IN2014MN01654A - - Google Patents
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- Publication number
- IN2014MN01654A IN2014MN01654A IN1654MUN2014A IN2014MN01654A IN 2014MN01654 A IN2014MN01654 A IN 2014MN01654A IN 1654MUN2014 A IN1654MUN2014 A IN 1654MUN2014A IN 2014MN01654 A IN2014MN01654 A IN 2014MN01654A
- Authority
- IN
- India
- Prior art keywords
- biopolymer
- substrate
- solution
- graphene
- aqueous
- Prior art date
Links
- 229920001222 biopolymer Polymers 0.000 abstract 7
- 238000000034 method Methods 0.000 abstract 4
- 239000000758 substrate Substances 0.000 abstract 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 3
- 229910021389 graphene Inorganic materials 0.000 abstract 3
- 239000000243 solution Substances 0.000 abstract 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 abstract 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
- 238000002360 preparation method Methods 0.000 abstract 2
- FHVDTGUDJYJELY-UHFFFAOYSA-N 6-{[2-carboxy-4,5-dihydroxy-6-(phosphanyloxy)oxan-3-yl]oxy}-4,5-dihydroxy-3-phosphanyloxane-2-carboxylic acid Chemical compound O1C(C(O)=O)C(P)C(O)C(O)C1OC1C(C(O)=O)OC(OP)C(O)C1O FHVDTGUDJYJELY-UHFFFAOYSA-N 0.000 abstract 1
- 229920001661 Chitosan Polymers 0.000 abstract 1
- 229920002472 Starch Polymers 0.000 abstract 1
- 229940072056 alginate Drugs 0.000 abstract 1
- 229920000615 alginic acid Polymers 0.000 abstract 1
- 235000010443 alginic acid Nutrition 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 229910052786 argon Inorganic materials 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 238000003763 carbonization Methods 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 abstract 1
- 230000003750 conditioning effect Effects 0.000 abstract 1
- 150000004676 glycans Chemical class 0.000 abstract 1
- 238000001027 hydrothermal synthesis Methods 0.000 abstract 1
- 238000007654 immersion Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 238000004377 microelectronic Methods 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 229920001282 polysaccharide Polymers 0.000 abstract 1
- 239000005017 polysaccharide Substances 0.000 abstract 1
- 229920006395 saturated elastomer Polymers 0.000 abstract 1
- 238000004528 spin coating Methods 0.000 abstract 1
- 235000019698 starch Nutrition 0.000 abstract 1
- 239000008107 starch Substances 0.000 abstract 1
- 238000005979 thermal decomposition reaction Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D5/00—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures
- B05D5/12—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures to obtain a coating with specific electrical properties
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/18—Nanoonions; Nanoscrolls; Nanohorns; Nanocones; Nanowalls
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
- H01B1/04—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of carbon-silicon compounds, carbon or silicon
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/184—Preparation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/26—Web or sheet containing structurally defined element or component, the element or component having a specified physical dimension
- Y10T428/263—Coating layer not in excess of 5 mils thick or equivalent
- Y10T428/264—Up to 3 mils
- Y10T428/265—1 mil or less
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/30—Self-sustaining carbon mass or layer with impregnant or other layer
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Composite Materials (AREA)
- Inorganic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
The present invention describes a method for the preparation of films of graphene or of a graphene material by means of biopolymer carbonization. The method comprises the following steps: preparation of an aqueous solution of a non crystallizable biopolymer or a derivative of said biopolymer at a suitable pH; coating the substrate with the aqueous biopolymer solution prepared in the preceding step by means of immersion of the substrate in said solution or by using the spin coating technique; conditioning the aqueous biopolymer solution by means of a hydrothermal process consisting in subjecting the coated surface to a flow of nitrogen or argon saturated with water vapour at a temperature of between 100 and 250°C for a period of time of between 30 min and a number of hours; and thermal decomposition of the biopolymer deposited on the substrate in the absence of oxygen at temperatures below 1200°C. The preferred biopolymers in the present invention include polysaccharides such as alginate chitosan starch and carraghenates and derivatives thereof. Owing to the properties of the graphene the substrates coated by means of this process can be used in the microelectronic and photovoltaic industries as components for solar cells etc.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ES201200100A ES2383356B1 (en) | 2012-02-06 | 2012-02-06 | Procedure for the preparation of graphene films or graphene materials on non-metallic substrates |
