IN2015DN03728A - - Google Patents

Info

Publication number
IN2015DN03728A
IN2015DN03728A IN3728DEN2015A IN2015DN03728A IN 2015DN03728 A IN2015DN03728 A IN 2015DN03728A IN 3728DEN2015 A IN3728DEN2015 A IN 3728DEN2015A IN 2015DN03728 A IN2015DN03728 A IN 2015DN03728A
Authority
IN
India
Prior art keywords
compound
oxazolidinone
relates
epoxide
astm
Prior art date
Application number
Inventor
Thomas Ernst Müller
Christoph Gürtler
Susmit Basu
Walter Leitner
Original Assignee
Bayer Materialscience Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Materialscience Ag filed Critical Bayer Materialscience Ag
Publication of IN2015DN03728A publication Critical patent/IN2015DN03728A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/003—Polymeric products of isocyanates or isothiocyanates with epoxy compounds having no active hydrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/75—Polyisocyanates or polyisothiocyanates cyclic cycloaliphatic
    • C08G18/758—Polyisocyanates or polyisothiocyanates cyclic cycloaliphatic containing two or more cycloaliphatic rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/22—Catalysts containing metal compounds
    • C08G18/222—Catalysts containing metal compounds metal compounds not provided for in groups C08G18/225 - C08G18/26
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/22—Catalysts containing metal compounds
    • C08G18/225—Catalysts containing metal compounds of alkali or alkaline earth metals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/22—Catalysts containing metal compounds
    • C08G18/227—Catalysts containing metal compounds of antimony, bismuth or arsenic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3203—Polyhydroxy compounds
    • C08G18/3218—Polyhydroxy compounds containing cyclic groups having at least one oxygen atom in the ring
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/71—Monoisocyanates or monoisothiocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
    • C08G59/22—Di-epoxy compounds
    • C08G59/26—Di-epoxy compounds heterocyclic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
    • C08G59/4007—Curing agents not provided for by the groups C08G59/42 - C08G59/66
    • C08G59/4014—Nitrogen containing compounds
    • C08G59/4028—Isocyanates; Thioisocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/02—Polycondensates containing more than one epoxy group per molecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2400/00—Characterised by the use of unspecified polymers
    • C08J2400/14—Water soluble or water swellable polymers, e.g. aqueous gels
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/09—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in organic liquids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Catalysts (AREA)

Abstract

The present invention relates to a method for the production of oxazolidinone compounds comprising the step of slowly reacting an isocyanate compound with an epoxide compound in the presence of a Lewis acid catalyst. The invention further relates to an oxazolidinone compound obtainable by a method according to the invention with a colour as determined according to ASTM D1209 05 (2011) of = 200 and a molar ratio of the oxazolidinone compound to isocyanurate by¬ product o/i of = 85/15. Lastly the invention relates to an oligomeric or polymeric oxazolidinone compound obtainable by a method according to the invention using an isocyanate compound with two or more NCO groups per molecule and an epoxide compound with two or more epoxy groups per molecule comprising at least two units derived from the isocyanate compound and at least two units derived from the epoxide compound with a colour as determined according to ASTM D1209 05 (2011) of = 200.
IN3728DEN2015 2012-11-14 2013-11-11 IN2015DN03728A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12192611 2012-11-14
PCT/EP2013/073468 WO2014076024A1 (en) 2012-11-14 2013-11-11 Method for the production of oxazolidinone compounds

Publications (1)

Publication Number Publication Date
IN2015DN03728A true IN2015DN03728A (en) 2015-09-18

Family

ID=47177827

Family Applications (1)

Application Number Title Priority Date Filing Date
IN3728DEN2015 IN2015DN03728A (en) 2012-11-14 2013-11-11

Country Status (11)

