IN2012DN04890A - - Google Patents

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Publication number
IN2012DN04890A
IN2012DN04890A IN4890DEN2012A IN2012DN04890A IN 2012DN04890 A IN2012DN04890 A IN 2012DN04890A IN 4890DEN2012 A IN4890DEN2012 A IN 4890DEN2012A IN 2012DN04890 A IN2012DN04890 A IN 2012DN04890A
Authority
IN
India
Prior art keywords
glycerol
acrolein
dehydration
reaction
manufacture
Prior art date
Application number
Inventor
Devaux Jean-Francois
Fauconet Michel
Tlili Nabil
Haller Philippe
Combat Jean-Paul
Original Assignee
Arkema France
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema France filed Critical Arkema France
Publication of IN2012DN04890A publication Critical patent/IN2012DN04890A/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/52—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition by dehydration and rearrangement involving two hydroxy groups in the same molecule
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/85—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to a chemical modification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00—Compounds having —CHO groups
    • C07C47/20—Unsaturated compounds having —CHO groups bound to acyclic carbon atoms
    • C07C47/21—Unsaturated compounds having —CHO groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C47/22—Acryaldehyde; Methacryaldehyde
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03—Monocarboxylic acids
    • C07C57/04—Acrylic acid; Methacrylic acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02B—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS
    • Y02B30/00—Energy efficient heating, ventilation or air conditioning [HVAC]
    • Y02B30/52—Heat recovery pumps, i.e. heat pump based systems or units able to transfer the thermal energy from one area of the premises or part of the facilities to a different one, improving the overall efficiency
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The present invention relates to the manufacture of bioresourced acrolein and bioresourced acrylic acid from glycerol as starting material and more particularly comes within the scope of a process for the manufacture of acrolein and acrylic acid according to which the reaction for the dehydration of glycerol to give acrolein is carried out and a stage of oxidizing a water-rich phase separated from the reaction mixture coming from this dehydration reaction is carried out, before it is recycled to the glycerol dehydration stage. This oxidation treatment prevents organic impurities from accumulating during the process, while minimizing the consumption of water and the discharge of polluted aqueous streams.
IN4890DEN2012 2009-12-14 2010-12-13 IN2012DN04890A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0958937A FR2953830B1 (en) 2009-12-14 2009-12-14 PROCESS FOR PRODUCING ACROLEIN AND / OR ACRYLIC ACID FROM GLYCEROL
US31423410P 2010-03-16 2010-03-16
PCT/FR2010/052692 WO2011080447A1 (en) 2009-12-14 2010-12-13 Process for manufacturing acrolein and/or acrylic acid from glycerol

Publications (1)

Publication Number Publication Date
IN2012DN04890A true IN2012DN04890A (en) 2015-09-25

Family

ID=42270078

Family Applications (1)

Application Number Title Priority Date Filing Date
IN4890DEN2012 IN2012DN04890A (en) 2009-12-14 2010-12-13

Country Status (12)

Country Link
US (1) US8609904B2 (en)
EP (1) EP2513027B1 (en)
JP (1) JP5784627B2 (en)
KR (1) KR101802543B1 (en)
CN (1) CN102639478B (en)
BR (1) BR112012014147A2 (en)
FR (1) FR2953830B1 (en)
IN (1) IN2012DN04890A (en)
MY (1) MY157406A (en)
SG (1) SG181693A1 (en)
TW (1) TWI468383B (en)
WO (1) WO2011080447A1 (en)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2953829B1 (en) * 2009-12-14 2011-12-09 Arkema France PROCESS FOR PRODUCING ACROLEIN AND / OR ACRYLIC ACID FROM GLYCEROL
JP2013075842A (en) * 2011-09-29 2013-04-25 Nippon Shokubai Co Ltd Production method for acrolein, production method for acrylic acid, and production method for hydrophilic resin
US9422377B2 (en) 2011-09-29 2016-08-23 Nippon Shokubai Co., Ltd. Process for producing acrolein, acrylic acid and derivatives thereof
KR102044428B1 (en) 2015-12-23 2019-12-02 주식회사 엘지화학 Process for preparing acrylic acid from glycerin
CN106622040B (en) * 2017-01-18 2019-10-18 中国科学院过程工程研究所 A kind of system and preparation method thereof that acrylic acid and/or acrylate are prepared using moving-burden bed reactor
CN109304190B (en) * 2017-07-28 2021-06-18 中国石油化工股份有限公司 Catalyst for preparing acrolein from glycerol
CN108409044B (en) * 2018-04-04 2019-04-16 蓝星安迪苏南京有限公司 For handling the method and device of acrolein reaction device waste water
TWI756748B (en) * 2020-07-22 2022-03-01 華懋科技股份有限公司 Energy-saving dual-rotor cold side bypass temperature control system and method thereof
US12031719B2 (en) 2020-07-22 2024-07-09 Desiccant Technology Corporation System and method to prevent the oxidizer overheating using cold side bypass during high input for a VOCS treatment system with series rotor
TWI823017B (en) * 2020-07-22 2023-11-21 華懋科技股份有限公司 Energy-saving dual-runner high-concentration cold-side bypass temperature control system and method thereof
CN114653306B (en) * 2022-03-14 2023-07-21 北京奥科瑞丰新能源股份有限公司 Neutralization reaction kettle with automatic alkali adding mechanism for furfural production

