IN2015DN03228A - - Google Patents
Info
- Publication number
- IN2015DN03228A IN2015DN03228A IN3228DEN2015A IN2015DN03228A IN 2015DN03228 A IN2015DN03228 A IN 2015DN03228A IN 3228DEN2015 A IN3228DEN2015 A IN 3228DEN2015A IN 2015DN03228 A IN2015DN03228 A IN 2015DN03228A
- Authority
- IN
- India
- Prior art keywords
- ammonium metavanadate
- leach
- slurry
- recover
- liquid separation
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/20—Obtaining niobium, tantalum or vanadium
- C22B34/22—Obtaining vanadium
- C22B34/225—Obtaining vanadium from spent catalysts
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Catalysts (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Processing Of Solid Wastes (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
A method for recovering vanadium from a spent slurry catalyst for hydrocarbon oil hydroprocessing is disclosed. In one embodiment after de oiling the spent catalyst is treated with ammonia and air forming a leach slurry. The leach slurry is subsequently treated with a flocculant. After solid liquid separation to recover the solid residue containing coke and ammonium metavanadate the solid residue is washed with an ammonium sulfate solution and leached with hot water. After solid liquid separation to recover a solution containing ammonium metavanadate the ammonium metavanadate is crystallized and purified from the leach solution.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US13/784,325 US8815185B1 (en) | 2013-03-04 | 2013-03-04 | Recovery of vanadium from petroleum coke slurry containing solubilized base metals |
PCT/US2013/070725 WO2014137419A1 (en) | 2013-03-04 | 2013-11-19 | Recovery of vanadium from petroleum coke slurry containing solubilized base metals |
Publications (1)
Publication Number | Publication Date |
---|---|
IN2015DN03228A true IN2015DN03228A (en) | 2015-10-02 |
Family
ID=49679687
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
IN3228DEN2015 IN2015DN03228A (en) | 2013-03-04 | 2013-11-19 |
Country Status (7)
Country | Link |
---|---|
US (1) | US8815185B1 (en) |
EP (1) | EP2964795A1 (en) |
CN (1) | CN104755641A (en) |
CA (1) | CA2885073A1 (en) |
IN (1) | IN2015DN03228A (en) |
RU (1) | RU2015111518A (en) |
WO (1) | WO2014137419A1 (en) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9580770B2 (en) | 2014-10-22 | 2017-02-28 | Chevron U.S.A. Inc. | Process for preparing a spent catalyst for precious metals recovery |
US10017837B2 (en) | 2014-10-22 | 2018-07-10 | Chevron U.S.A. Inc. | Metallurgical extraction technique to recover platinum group metals from a filter cake |
CN104386747B (en) * | 2014-11-18 | 2016-03-30 | 河北钢铁股份有限公司承德分公司 | A kind of ion exchange method prepares the method for high purity barium oxide |
CN104628035A (en) * | 2015-01-06 | 2015-05-20 | 大连东泰资源再生有限公司 | Resourceful utilization method of waste catalyst |
CN109207721B (en) * | 2018-10-17 | 2020-06-12 | 中国科学院过程工程研究所 | Method for crystallizing and separating ammonium metavanadate from vanadium-containing raw material roasting clinker leaching solution |
WO2023154077A1 (en) | 2022-02-14 | 2023-08-17 | Chevron U.S.A. Inc. | Metals recovery from spent supported catalyst |
US11682801B1 (en) | 2022-06-08 | 2023-06-20 | Aleon Renewable Metals, Llc. | Processes for recycling spent catalysts, recycling rechargeable batteries, and integrated processes thereof |
Family Cites Families (59)
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US3653816A (en) | 1970-05-28 | 1972-04-04 | Sylvania Electric Prod | Production of ammonium metavanadate |
JPS593936B2 (en) | 1977-01-20 | 1984-01-26 | 千代田化工建設株式会社 | Method for recovering panadium and nickel deposited on waste catalyst |
US4243639A (en) | 1979-05-10 | 1981-01-06 | Tosco Corporation | Method for recovering vanadium from petroleum coke |
JPS6041612B2 (en) | 1980-12-02 | 1985-09-18 | 工業技術院長 | Method for extracting molybdenum and vanadium from desulfurization waste catalyst |