Country Link
US (1) US9458281B2 (en)
EP (1) EP2920218B1 (en)
KR (1) KR20150084957A (en)
CN (1) CN104797614A (en)
BR (1) BR112015010973A2 (en)
CA (1) CA2891200A1 (en)
IN (1) IN2015DN03728A (en)
MX (1) MX2015006088A (en)
RU (1) RU2015122509A (en)
SG (1) SG11201503362QA (en)
WO (1) WO2014076024A1 (en)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103834168B (en) 2014-02-25 2016-09-07 广东生益科技股份有限公司 A kind of halogen-free flame resistance resin composite
US20170081462A1 (en) * 2014-05-12 2017-03-23 Covestro Deutschland Ag Catalysts for the synthesis of oxazolidinone compounds
CN105778414B (en) 2014-12-26 2018-05-29 广东生益科技股份有限公司 A kind of composition epoxy resin and use its prepreg and laminate
ES2731925T3 (en) * 2015-02-13 2019-11-19 Covestro Deutschland Ag Procedure for the synthesis of polyoxazolidinone compounds with high stability
CN105153059B (en) * 2015-09-11 2018-03-06 苏州大学 The preparation method of Yi Zhong oxazolidinone compounds
CN105524253A (en) * 2015-12-15 2016-04-27 广东广山新材料有限公司 Isocyanate modified epoxy resin and application thereof
CN106916282B (en) * 2015-12-28 2019-07-26 广东生益科技股份有限公司 A kind of composition epoxy resin and prepreg and laminate using it
CN107227001B (en) 2016-03-25 2019-06-14 广东生益科技股份有限公司 A kind of halogen-free thermosetting resin composite and prepreg, laminate and printed circuit board containing it
JP2019526664A (en) 2016-08-19 2019-09-19 コベストロ、ドイチュラント、アクチエンゲゼルシャフトＣｏｖｅｓｔｒｏ Ｄｅｕｔｓｃｈｌａｎｄ Ａｇ Synthesis method of polyoxazolidinone compounds
EP3357949A1 (en) * 2017-02-02 2018-08-08 Covestro Deutschland AG Method for the production of polyoxazolidinone polymer compounds
KR102587180B1 (en) * 2017-02-16 2023-10-06 바스프 에스이 Polyoxazolidone and its preparation method
EP3456754A1 (en) * 2017-09-15 2019-03-20 Covestro Deutschland AG Method for the production of thermoplastic polyoxazolidinone polymers
EP3456753A1 (en) * 2017-09-15 2019-03-20 Covestro Deutschland AG Method for the production of thermplastic polyoxazolidinone polymers
EP3694897A1 (en) 2017-10-13 2020-08-19 Covestro Deutschland AG Method for producing a cross-linkable polymer with the formation of oxazolidinones
BR112020005370A2 (en) 2017-10-27 2020-09-24 Huntsman International Llc method for the production of oxazolidinone compounds, and, use of compounds.
WO2020016276A1 (en) 2018-07-18 2020-01-23 Basf Se Bulk polymerisation of polyoxazolidone
US20210261715A1 (en) * 2018-07-30 2021-08-26 Dow Global Technologies Llc Curable resin composition
EP3604370A1 (en) 2018-08-03 2020-02-05 Covestro Deutschland AG Catalysts for the synthesis of oxazolidinones
CN112839972B (en) * 2018-09-10 2022-11-04 亨茨曼国际有限公司 Oxazolidinedione terminated prepolymers
US20210324132A1 (en) * 2018-09-10 2021-10-21 Huntsman International Llc Oxazolidinedione-terminated prepolymer
EP3640276A1 (en) * 2018-10-16 2020-04-22 SABIC Global Technologies B.V. High heat epoxy-terminated polyoxazolidones, compositions, methods of manufacture, and uses thereof
EP3647335A1 (en) * 2018-10-30 2020-05-06 Covestro Deutschland AG Method for the production of thermoplastic polyoxazolidinone polymers
EP3647336A1 (en) 2018-10-30 2020-05-06 Covestro Deutschland AG Method for the production of thermoplastic polyoxazolidinone polymers
EP3750934A1 (en) * 2019-06-12 2020-12-16 Covestro Deutschland AG Method for the production of isocyanate-group terminated polyoxazolidinones
EP3750933A1 (en) * 2019-06-12 2020-12-16 Covestro Deutschland AG Method for the production of epoxy-group terminated polyoxazolidinones
CN110790919B (en) * 2019-08-01 2022-03-29 宁夏清研高分子新材料有限公司 Soluble polyaryletherketone terpolymer and synthesis method thereof
US20210253772A1 (en) 2020-02-18 2021-08-19 Covestro Llc Polyoxazolidinone compositions
EP3964536A1 (en) 2021-02-23 2022-03-09 Basf Se Polyoxazolidinone intermediate containing an antioxidant

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3020262A (en) 1957-12-19 1962-02-06 Jefferson Chem Co Inc Method for producing 2-oxazolidones from epoxides and isocyanates
US3471442A (en) 1967-02-02 1969-10-07 American Cyanamid Co Process for the preparation of thermoplastic polymers prepared by reacting diepoxide monomers with aromatic diisocyanates
US4658007A (en) 1985-05-07 1987-04-14 The Dow Chemical Company Polyisocyanurate-based polyoxazolidone polymers and process for their preparation
JP2010539287A (en) * 2007-09-11 2010-12-16 ダウ グローバル テクノロジーズ インコーポレイティド Isocyanate-modified epoxy resin for fused epoxy foam
BRPI0816499A2 (en) * 2007-10-05 2019-09-24 Dow Global Technologies Inc powder coating epoxy resin composition and article
BRPI0817181A8 (en) 2007-10-31 2016-12-20 Dow Global Technologies Inc THERMOSET POLYMER CONTAINING EPOXY-TERMINATED OXAZOLIDINONE RING, THERMOSET POWDER COATING COMPOSITION, SUBSTRATE, METHOD FOR PROVIDING A SUBSTRATE WITH A FUSION-BONDED EPOXY COATING (FBE), COATED SUBSTRATE, METHOD FOR PREPARING A POLYMER CONTAINING AN OXAZOLIDIN PORONE RING EPOXY AND POLYMER

Also Published As

Publication number Publication date
KR20150084957A (en) 2015-07-22
CA2891200A1 (en) 2014-05-22
EP2920218A1 (en) 2015-09-23
US20150291726A1 (en) 2015-10-15
MX2015006088A (en) 2015-08-06
SG11201503362QA (en) 2015-05-28
CN104797614A (en) 2015-07-22
US9458281B2 (en) 2016-10-04
EP2920218B1 (en) 2020-09-30
RU2015122509A (en) 2017-01-10
BR112015010973A2 (en) 2017-08-29
WO2014076024A1 (en) 2014-05-22

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