IN2014DN06491A - - Google Patents
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- Publication number
- IN2014DN06491A IN2014DN06491A IN6491DEN2014A IN2014DN06491A IN 2014DN06491 A IN2014DN06491 A IN 2014DN06491A IN 6491DEN2014 A IN6491DEN2014 A IN 6491DEN2014A IN 2014DN06491 A IN2014DN06491 A IN 2014DN06491A
- Authority
- IN
- India
- Prior art keywords
- hmf
- product
- reduced
- sugar solution
- residual sugars
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
- C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
- C07C29/14—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
- C07D307/50—Preparation from natural products
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P13/00—Preparation of nitrogen-containing organic compounds
- C12P13/04—Alpha- or beta- amino acids
- C12P13/08—Lysine; Diaminopimelic acid; Threonine; Valine
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
- C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
- C12P7/06—Ethanol, i.e. non-beverage
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
- C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
- C12P7/18—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic polyhydric
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/40—Preparation of oxygen-containing organic compounds containing a carboxyl group including Peroxycarboxylic acids
- C12P7/56—Lactic acid
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Abstract
Hydroxymethylfurfural is made from an aqueous hexose sugar solution especially from a high fructose corn syrup product. By rapidly heating the sugar solution to the elevated temperatures involved as well as rapidly cooling the resultant product mixture a limited per pass conversion to HMF is obtained; correspondingly however the overall exposure of the HMF that is formed to acidic elevated temperature conditions is also limited so that byproducts are reduced. Separation and recovery of the products is simplified and levels of HMF and other hexose dehydration products known to inhibit ethanol production by fermentation are reduced in the residual sugars product to an extent whereby the residual sugars product is suited to be directly fermented to ethanol or for other uses.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201261584900P | 2012-01-10 | 2012-01-10 | |
PCT/US2012/066708 WO2013106136A1 (en) | 2012-01-10 | 2012-11-28 | Process for making hmf and hmf derivatives from sugars, with recovery of unreacted sugars suitable for direct fermentation to ethanol |
Publications (1)
Publication Number | Publication Date |
---|---|
IN2014DN06491A true IN2014DN06491A (en) | 2015-06-12 |
Family
ID=48781802
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
IN6491DEN2014 IN2014DN06491A (en) | 2012-01-10 | 2012-11-28 |
Country Status (13)
Country | Link |
---|---|
US (1) | US20140315262A1 (en) |
EP (1) | EP2802570A4 (en) |
JP (1) | JP2015504069A (en) |
KR (1) | KR20140117522A (en) |
CN (1) | CN104053649A (en) |
AU (1) | AU2012364787A1 (en) |
BR (1) | BR112014016687A8 (en) |
CA (1) | CA2860834A1 (en) |
EA (1) | EA201491190A1 (en) |
IN (1) | IN2014DN06491A (en) |
MX (1) | MX2014008376A (en) |
SG (1) | SG11201403204TA (en) |
WO (1) | WO2013106136A1 (en) |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP6267240B2 (en) | 2013-03-05 | 2018-01-24 | アーチャー−ダニエルズ−ミッドランド カンパニー | Method for acid dehydration of sugar alcohols |
