IN2015DN00635A - - Google Patents

Info

Publication number
IN2015DN00635A
IN2015DN00635A IN635DEN2015A IN2015DN00635A IN 2015DN00635 A IN2015DN00635 A IN 2015DN00635A IN 635DEN2015 A IN635DEN2015 A IN 635DEN2015A IN 2015DN00635 A IN2015DN00635 A IN 2015DN00635A
Authority
IN
India
Prior art keywords
alkenone
reaction mixture
hydrogen halide
halogenated precursor
reaction
Prior art date
Application number
Inventor
Max Josef Braun
Stefan Palsherm
Original Assignee
Solvay
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Solvay filed Critical Solvay
Publication of IN2015DN00635A publication Critical patent/IN2015DN00635A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/65—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by splitting-off hydrogen atoms or functional groups; by hydrogenolysis of functional groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/41—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrogenolysis or reduction of carboxylic groups or functional derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

A process for the manufacture of an alkenone comprising the steps of: (a) providing a halogenated precursor of the alkenone and (b) subjecting at least a fraction of the halogenated precursor of step (a) to a thermolysis reaction to form a reaction mixture comprising the alkenone and a hydrogen halide wherein the hydrogen halide is removed from the reaction mixture by cyclonic separation is described.
IN635DEN2015 2012-08-22 2013-08-20 IN2015DN00635A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12181334 2012-08-22
PCT/EP2013/067344 WO2014029786A1 (en) 2012-08-22 2013-08-20 Process for the manufacture of alkenones

Publications (1)

Publication Number Publication Date
IN2015DN00635A true IN2015DN00635A (en) 2015-06-26

Family

ID=49084984

Family Applications (1)

Application Number Title Priority Date Filing Date
IN635DEN2015 IN2015DN00635A (en) 2012-08-22 2013-08-20

Country Status (7)

Country Link
US (1) US9365480B2 (en)
EP (1) EP2888219B1 (en)
JP (1) JP6426090B2 (en)
CN (1) CN104583167B (en)
DK (1) DK2888219T3 (en)
IN (1) IN2015DN00635A (en)
WO (1) WO2014029786A1 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104072347B (en) * 2014-06-30 2016-07-13 湖南海利化工股份有限公司 4-alkoxyl-1, the preparation method of 1,1-tri-fluoro-3-butene-2-one
CN112979443A (en) * 2019-12-13 2021-06-18 浙江蓝天环保高科技股份有限公司 Continuous preparation method of trifluoromethyl butenone derivative

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL293952A (en) * 1962-06-12 1900-01-01
US4102985A (en) * 1977-01-06 1978-07-25 Westinghouse Electric Corp. Arc heater production of silicon involving a hydrogen reduction
ES2332037T3 (en) 1995-05-26 2010-01-25 Ishihara Sangyo Kaisha, Ltd. PROCEDURE FOR THE PRODUCTION OF 1,1,1-TRIFLUORO-3-BUTEN-2-ONA SUBSTITUTED.
DE10154943C1 (en) * 2001-11-08 2002-11-21 Wacker Chemie Gmbh Production of chloromethylsilane compounds involves liquid phase photochlorination of corresponding methylsilane compound with substoichiometric amount of chlorine in presence of hydrogen chloride
DE10325715A1 (en) 2003-06-06 2004-12-23 Solvay Fluor Und Derivate Gmbh Simplified production of alkenones
WO2010000871A2 (en) 2008-07-04 2010-01-07 Solvay Sa Process for the manufacture of alkenones
CN106083710B (en) * 2008-09-30 2021-03-12 索尔维公司 Process for the synthesis of halogenated cyclic compounds
ES2537676T3 (en) 2009-07-06 2015-06-10 Solvay Sa Process for the manufacture of halogenated alkenone precursors in the presence of a solvent
MX2012000382A (en) 2009-07-06 2012-03-07 Solvay Process for the manufacture of alkenones.
WO2011003856A1 (en) 2009-07-06 2011-01-13 Solvay Sa Process for the manufacture of halogenated precursors of alkenones under specific conditions
WO2012085195A1 (en) * 2010-12-23 2012-06-28 Solvay Sa Environmental friendly purification of an organic solution of etfbo

Also Published As

Publication number Publication date
EP2888219A1 (en) 2015-07-01
US20150239817A1 (en) 2015-08-27
JP6426090B2 (en) 2018-11-21
EP2888219B1 (en) 2019-02-06
JP2015527354A (en) 2015-09-17
WO2014029786A1 (en) 2014-02-27
CN104583167A (en) 2015-04-29
CN104583167B (en) 2017-09-19
DK2888219T3 (en) 2019-05-13
US9365480B2 (en) 2016-06-14

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