IN2015DN00743A - - Google Patents

Info

Publication number
IN2015DN00743A
IN2015DN00743A IN743DEN2015A IN2015DN00743A IN 2015DN00743 A IN2015DN00743 A IN 2015DN00743A IN 743DEN2015 A IN743DEN2015 A IN 743DEN2015A IN 2015DN00743 A IN2015DN00743 A IN 2015DN00743A
Authority
IN
India
Prior art keywords
chloride
aluminium
containing stock
mixed
ammonium
Prior art date
Application number
Inventor
Aleksandr Sergeevich Senyuta
Andrey Vladimirovich Panov
Original Assignee
Obsh Estvo S Ogranichennoy Otvetstvennostyu Obedinennaya Kompaniya Rusal Inzh T Ts
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Obsh Estvo S Ogranichennoy Otvetstvennostyu Obedinennaya Kompaniya Rusal Inzh T Ts filed Critical Obsh Estvo S Ogranichennoy Otvetstvennostyu Obedinennaya Kompaniya Rusal Inzh T Ts
Publication of IN2015DN00743A publication Critical patent/IN2015DN00743A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/30—Preparation of aluminium oxide or hydroxide by thermal decomposition or by hydrolysis or oxidation of aluminium compounds
    • C01F7/306—Thermal decomposition of hydrated chlorides, e.g. of aluminium trichloride hexahydrate
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/34—Preparation of aluminium hydroxide by precipitation from solutions containing aluminium salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/44—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water
    • C01F7/441—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water by calcination
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/48—Halides, with or without other cations besides aluminium
    • C01F7/56—Chlorides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00—Compounds of iron
    • C01G49/02—Oxides; Hydroxides
    • C01G49/06—Ferric oxide [Fe2O3]
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B21/00—Obtaining aluminium
    • C22B21/0015—Obtaining aluminium by wet processes
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • C22B3/10—Hydrochloric acid, other halogenated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Abstract

The invention relates to metallurgy in particular to acidic methods for producing alumina and can be used in the processing of low grade aluminium containing stock. The method for producing alumina comprises burning the aluminium containing stock treating the product with hydrochloric acid salting out aluminium chloride by saturating the clarified chloride solution with gaseous hydrogen chloride calcining the aluminium chloride in order to produce aluminium oxide and pyrohydrolyzing the mother liquor with the hydrogen chloride being returned to the acid treatment stage and being salted out. In order to increase the quality of the alumina and reduce energy consumption the aluminium chloride precipitated during the salting out process is treated with ammonium hydroxide the residue produced is sent for calcination and the solution of ammonium chloride is mixed with the aluminium containing stock before the latter is burned or during the burning process ammonia separated out during the burning is dissolved in water and the ammonium hydroxide produced is sent for treating the aluminium chloride. The solution of ammonium chloride can be subjected to phased concentration by evaporation with repeated use of heating steam before being mixed with the aluminium containing stock. The ammonium chloride separated out when concentrating the ammonium chloride by evaporation can be mixed with the aluminium containing stock.
IN743DEN2015 2012-07-20 2012-07-20 IN2015DN00743A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/RU2012/000592 WO2014014379A1 (en) 2012-07-20 2012-07-20 Method for producing alumina

Publications (1)

Publication Number Publication Date
IN2015DN00743A true IN2015DN00743A (en) 2015-07-10

Family

ID=49949094

Family Applications (1)

Application Number Title Priority Date Filing Date
IN743DEN2015 IN2015DN00743A (en) 2012-07-20 2012-07-20

Country Status (7)