JP6394221B2 (en) * | 2013-09-20 | 2018-09-26 | 三菱ケミカル株式会社 | Method for producing purified sugar solution, method for producing organic compound, and method for culturing microorganism |
EP3099670A2 (en) | 2014-01-27 | 2016-12-07 | Rennovia Inc. | Conversion of fructose-containing feedstocks to hmf-containing product |
EP3129363B1 (en) * | 2014-04-10 | 2020-01-22 | Archer Daniels Midland Company | Dehydration of a sugar alcohol with mixed combination of acid catalysts |
KR102196777B1 (en) | 2014-08-19 | 2020-12-30 | 아처 다니엘 미드랜드 캄파니 | Catalyst and process for producing 2,5-furandicarboxylic acid from hydromethylfurfural in water |
KR101626808B1 (en) | 2014-10-29 | 2016-06-02 | 군산대학교산학협력단 | Method of purification of sugars in lignocellulose biomass hydrolysates |
US10252961B2 (en) * | 2015-02-03 | 2019-04-09 | Archer Daniels Midland Company | One vessel process for making 1,2-propanediol from a high fructose feedstock |
BR112017017105A2 (en) | 2015-02-10 | 2018-04-03 | Avantium Knowledge Centre Bv | composition, and use of humines. |
US10538499B2 (en) | 2015-04-14 | 2020-01-21 | Dupont Industrial Biosciences Usa, Llc | Processes for producing 2,5-furandicarboxylic acid and derivatives thereof and polymers made therefrom |
EP3337790A4 (en) * | 2015-08-21 | 2019-01-23 | GFBiochemicals Limited | Process to prepare hydroxymethylfurfural derivatives |
CN108779088B (en) | 2016-01-13 | 2021-10-08 | 斯道拉恩索公司 | Process for the preparation of 2,5-furandicarboxylic acid and intermediates and derivatives thereof |
DE102016224073A1 (en) * | 2016-12-02 | 2018-06-07 | Südzucker AG | Improved HMF manufacturing process |
EP3424914A1 (en) * | 2017-07-05 | 2019-01-09 | AVALON Industries AG | Method for the extraction of (5-hydroxymethylfurfural,5-hmf) |
AU2018301662B2 (en) | 2017-07-12 | 2022-06-30 | Stora Enso Oyj | Purified 2,5-furandicarboxylic acid pathway products |
DE102018208510A1 (en) * | 2018-05-29 | 2019-12-05 | Südzucker AG | Salt and acid mixture catalyzed HMF production |
DE102018208507A1 (en) | 2018-05-29 | 2019-12-05 | Südzucker AG | Anolyte fraction-catalyzed HMF production |
EP4263654A1 (en) | 2020-12-18 | 2023-10-25 | Basf Se | Polyester polyols comprising 2,5-bis(hydroxymethyl)tetrahydrofuran |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB600871A (en) * | 1945-10-17 | 1948-04-21 | Walter Norman Haworth | Improvements relating to the manufacture of 5-hydroxymethyl 2-furfural |
US2929823A (en) * | 1956-11-26 | 1960-03-22 | Merck & Co Inc | Production of 5-hydroxymethylfurfural |
CA1174191A (en) * | 1980-03-05 | 1984-09-11 | Peter L. Rogers | Ethanol production |
DE3601281A1 (en) * | 1986-01-17 | 1987-07-23 | Sueddeutsche Zucker Ag | METHOD FOR PRODUCING 5-HYDROXYMETHYLFURFURAL, INCLUDING A CRYSTALINE PRODUCT, WITH THE EXCLUSIVE USE OF WATER AS A SOLVENT |
FR2664273B1 (en) * | 1990-06-27 | 1994-04-29 | Beghin Say Sa | NEW PROCESS FOR THE PREPARATION OF 5-HYDROXYMETHYLFURFURAL FROM SACCHARIDES. |
WO1999067409A1 (en) * | 1998-06-23 | 1999-12-29 | The Regents Of The University Of California | Method of treating biomass material |
EP1834950A1 (en) * | 2006-03-10 | 2007-09-19 | Avantium International B.V. | Method for the synthesis of 5-alkoxymethylfurfural ethers and their use |