US4420464A (en) | 1981-10-26 | 1983-12-13 | Rockwell International Corporation | Recovery of vanadium from carbonaceous materials |
US4443415A (en) | 1982-06-22 | 1984-04-17 | Amax Inc. | Recovery of V2 O5 and nickel values from petroleum coke |
US4536374A (en) | 1983-07-25 | 1985-08-20 | Gulf Canada Limited | Process using carbonate reagent for recovering vanadium from cokes and ashes derived from heavy oils |
US4554138A (en) | 1984-10-30 | 1985-11-19 | Chevron Research Company | Leaching metals from spent hydroprocessing catalysts with ammonium sulfate |
CA1293380C (en) | 1985-12-11 | 1991-12-24 | Just Jan Christiaan Jansz | Vanadium recovery process |
US5702500A (en) | 1995-11-02 | 1997-12-30 | Gulf Chemical & Metallurgical Corporation | Integrated process for the recovery of metals and fused alumina from spent catalysts |
JPH10152325A (en) | 1996-11-19 | 1998-06-09 | Kashima Kita Kyodo Hatsuden Kk | Production of ammonium metavanadate |
US6033637A (en) | 1996-12-25 | 2000-03-07 | Kashima-Kita, Electric Power Corporation | Method for treating combustion ashes |
CA2331322C (en) | 1998-05-08 | 2009-09-29 | Shell Oil Company | Process to recover molybdenum and vanadium metals from spent catalyst by alkaline leaching |
US6241806B1 (en) | 1998-06-09 | 2001-06-05 | Marathon Ashland Petroleum, Llc | Recovering vanadium from petroleum coke as dust |
US6231640B1 (en) | 1998-06-09 | 2001-05-15 | Marathon Ashland Petroleum Llc | Dissolving petroleum coke in molten iron to recover vanadium metal |
US6235253B1 (en) | 1998-06-09 | 2001-05-22 | Marathon Ashland Petroleum, Llc | Recovering vanadium oxides from petroleum coke by melting |
JP2005200231A (en) | 2004-01-13 | 2005-07-28 | Kashima Kita Electric Power Corp | Method for producing ammonium metavanadate |
JP2005298925A (en) | 2004-04-13 | 2005-10-27 | Ysk Techno System:Kk | Method for recovering vanadium compound from vanadium-containing matter |
US10941353B2 (en) | 2004-04-28 | 2021-03-09 | Hydrocarbon Technology & Innovation, Llc | Methods and mixing systems for introducing catalyst precursor into heavy oil feedstock |
JP5318410B2 (en) | 2004-04-28 | 2013-10-16 | ヘッドウォーターズ ヘビー オイル リミテッド ライアビリティ カンパニー | Boiling bed hydroprocessing method and system and method for upgrading an existing boiling bed system |
EP1753845B1 (en) | 2004-04-28 | 2018-01-03 | Headwaters Heavy Oil, LLC | Fixed bed hydroprocessing methods and systems and methods for upgrading an existing fixed bed system |
EP2813562A1 (en) | 2004-04-28 | 2014-12-17 | Headwaters Heavy Oil, LLC | Hydroprocessing method and system for upgrading heavy oil using a colloidal or molecular catalyst |
US7214309B2 (en) | 2004-09-10 | 2007-05-08 | Chevron U.S.A. Inc | Process for upgrading heavy oil using a highly active slurry catalyst composition |
US7431824B2 (en) | 2004-09-10 | 2008-10-07 | Chevron U.S.A. Inc. | Process for recycling an active slurry catalyst composition in heavy oil upgrading |
US7238273B2 (en) | 2004-09-10 | 2007-07-03 | Chevron U.S.A. Inc | Process for upgrading heavy oil using a highly active slurry catalyst composition |
US7737072B2 (en) | 2004-09-10 | 2010-06-15 | Chevron Usa Inc. | Hydroprocessing bulk catalyst and uses thereof |
US20060058174A1 (en) | 2004-09-10 | 2006-03-16 | Chevron U.S.A. Inc. | Highly active slurry catalyst composition |
US7591942B2 (en) | 2004-09-22 | 2009-09-22 | Exxonmobil Research And Engineering Company | Bulk bi-metallic catalysts made from precursors containing an organic agent |
US7375143B2 (en) | 2004-11-22 | 2008-05-20 | Conocophillips Company | Catalyst recover from a slurry |
US7485267B2 (en) | 2005-07-29 | 2009-02-03 | Chevron U.S.A. Inc. | Process for metals recovery from spent catalyst |
US7897537B2 (en) | 2005-11-23 | 2011-03-01 | University Of Calgary | Ultradispersed catalyst compositions and methods of preparation |