| PCT/ES2013/000026 WO2013117780A1 (en) | 2012-02-06 | 2013-02-05 | Method for preparing films of graphene or graphene materials on non-metallic substrates |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IN2014MN01654A true IN2014MN01654A (en) | 2015-05-29 |
Family
ID=46173009
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IN1654MUN2014 IN2014MN01654A (en) | 2012-02-06 | 2013-02-05 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US9216435B2 (en) |
| EP (1) | EP2813469A4 (en) |
| CN (1) | CN104203814A (en) |
| CL (1) | CL2014002066A1 (en) |
| ES (1) | ES2383356B1 (en) |
| IN (1) | IN2014MN01654A (en) |
| MX (1) | MX2014009328A (en) |
| WO (1) | WO2013117780A1 (en) |
| ZA (1) | ZA201405836B (en) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103626158B (en) * | 2012-08-23 | 2016-04-06 | 中国科学院宁波材料技术与工程研究所 | The preparation method of nitrogen-doped graphene and application thereof |
| ES2471318B1 (en) * | 2012-11-22 | 2015-04-24 | Abengoa Solar New Technologies S.A. | Procedure for obtaining suspensions or solid graphene samples |
| CN103839695A (en) * | 2012-11-23 | 2014-06-04 | 海洋王照明科技股份有限公司 | Graphene electrode plate, and preparation method and application thereof |
| JP6201801B2 (en) * | 2014-02-14 | 2017-09-27 | 株式会社デンソー | Method for producing graphite thin film |
| CN103803542B (en) * | 2014-02-24 | 2016-01-20 | 南京理工大学 | A kind of preparation method of microbiological fuel cell mixt bacteria nitrogen-doped graphene |
| CN103922328A (en) * | 2014-04-18 | 2014-07-16 | 山东大学 | Method for preparing nitrogenous hierarchical pore three-dimensional graphene by using chitosan |
| CN104759253B (en) * | 2015-04-14 | 2017-10-20 | 中国广州分析测试中心 | It is a kind of to be used for heavy metal accumulation or the graphene sponge of pollutant gone in water removal and preparation method thereof |
| US11383252B2 (en) | 2015-11-12 | 2022-07-12 | Cornell University | Air controlled electrospray manufacturing and products thereof |
| CN110139896B (en) * | 2016-09-12 | 2021-12-31 | 阿德莱德大学 | Multipurpose graphene-based composite material |
| WO2019010561A1 (en) * | 2017-07-11 | 2019-01-17 | Tofigh Rayhani Mohammad | Graphene coated glass material and uses thereof |
| ES2843743B2 (en) * | 2020-01-20 | 2022-02-15 | Primalchit Solutions S L | ANTICORROSIVE ENAMEL OF CARBONOUS MATERIAL, ITS PROCEDURE FOR OBTAINING AND ITS USE |
| CN113024278A (en) * | 2021-03-04 | 2021-06-25 | 四川大学 | Calcium phosphate ceramic with in-situ graphene film and preparation method and application thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2149853A1 (en) * | 1995-05-19 | 1996-11-20 | Jiayu Simon Xue | Pre-graphitic carbonaceous insertion compounds and use as anodes in rechargeable batteries |
| US9309121B2 (en) * | 2009-07-22 | 2016-04-12 | Wisys Technology Foundation, Inc. | Carbon microbeads with hierarchical structure |
| KR101622304B1 (en) | 2009-08-05 | 2016-05-19 | 삼성전자주식회사 | Substrate comprising graphene and process for preparing the same |
-
2012
- 2012-02-06 ES ES201200100A patent/ES2383356B1/en not_active Expired - Fee Related
-
2013
- 2013-02-04 US US13/758,415 patent/US9216435B2/en not_active Expired - Fee Related
- 2013-02-05 EP EP13746795.7A patent/EP2813469A4/en not_active Withdrawn
- 2013-02-05 MX MX2014009328A patent/MX2014009328A/en unknown
- 2013-02-05 IN IN1654MUN2014 patent/IN2014MN01654A/en unknown
- 2013-02-05 CN CN201380008199.6A patent/CN104203814A/en active Pending
- 2013-02-05 WO PCT/ES2013/000026 patent/WO2013117780A1/en not_active Ceased
-
2014
- 2014-08-04 CL CL2014002066A patent/CL2014002066A1/en unknown
- 2014-08-08 ZA ZA2014/05836A patent/ZA201405836B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| WO2013117780A1 (en) | 2013-08-15 |
| EP2813469A1 (en) | 2014-12-17 |
| ES2383356B1 (en) | 2013-04-04 |
| US20130209793A1 (en) | 2013-08-15 |
| US9216435B2 (en) | 2015-12-22 |
| CL2014002066A1 (en) | 2015-03-13 |
| ZA201405836B (en) | 2015-10-28 |
| MX2014009328A (en) | 2015-02-24 |
| ES2383356A1 (en) | 2012-06-20 |
| EP2813469A4 (en) | 2015-09-16 |
| CN104203814A (en) | 2014-12-10 |
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