EP2050742B1 (en) * | 2006-03-10 | 2010-07-07 | Furanix Technologies B.V | Use of an organic acid esters of 5-hydroxymethylfurfural |
ATE498616T1 (en) * | 2007-09-07 | 2011-03-15 | Furanix Technologies Bv | HYDROXYMETHYLFURFURAL ETHERS AND ESTERS PRODUCED IN IONIC LIQUIDS |
BRPI0819406B1 (en) * | 2007-12-12 | 2021-07-20 | Archer Daniels Midland Co | METHOD FOR OXIDIZING A 2-HYDROXYMETHYL-5-FURALDEHYDE (HMF) ESTER TO 2,5- FURANODICARBOXYLIC ACID (FDCA) |
EP2484437A3 (en) * | 2008-11-17 | 2017-01-18 | Ingelia, S.L. | Process of hydrothermal carbonization of biomass and installation for carrying out said process |
CN101475543A (en) * | 2009-02-11 | 2009-07-08 | 中国科学院山西煤炭化学研究所 | Method for preparing hydroxymethyl-furfural from glucide under low temperature and normal pressure |
FR2945543B1 (en) * | 2009-05-15 | 2011-05-06 | Inst Francais Du Petrole | PROCESS FOR THE PRODUCTION OF ALCOHOLS AND / OR SOLVENTS FROM LIGNOCELLULOSIC BIOMASS WITH ACIDIC RECYCLING OF SOLID RESIDUES |
US20100311137A1 (en) * | 2009-06-08 | 2010-12-09 | Ut-Battelle, Llc | Microorganisms Having Enhanced Tolerance To Inhibitors and Stress |
JP2011078327A (en) * | 2009-10-05 | 2011-04-21 | Gunma Univ | Method for separating fermentation inhibitor from sugar solution |
US9242222B2 (en) * | 2010-04-19 | 2016-01-26 | The University Of Toledo | Aldose-ketose transformation for separation and/or chemical conversion of C6 and C5 sugars from biomass materials |
CN102260229A (en) * | 2010-05-28 | 2011-11-30 | 中国科学院大连化学物理研究所 | Method for preparing 5-hydroxymethylfurfural and 5-alkoxymethylfurfural |
US9090579B2 (en) * | 2012-03-12 | 2015-07-28 | Archer Daniels Midland Co. | Processes for making sugar and/or sugar alcohol dehydration products |
-
2012
- 2012-11-28 US US14/358,363 patent/US20140315262A1/en not_active Abandoned
- 2012-11-28 BR BR112014016687A patent/BR112014016687A8/en not_active Application Discontinuation
- 2012-11-28 CN CN201280066380.8A patent/CN104053649A/en active Pending
- 2012-11-28 JP JP2014551244A patent/JP2015504069A/en active Pending
- 2012-11-28 KR KR1020147022308A patent/KR20140117522A/en not_active Application Discontinuation
- 2012-11-28 MX MX2014008376A patent/MX2014008376A/en unknown
- 2012-11-28 IN IN6491DEN2014 patent/IN2014DN06491A/en unknown
- 2012-11-28 EA EA201491190A patent/EA201491190A1/en unknown
- 2012-11-28 AU AU2012364787A patent/AU2012364787A1/en not_active Abandoned
- 2012-11-28 CA CA2860834A patent/CA2860834A1/en not_active Abandoned
- 2012-11-28 WO PCT/US2012/066708 patent/WO2013106136A1/en active Application Filing
- 2012-11-28 SG SG11201403204TA patent/SG11201403204TA/en unknown
- 2012-11-28 EP EP12864693.2A patent/EP2802570A4/en not_active Withdrawn
Also Published As
Publication number | Publication date |
---|---|
KR20140117522A (en) | 2014-10-07 |
JP2015504069A (en) | 2015-02-05 |
BR112014016687A2 (en) | 2017-06-13 |
BR112014016687A8 (en) | 2017-07-04 |
EA201491190A1 (en) | 2014-12-30 |
MX2014008376A (en) | 2015-04-09 |
SG11201403204TA (en) | 2014-09-26 |
EP2802570A4 (en) | 2016-01-06 |
EP2802570A1 (en) | 2014-11-19 |
AU2012364787A1 (en) | 2014-07-03 |
US20140315262A1 (en) | 2014-10-23 |
CA2860834A1 (en) | 2013-07-18 |
CN104053649A (en) | 2014-09-17 |
WO2013106136A1 (en) | 2013-07-18 |
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