Family Cites Families (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR695931A (en) 1929-06-15 1930-12-23 Schering Kahlbaum Ag Acrolein manufacturing process
US2558520A (en) 1948-01-29 1951-06-26 Us Ind Chemicals Inc Production of acrolein from glycerol
US3433840A (en) 1966-12-29 1969-03-18 Sumitomo Chemical Co Process for recovering acrolein by quenching,absorption and plural distillation
BE786398A (en) 1971-07-21 1973-01-18 Basf Ag PROCESS FOR PREPARING ANHYDROUS ACRYLIC ACID
DE4238493C1 (en) 1992-11-14 1994-04-21 Degussa Process for the production of acrolein and its use
DE4308087C2 (en) 1993-03-13 1997-02-06 Basf Ag Process for the separation of acrylic acid from the reaction gases of the catalytic oxidation of propylene and / or acrolein
JPH07133249A (en) * 1993-09-17 1995-05-23 Daicel Chem Ind Ltd Production of high-purity acetic acid
GB9400081D0 (en) * 1994-01-05 1994-03-02 Dow Deutschland Inc Process for producing chlorohydrins
DE19624674A1 (en) * 1996-06-20 1998-01-02 Basf Ag Process for the disposal of secondary components resulting from the production of acrylic acid or methacrylic acid
TW476746B (en) 1997-07-23 2002-02-21 Shell Int Research Hydrogenolysis of glycerol
FR2775685B1 (en) * 1998-03-05 2000-12-29 Rhone Poulenc Fibres PROCESS FOR SEPARATION AND PURIFICATION OF ADIPIC ACID
DE19848208A1 (en) 1998-10-20 2000-04-27 Deg Engineering Gmbh Reactor for the catalytic conversion of reaction media, especially gaseous reaction media
US6303826B1 (en) * 2000-01-19 2001-10-16 Sunoco, Inc. (R&M) Method for purification of acetone
DE10019381B4 (en) 2000-04-19 2006-05-18 Daun, Klaus-Dieter, Dipl.-Ing. Reactor for the catalytic conversion of reaction media, in particular gaseous reaction media
US6515187B1 (en) 2001-10-03 2003-02-04 Atofina Chemicals, Inc. Process for recovering acrolein or propionaldehyde from dilute aqueous streams
FR2835831B1 (en) 2002-02-12 2006-09-01 Aventis Animal Nutrition Sa PROCESS FOR PURIFYING ACROLEIN
US6667418B2 (en) * 2002-04-16 2003-12-23 Celanese International Corporation Oxidation treatment of a recycle stream in production of acetic acid by methanol carbonylation
US7268254B2 (en) 2003-07-24 2007-09-11 Basf Aktiengesellschaft Preparation of (meth)acrolein and/or (meth)acrylic acid by heterogeneously catalyzed partial oxidation of C3 and/or C4 precursor compounds in a reactor having thermoplate modules
JP5006507B2 (en) 2004-01-30 2012-08-22 株式会社日本触媒 Acrylic acid production method
US7414149B2 (en) * 2004-11-22 2008-08-19 Rohm And Haas Company Non-routine reactor shutdown method
FR2882052B1 (en) 2005-02-15 2007-03-23 Arkema Sa PROCESS FOR THE DEHYDRATION OF GLYCEROL IN ACROLEIN
FR2882053B1 (en) 2005-02-15 2007-03-23 Arkema Sa METHOD FOR DEHYDRATING GLYCEROL IN ACROLENE
TWI529181B (en) 2005-02-28 2016-04-11 贏創德固賽有限責任公司 Water-absorbing polymer structures based upon renewable raw materials and process for their production
TWI522092B (en) * 2005-02-28 2016-02-21 贏創德固賽有限責任公司 Acrylic acid and water-absorbing polymer structures based upon renewable raw materials and process for their preparation
FR2884818B1 (en) 2005-04-25 2007-07-13 Arkema Sa PROCESS FOR THE PREPARATION OF ACRYLIC ACID FROM GLYCEROL
US20090068440A1 (en) 2005-06-20 2009-03-12 Gunther Bub Production of acrolein, acrylic acid and water-absorbent polymer structures made from glycerine
EP1847522A1 (en) * 2006-04-18 2007-10-24 INEOS Phenol GmbH & Co. KG Process for removal of hydroxyacetone from phenol
US7495505B2 (en) 2006-07-18 2009-02-24 Faraday Technology Corp. Low supply voltage band-gap reference circuit and negative temperature coefficient current generation unit thereof and method for supplying band-gap reference current
FR2909999B1 (en) * 2006-12-19 2009-04-03 Arkema France PROCESS FOR THE PREPARATION OF ACRYLIC ACID FROM GLYCEROL
EP1978009A1 (en) 2007-04-04 2008-10-08 Rohm and Haas Company Method for purification of glycerol
FR2921361B1 (en) 2007-09-20 2012-10-12 Arkema France PROCESS FOR PRODUCING ACROLEIN FROM GLYCEROL
FR2928648B1 (en) 2008-03-12 2012-03-02 Arkema France COMPRESSION SYSTEM

Also Published As

Publication number Publication date
JP2013513593A (en) 2013-04-22
KR101802543B1 (en) 2017-11-28
FR2953830B1 (en) 2012-01-20
CN102639478B (en) 2015-04-01
BR112012014147A2 (en) 2017-01-24
JP5784627B2 (en) 2015-09-24
TWI468383B (en) 2015-01-11
MY157406A (en) 2016-06-15
US20120302797A1 (en) 2012-11-29
TW201136887A (en) 2011-11-01
EP2513027B1 (en) 2014-08-13
WO2011080447A1 (en) 2011-07-07
CN102639478A (en) 2012-08-15
KR20120105029A (en) 2012-09-24
SG181693A1 (en) 2012-07-30
US8609904B2 (en) 2013-12-17
FR2953830A1 (en) 2011-06-17
EP2513027A1 (en) 2012-10-24

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