Country Link
US (1) US9517944B2 (en)
CN (1) CN104507867B (en)
AU (1) AU2012385519B2 (en)
CA (1) CA2877650C (en)
IN (1) IN2015DN00743A (en)
RU (1) RU2554136C2 (en)
WO (1) WO2014014379A1 (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014120037A1 (en) * 2013-02-04 2014-08-07 Общество с ограниченной ответственностью "Объединенная Компания РУСАЛ Инженерно-технологический центр" Aluminum oxide
AU2013377154B2 (en) * 2013-02-04 2017-10-26 Obshchestvo S Ogranichennoy Otvetstvennost'yu "Ob'edinennaya Kompaniya Rusal Inzhenerno-Tekhnologicheskiy Tsentr" Aluminum oxide production method
WO2016064558A1 (en) * 2014-10-24 2016-04-28 Halliburton Energy Services, Inc. Methods to make ceramic proppants
RU2647041C1 (en) * 2016-09-30 2018-03-13 Общество с ограниченной ответственностью "Объединенная Компания РУСАЛ Инженерно-технологический центр" Method of producing metallurgical alumina (variants)
CN106800346A (en) * 2017-02-07 2017-06-06 泰山医学院 A kind of method of integrated treatment containing alchlor industrial wastewater
RU2705071C1 (en) * 2018-11-07 2019-11-01 Федеральное государственное автономное образовательное учреждение высшего образования "Национальный исследовательский технологический университет "МИСиС" Method of producing metallurgical alumina by an acid-alkaline method
US11746021B2 (en) 2019-04-18 2023-09-05 Nextchem, Llc High purity aluminum oxide via electrodialysis
CN110217812A (en) * 2019-07-12 2019-09-10 神华准能资源综合开发有限公司 A method of aluminium oxide is prepared by crystal aluminum chloride
AU2021209433A1 (en) * 2020-01-20 2022-07-21 Tianqi Lithium Kwinana Pty Ltd A process for producing alumina and a lithium salt
CN111689508B (en) * 2020-06-15 2021-12-28 浙江新安化工集团股份有限公司 Method for treating tetrachloro sodium aluminate solid slag
CN116177580B (en) * 2021-11-29 2024-12-17 国家能源投资集团有限责任公司 Soxhlet purification device and method for purifying crude crystalline aluminum chloride
EP4469400A4 (en) * 2022-01-25 2026-01-21 Aditya Birla Science And Tech Company Pvt Ltd METHOD FOR THE PRODUCTION OF HIGH-PURITY ALUMINUM OXIDE

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE7703590L (en) * 1976-04-02 1977-10-03 Inst Atomenergi WAY TO EXTRACT ALUMINUM OXIDE
FR2426018A1 (en) * 1978-05-18 1979-12-14 Pechiney Aluminium PROCESS FOR OBTAINING PURE ALUMINA BY HYDROCHLORIC ATTACK OF ALUMINOUS ORES AND EXTRACTION OF IMPURITIES BY A SULFURIC TREATMENT
NO790460L (en) * 1979-02-13 1980-08-14 Elkem Spigerverket As PREPARATION OF A PURE ALUMINUM OXIDE FROM SOLUTIONS CONTAINING DISSOLVED ALUMINUM AND IRON IONS
SU1258815A1 (en) 1985-05-22 1986-09-23 Казахский Ордена Трудового Красного Знамени Политехнический Институт Им.В.И.Ленина Method of producing alumina
SU1669864A1 (en) * 1989-01-03 1991-08-15 Челябинский Государственный Педагогический Институт Method for obtaining alumina
CN1040845C (en) * 1993-07-16 1998-11-25 中国石油化工总公司 Preparation method of microspherical γ-alumina
RU2153466C1 (en) 1999-02-08 2000-07-27 Винокуров Станислав Федорович Method of stripping high-silicon aluminum-containing raw material
US6468483B2 (en) * 2000-02-04 2002-10-22 Goldendale Aluminum Company Process for treating alumina-bearing ores to recover metal values therefrom
CN100584755C (en) * 2008-04-02 2010-01-27 中国高岭土公司 Method for preparing superfine white carbon black and nano-alumina with kaolin as raw material
CN101863501B (en) * 2010-04-27 2012-12-19 中国神华能源股份有限公司 Method for producing superfine aluminum hydroxide and aluminum oxide by using solution of aluminum chloride
CN102502739B (en) * 2011-11-11 2013-09-04 昆明冶金研究院 Method for producing high-purity alpha-aluminum oxide

Also Published As

Publication number Publication date
RU2554136C2 (en) 2015-06-27
CN104507867A (en) 2015-04-08
CA2877650C (en) 2017-08-15
WO2014014379A1 (en) 2014-01-23
RU2013151919A (en) 2015-05-27
AU2012385519B2 (en) 2017-01-05
CA2877650A1 (en) 2014-01-23
US9517944B2 (en) 2016-12-13
CN104507867B (en) 2018-02-09
US20150175435A1 (en) 2015-06-25
AU2012385519A1 (en) 2015-01-22

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