IN2014MN01307A - - Google Patents

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Publication number
IN2014MN01307A
IN2014MN01307A IN1307MUN2014A IN2014MN01307A IN 2014MN01307 A IN2014MN01307 A IN 2014MN01307A IN 1307MUN2014 A IN1307MUN2014 A IN 1307MUN2014A IN 2014MN01307 A IN2014MN01307 A IN 2014MN01307A
Authority
IN
India
Prior art keywords
turpentine
grease
base
dibasic acid
composite
Prior art date
Application number
Inventor
Jianling Xia
Mei Li
Xiaohua Yang
Shouhai Li
Mei Wang
Yan Zhang
Kun Huang
Original Assignee
Inst Chem Ind Forest Prod Caf
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Inst Chem Ind Forest Prod Caf filed Critical Inst Chem Ind Forest Prod Caf
Publication of IN2014MN01307A publication Critical patent/IN2014MN01307A/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
    • C08K5/098—Metal salts of carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
    • C08K5/005—Stabilisers against oxidation, heat, light, ozone

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)
  • Anti-Oxidant Or Stabilizer Compositions (AREA)

Abstract

A method for preparing a grease/turpentine base liquid calcium zinc composite thermal stabilizer for PVC use comprising the steps of: 1) using industrial fatty acid and turpentine as raw materials to synthesize a grease/turpentine base composite dibasic acid through a Diels Alder reaction; 2) uniformly mixing any two metallic compounds of zinc oxide calcium hydroxide and calcium oxide with the grease/turpentine base composite dibasic acid and a solvent respectively heating to 80 150 ? refluxing for 0.5 4 h and distilling to remove the solvent at a vacuum degree of 1 2mmHg so as to obtain the corresponding grease/turpentine base composite dibasic acid salts of the two metals; and 3) dissolving an appropriate amount of the grease/turpentine base composite dibasic acid salts of the two metals in a mixed solution of epoxidized soybean oil an antioxidant liquid paraffin phosphite ester ß diketone and the like and filtering to obtain a grease/turpentine base liquid calcium zinc composite thermal stabilizer. The prepared grease/turpentine base liquid calcium zinc composite thermal stabilizer is used in the field of PVC plastic processing and employs renewable natural grease resources as main raw materials; the product has good thermal stability and essentially no toxicity and is environmentally friendly and highly cost effective.
IN1307MUN2014 2012-09-21 2013-09-17 IN2014MN01307A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN201210356997.5A CN102838819B (en) 2012-09-21 2012-09-21 Preparation method of oil/rosin base liquid calcium-zinc composite stabilizing agent used for PVC (Polyvinyl Chloride)
PCT/CN2013/083599 WO2014044160A1 (en) 2012-09-21 2013-09-17 Method for preparing grease/turpentine base liquid calcium-zinc composite thermal stabilizer for pvc use

Publications (1)

Publication Number Publication Date
IN2014MN01307A true IN2014MN01307A (en) 2015-07-03

Family

ID=47366559

Family Applications (1)

Application Number Title Priority Date Filing Date
IN1307MUN2014 IN2014MN01307A (en) 2012-09-21 2013-09-17

Country Status (4)

Country Link
JP (1) JP5851629B2 (en)
CN (1) CN102838819B (en)
IN (1) IN2014MN01307A (en)
WO (1) WO2014044160A1 (en)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102838819B (en) * 2012-09-21 2014-08-20 中国林业科学研究院林产化学工业研究所 Preparation method of oil/rosin base liquid calcium-zinc composite stabilizing agent used for PVC (Polyvinyl Chloride)
CN105949508B (en) * 2016-05-23 2018-09-04 中国林业科学研究院林产化学工业研究所 A kind of heat stabilizer for PVC and its preparation method and application
CN106800670B (en) * 2016-12-23 2019-05-03 中国林业科学研究院林产化学工业研究所 Tung oil base binary amic acid calcium-zinc composite liquid heat stabilizer and its preparation method and application
CN106751213B (en) * 2016-12-26 2018-11-27 中国林业科学研究院林产化学工业研究所 PVC grease source sodium/zinc composite liquid heat stabilizer and its preparation method and application
CN106893138B (en) * 2017-03-07 2019-03-29 中国林业科学研究院林产化学工业研究所 PVC laurene source composite thermal stabilizer and its preparation method and application
KR102152066B1 (en) * 2019-03-04 2020-09-04 프로켐 주식회사 Hybrid type PVC stabilizer comprising liquid and powder
CN110692632B (en) * 2019-09-04 2022-02-08 深圳诺普信农化股份有限公司 Stabilizing agent for sulfonylurea herbicide and preparation method and application thereof
CN111704774B (en) * 2020-05-26 2022-04-19 广东原基新材料有限公司 Nano-emulsion calcium-zinc stabilizer for PVC (polyvinyl chloride) products and preparation method thereof
CN113970545B (en) * 2021-10-22 2024-03-29 百尔罗赫新材料科技有限公司 Method for detecting performance of heat stabilizer in PVC product processing process

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5599943A (en) * 1979-01-26 1980-07-30 Adeka Argus Chem Co Ltd Vinyl chloride resin composition
US5322872A (en) * 1993-04-14 1994-06-21 The Lubrizol Corporation Stabilized compositions of mixed metal carboxylates
BR9504838A (en) * 1994-11-15 1997-10-07 Lubrizol Corp Polyol ester lubricating oil composition
JP2952258B1 (en) * 1998-09-24 1999-09-20 昭島化学工業株式会社 Heat stabilized vinyl chloride resin composition
JP2000319468A (en) * 1999-05-07 2000-11-21 Asahi Denka Kogyo Kk Stabilizer composition for vinyl chloride-based resin
CN101041728A (en) * 2006-03-23 2007-09-26 汕头市高科达有限公司 Preparation method for (PVC) nontoxic calcium zinc heat stabilizer and uses thereof
CN101486805B (en) * 2008-11-20 2011-08-10 靖江旭光塑胶有限公司 Preparation of calcium zinc composite stabilizer for processing plastic
CN101456977B (en) * 2008-12-16 2010-12-15 浙江传化华洋化工有限公司 Method for preparing Ca-Zn composite heat stabilizer
CN101575422A (en) * 2009-06-18 2009-11-11 浙江嘉澳环保科技股份有限公司 Method for preparing environmental-friendly calcium-zinc composite liquid stabilizing agent
CN101602863B (en) * 2009-06-22 2011-09-14 温州天盛塑料助剂有限公司 Environmental-friendly dust-free calcium-zinc composite heat stabilizer for PVC processing
CN101747529B (en) * 2009-12-16 2011-09-21 杭州三叶新材料股份有限公司 Ca-Zn liquid composite stabilizing agent and application thereof
CN102838819B (en) * 2012-09-21 2014-08-20 中国林业科学研究院林产化学工业研究所 Preparation method of oil/rosin base liquid calcium-zinc composite stabilizing agent used for PVC (Polyvinyl Chloride)

Also Published As

Publication number Publication date
CN102838819A (en) 2012-12-26
CN102838819B (en) 2014-08-20
JP5851629B2 (en) 2016-02-03
JP2015507042A (en) 2015-03-05
WO2014044160A1 (en) 2014-03-27

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