US7431823B2 (en) | 2005-12-16 | 2008-10-07 | Chevron U.S.A. Inc. | Process for upgrading heavy oil using a highly active slurry catalyst composition |
US7708877B2 (en) | 2005-12-16 | 2010-05-04 | Chevron Usa Inc. | Integrated heavy oil upgrading process and in-line hydrofinishing process |
US7390398B2 (en) | 2005-12-16 | 2008-06-24 | Chevron U.S.A. Inc. | Process for upgrading heavy oil using a highly active slurry catalyst composition |
US7431822B2 (en) | 2005-12-16 | 2008-10-07 | Chevron U.S.A. Inc. | Process for upgrading heavy oil using a reactor with a novel reactor separation system |
US7674369B2 (en) | 2006-12-29 | 2010-03-09 | Chevron U.S.A. Inc. | Process for recovering ultrafine solids from a hydrocarbon liquid |
ITMI20071198A1 (en) | 2007-06-14 | 2008-12-15 | Eni Spa | IMPROVED PROCEDURE FOR THE HYDROCONVERSION OF HEAVY OILS WITH BULLETS |
WO2009058861A2 (en) | 2007-10-31 | 2009-05-07 | Chevron U.S.A. Inc. | Hydroprocessing bulk catalyst and uses thereof |
US7658895B2 (en) | 2007-11-28 | 2010-02-09 | Chevron U.S.A. Inc | Process for recovering base metals from spent hydroprocessing catalyst |
US7737068B2 (en) | 2007-12-20 | 2010-06-15 | Chevron U.S.A. Inc. | Conversion of fine catalyst into coke-like material |
US7790646B2 (en) | 2007-12-20 | 2010-09-07 | Chevron U.S.A. Inc. | Conversion of fine catalyst into coke-like material |
US8221710B2 (en) | 2007-11-28 | 2012-07-17 | Sherritt International Corporation | Recovering metals from complex metal sulfides |
US7846404B2 (en) | 2007-11-28 | 2010-12-07 | Chevron U.S.A. Inc. | Process for separating and recovering base metals from used hydroprocessing catalyst |
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US8722556B2 (en) | 2007-12-20 | 2014-05-13 | Chevron U.S.A. Inc. | Recovery of slurry unsupported catalyst |
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GB2456537A (en) | 2008-01-17 | 2009-07-22 | Grimley Smith Associates | Process for vanadium recovery from residues |
US20090023965A1 (en) | 2008-05-01 | 2009-01-22 | Intevep, S.A. | Dispersed metal sulfide-based catalysts |
US7897036B2 (en) | 2008-09-18 | 2011-03-01 | Chevron U.S.A. Inc. | Systems and methods for producing a crude product |
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US20100163499A1 (en) | 2008-12-30 | 2010-07-01 | Odueyungbo Seyi A | Optimizing solid / liquid separation with solvent addition |
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IT1398278B1 (en) | 2009-06-10 | 2013-02-22 | Eni Spa | PROCEDURE FOR RECOVERING METALS FROM A CURRENT RICH IN HYDROCARBONS AND CARBON RESIDUES |
US8636967B2 (en) | 2010-01-21 | 2014-01-28 | Intevep, S.A. | Metal recovery from hydroconverted heavy effluent |
GB2478332A (en) | 2010-03-04 | 2011-09-07 | Grimley Smith Associates | Method of metals recovery from refinery residues |
US8815184B2 (en) | 2010-08-16 | 2014-08-26 | Chevron U.S.A. Inc. | Process for separating and recovering metals |
-
2013
- 2013-03-04 US US13/784,325 patent/US8815185B1/en not_active Expired - Fee Related
- 2013-11-19 WO PCT/US2013/070725 patent/WO2014137419A1/en active Application Filing
- 2013-11-19 IN IN3228DEN2015 patent/IN2015DN03228A/en unknown
- 2013-11-19 CA CA2885073A patent/CA2885073A1/en not_active Abandoned
- 2013-11-19 RU RU2015111518A patent/RU2015111518A/en not_active Application Discontinuation
- 2013-11-19 CN CN201380056032.7A patent/CN104755641A/en active Pending
- 2013-11-19 EP EP13798519.8A patent/EP2964795A1/en not_active Withdrawn
Also Published As
Publication number | Publication date |
---|---|
US8815185B1 (en) | 2014-08-26 |
US20140248199A1 (en) | 2014-09-04 |
CA2885073A1 (en) | 2014-09-12 |
CN104755641A (en) | 2015-07-01 |
RU2015111518A (en) | 2017-04-10 |
WO2014137419A1 (en) | 2014-09-12 |
EP2964795A1 (en) | 2016-01-13 |
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