IN2012DN01790A - - Google Patents

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Publication number
IN2012DN01790A
IN2012DN01790A IN1790DEN2012A IN2012DN01790A IN 2012DN01790 A IN2012DN01790 A IN 2012DN01790A IN 1790DEN2012 A IN1790DEN2012 A IN 1790DEN2012A IN 2012DN01790 A IN2012DN01790 A IN 2012DN01790A
Authority
IN
India
Prior art keywords
silica
titanium
amount
product
fluidized bed
Prior art date
Application number
Inventor
Jr James Elliott Merkle
Jr Raymond Roy Beets
Original Assignee
Du Pont
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Du Pont filed Critical Du Pont
Publication of IN2012DN01790A publication Critical patent/IN2012DN01790A/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1218Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes
    • C22B34/1231Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes treatment or purification of titanium containing products obtained by dry processes, e.g. condensation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1809Controlling processes
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00Compounds of titanium
    • C01G23/02Halides of titanium
    • C01G23/022Titanium tetrachloride
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00Compounds of titanium
    • C01G23/04Oxides; Hydroxides
    • C01G23/047Titanium dioxide
    • C01G23/07Producing by vapour phase processes, e.g. halide oxidation
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1218Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes
    • C22B34/1222Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes using a halogen containing agent
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/50Solid solutions
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00Chemistry: analytical and immunological testing
    • Y10T436/12Condition responsive control

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Silicon Compounds (AREA)

Abstract

This disclosure relates to a process for controlling chlorination reactions in manufacturing titanium tetrachloride in a fluidized bed reactor, followed by processing to form a titanium product comprising an amount of silica, the process comprising: (a) feeding carbonaceous material, titanium bearing material comprising an amount of silica, and chlorine to the fluidized bed reactor to form a gaseous stream, and condensing the gaseous stream to form titanium tetrachloride, a non-condensed gas stream and a condensable product stream; (b) processing the titanium tetrachloride to form a titanium product comprising an amount of silica; (c) analyzing the titanium product comprising an amount of silica to determine the analyzed concentration of silica; (d) identifying a set point concentration of silica; (e) calculating the difference between the analyzed concentration of silica and the set point concentration of silica; and (f) generating a signal which corresponds to the difference calculated in step (e) which provides a feedback response that controls the flow of the titanium bearing material into the fluidized bed reactor.
IN1790DEN2012 2009-09-03 2010-09-02 IN2012DN01790A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US23956509P 2009-09-03 2009-09-03
PCT/US2010/047660 WO2011028892A1 (en) 2009-09-03 2010-09-02 Titanium bearing material flow control in the manufacture of titanium tetrachloride with silica content monitoring of the titanium product

Publications (1)

Publication Number Publication Date
IN2012DN01790A true IN2012DN01790A (en) 2015-06-05

Family

ID=42800011

Family Applications (1)

Application Number Title Priority Date Filing Date
IN1790DEN2012 IN2012DN01790A (en) 2009-09-03 2010-09-02

Country Status (6)

Country Link
US (1) US8748184B2 (en)
EP (1) EP2473642B1 (en)
CN (1) CN102762753B (en)
AU (1) AU2010289435B2 (en)
IN (1) IN2012DN01790A (en)
WO (1) WO2011028892A1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103979604B (en) * 2014-05-29 2017-01-04 重庆大学 The inner circulation fluidized device and method preparing titanium tetrachloride of a kind of vibration type

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2446181A (en) 1946-04-03 1948-08-03 Du Pont Process for condensing vaporized metal halides
US2701179A (en) 1951-02-24 1955-02-01 Du Pont Metal halide production
US3883636A (en) 1967-11-17 1975-05-13 British Titan Ltd Chlorination process
US3591333A (en) 1970-04-30 1971-07-06 Ppg Industries Inc Method of chlorinating titanium-bearing materials
CA1323977C (en) * 1987-03-25 1993-11-09 Guillermo F. Garrido Nitrogen-free process for chloride-route tio_pigment manufacture
CH692654A5 (en) * 1993-07-29 2002-09-13 Buehler Ag Apparatus and method for varying the spatial distribution of a powdery solid.
DE4442783A1 (en) * 1994-12-01 1996-06-05 Kronos Titan Gmbh Process for increasing the yield in the chlorination of titanium-containing raw materials
US5670121A (en) 1995-05-05 1997-09-23 E. I. Du Pont De Nemours And Company Process for controlling the temperature of a fluidized bed reactor in the manufacture of titanium tetrachloride
US6562314B2 (en) 2001-02-20 2003-05-13 Millennium Inorganic Chemicals, Inc. Methods of producing substantially anatase-free titanium dioxide with silicon halide addition
JP2004210586A (en) 2002-12-27 2004-07-29 Showa Denko Kk Method for production of high bulk density titania-silica mixed crystal particle, titania-silica mixed crystal particle obtained by the method, and use thereof
EP1717203A1 (en) 2005-04-26 2006-11-02 Kerr-McGee Corporation Production of titanium tetrachloride using a fluidized bed reactor
DE102006050336A1 (en) 2006-10-25 2008-05-08 Wacker Polymer Systems Gmbh & Co. Kg Gemini surfactant-containing dispersion powder compositions

Also Published As

Publication number Publication date
AU2010289435A1 (en) 2012-03-15
EP2473642A1 (en) 2012-07-11
US8748184B2 (en) 2014-06-10
AU2010289435B2 (en) 2016-05-12
WO2011028892A1 (en) 2011-03-10
CN102762753B (en) 2014-03-05
EP2473642B1 (en) 2016-04-27
CN102762753A (en) 2012-10-31
US20120156790A1 (en) 2012-06-21

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