ effettuata mantenendo lo stampo ad una temperatura compresa tra 10 e 18 gradi centigradi. 3. Method according to claim 1, characterized in that the injection molding step is carried out by maintaining the mold at a temperature between 10 and 18 degrees centigrade. 4. Metodo secondo la rivendicazione 1, caratterizzato dal fatto che la fase di prelievo e deposito à ̈ effettuata tramite un robot Cartesiano che utilizza la tecnica del vuoto per aspirare detta lente direttamente dallo stampo e trasportare detta lente ad un'area di stoccaggio. 4. Method according to claim 1, characterized in that the pick-up and deposit step is carried out by means of a Cartesian robot which uses the vacuum technique to suck said lens directly from the mold and transport said lens to a storage area. 5. Apparecchiatura per la produzione di singole lenti di presentazione mediante il procedimento secondo la rivendicazione 1 , caratterizzata dal fatto di comprendere un deumidificatore per polietilene tereftalato in granuli, una pressa di iniezione ed uno stampo di iniezione, una centralina per raffreddare continuamente ad una bassa temperatura l’esterno di detto stampo, detta centralina di refrigerazione essendo una centralina di refrigerazione a circuito chiuso in grado di mantenere un liquido refrigerante ad una temperatura compresa tra 7 e 20 gradi centigradi, ed un robot Cartesiano, funzionante a vuoto, per il prelievo ed il deposito di ciascuna singola lente finita. 5. Apparatus for the production of single presentation lenses by the process according to claim 1, characterized in that it comprises a dehumidifier for polyethylene terephthalate in granules, an injection press and an injection mold, a control unit for continuously cooling to a low temperature on the outside of said mold, said refrigeration unit being a closed-circuit refrigeration unit capable of maintaining a coolant at a temperature between 7 and 20 degrees centigrade, and a Cartesian robot, operating in vacuum, for removal and deposit of each single finished lens. 6. Apparecchiatura secondo la rivendicazione 5, caratterizzata dal fatto che il deumidificatore utilizza aria compressa filtrata attraverso filtri minerali. 6. Apparatus according to claim 5, characterized in that the dehumidifier uses compressed air filtered through mineral filters. 7. Apparecchiatura secondo la rivendicazione 5, caratterizzata dal fatto che detta centralina mantiene detto stampo ad una temperatura compresa tra 10 e 18 gradi centigradi. 7. Apparatus according to claim 5, characterized in that said control unit maintains said mold at a temperature comprised between 10 and 18 degrees centigrade. 8. Apparecchiatura secondo la rivendicazione 5, caratterizzata dal fatto che detto stampo comprende un sistema di raffreddamento spinto dotato di ricircoli di liquido refrigerante che arrivano a raffreddare anche il tassello sagomante detta lente. 8. Apparatus according to claim 5, characterized in that said mold comprises a high-pressure cooling system equipped with recirculation of refrigerant liquid which also cools the block shaping said lens. 9. Lente di presentazione perfezionata caratterizzata dal fatto di essere prodotta mediante il procedimento secondo la rivendicazione 1 e l'apparecchiatura secondo la rivendicazione 5.9. Improved presentation lens characterized in that it is produced by the method according to claim 1 and the apparatus according to claim 5.
ITMI2009A000080A 2009-01-26 2009-01-26 METHOD FOR THE PRODUCTION OF PRESENTATION LENSES. IT1393078B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
ITMI2009A000080A IT1393078B1 (en) 2009-01-26 2009-01-26 METHOD FOR THE PRODUCTION OF PRESENTATION LENSES.

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Application Number Priority Date Filing Date Title
ITMI2009A000080A IT1393078B1 (en) 2009-01-26 2009-01-26 METHOD FOR THE PRODUCTION OF PRESENTATION LENSES.

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ITMI20090080A1 true ITMI20090080A1 (en) 2010-07-27
IT1393078B1 IT1393078B1 (en) 2012-04-11

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Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0821979A (en) * 1994-07-04 1996-01-23 Masahito Takeuchi Demonstration lens blank for spectacles and production of demonstration lens formed by using the same
EP0881246A2 (en) * 1997-05-28 1998-12-02 Shimadzu Corporation Biodegradable resin for forming spectacle-molded body and spectacle-molded body
JP2000015662A (en) * 1998-07-06 2000-01-18 Canon Inc Method for supplying resin material for molding machine, molding, molding machine, and resin material supplying apparatus for molding machine
JP2001018266A (en) * 1999-07-05 2001-01-23 Yushin Precision Equipment Co Ltd Injection molded product taking-out apparatus
JP2001028266A (en) * 1999-07-06 2001-01-30 Mitsubishi Chemicals Corp Battery electrode containing surface modifying component, battery, and manufacture thereof
WO2002020254A1 (en) * 2000-09-08 2002-03-14 Sola International, Inc Process for molding thermoplastic lenses and, steeply curved and/or thin lenses produced thereby
US20040232030A1 (en) * 2003-05-19 2004-11-25 Tomoaki Koseki PET resin mold processed goods
WO2005077628A1 (en) * 2004-02-16 2005-08-25 Plastic Systems S.P.A. Process and plant for dehumidification, heating and injection moulding of granulated plastics materials

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0821979A (en) * 1994-07-04 1996-01-23 Masahito Takeuchi Demonstration lens blank for spectacles and production of demonstration lens formed by using the same
EP0881246A2 (en) * 1997-05-28 1998-12-02 Shimadzu Corporation Biodegradable resin for forming spectacle-molded body and spectacle-molded body
JP2000015662A (en) * 1998-07-06 2000-01-18 Canon Inc Method for supplying resin material for molding machine, molding, molding machine, and resin material supplying apparatus for molding machine
JP2001018266A (en) * 1999-07-05 2001-01-23 Yushin Precision Equipment Co Ltd Injection molded product taking-out apparatus
JP2001028266A (en) * 1999-07-06 2001-01-30 Mitsubishi Chemicals Corp Battery electrode containing surface modifying component, battery, and manufacture thereof
WO2002020254A1 (en) * 2000-09-08 2002-03-14 Sola International, Inc Process for molding thermoplastic lenses and, steeply curved and/or thin lenses produced thereby
US20040232030A1 (en) * 2003-05-19 2004-11-25 Tomoaki Koseki PET resin mold processed goods
WO2005077628A1 (en) * 2004-02-16 2005-08-25 Plastic Systems S.P.A. Process and plant for dehumidification, heating and injection moulding of granulated plastics materials

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
DATABASE WPI Week 200014, Derwent World Patents Index; AN 2000-155497, XP002554515 *
DATABASE WPI Week 200124, Derwent World Patents Index; AN 2001-229477, XP002554514 *

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