IN2012DN01790A - - Google Patents
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- Publication number
- IN2012DN01790A IN2012DN01790A IN1790DEN2012A IN2012DN01790A IN 2012DN01790 A IN2012DN01790 A IN 2012DN01790A IN 1790DEN2012 A IN1790DEN2012 A IN 1790DEN2012A IN 2012DN01790 A IN2012DN01790 A IN 2012DN01790A
- Authority
- IN
- India
- Prior art keywords
- silica
- titanium
- amount
- product
- fluidized bed
- Prior art date
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 16
- 239000000377 silicon dioxide Substances 0.000 abstract 8
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 5
- 229910052719 titanium Inorganic materials 0.000 abstract 5
- 239000010936 titanium Substances 0.000 abstract 5
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 abstract 3
- 239000000463 material Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- 239000003575 carbonaceous material Substances 0.000 abstract 1
- 238000005660 chlorination reaction Methods 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1218—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes
- C22B34/1231—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes treatment or purification of titanium containing products obtained by dry processes, e.g. condensation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/1809—Controlling processes
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/02—Halides of titanium
- C01G23/022—Titanium tetrachloride
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/07—Producing by vapour phase processes, e.g. halide oxidation
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1218—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes
- C22B34/1222—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes using a halogen containing agent
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/50—Solid solutions
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/12—Condition responsive control
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Inorganic Chemistry (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Combustion & Propulsion (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Silicon Compounds (AREA)
Abstract
This disclosure relates to a process for controlling chlorination reactions in manufacturing titanium tetrachloride in a fluidized bed reactor, followed by processing to form a titanium product comprising an amount of silica, the process comprising: (a) feeding carbonaceous material, titanium bearing material comprising an amount of silica, and chlorine to the fluidized bed reactor to form a gaseous stream, and condensing the gaseous stream to form titanium tetrachloride, a non-condensed gas stream and a condensable product stream; (b) processing the titanium tetrachloride to form a titanium product comprising an amount of silica; (c) analyzing the titanium product comprising an amount of silica to determine the analyzed concentration of silica; (d) identifying a set point concentration of silica; (e) calculating the difference between the analyzed concentration of silica and the set point concentration of silica; and (f) generating a signal which corresponds to the difference calculated in step (e) which provides a feedback response that controls the flow of the titanium bearing material into the fluidized bed reactor.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US23956509P | 2009-09-03 | 2009-09-03 | |
| PCT/US2010/047660 WO2011028892A1 (en) | 2009-09-03 | 2010-09-02 | Titanium bearing material flow control in the manufacture of titanium tetrachloride with silica content monitoring of the titanium product |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IN2012DN01790A true IN2012DN01790A (en) | 2015-06-05 |
Family
ID=42800011
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IN1790DEN2012 IN2012DN01790A (en) | 2009-09-03 | 2010-09-02 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US8748184B2 (en) |
| EP (1) | EP2473642B1 (en) |
| CN (1) | CN102762753B (en) |
| AU (1) | AU2010289435B2 (en) |
| IN (1) | IN2012DN01790A (en) |
| WO (1) | WO2011028892A1 (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103979604B (en) * | 2014-05-29 | 2017-01-04 | 重庆大学 | The inner circulation fluidized device and method preparing titanium tetrachloride of a kind of vibration type |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2446181A (en) | 1946-04-03 | 1948-08-03 | Du Pont | Process for condensing vaporized metal halides |
| US2701179A (en) | 1951-02-24 | 1955-02-01 | Du Pont | Metal halide production |
| US3883636A (en) | 1967-11-17 | 1975-05-13 | British Titan Ltd | Chlorination process |
| US3591333A (en) | 1970-04-30 | 1971-07-06 | Ppg Industries Inc | Method of chlorinating titanium-bearing materials |
| CA1323977C (en) * | 1987-03-25 | 1993-11-09 | Guillermo F. Garrido | Nitrogen-free process for chloride-route tio_pigment manufacture |
| CH692654A5 (en) * | 1993-07-29 | 2002-09-13 | Buehler Ag | Apparatus and method for varying the spatial distribution of a powdery solid. |
| DE4442783A1 (en) * | 1994-12-01 | 1996-06-05 | Kronos Titan Gmbh | Process for increasing the yield in the chlorination of titanium-containing raw materials |
| US5670121A (en) | 1995-05-05 | 1997-09-23 | E. I. Du Pont De Nemours And Company | Process for controlling the temperature of a fluidized bed reactor in the manufacture of titanium tetrachloride |
| US6562314B2 (en) | 2001-02-20 | 2003-05-13 | Millennium Inorganic Chemicals, Inc. | Methods of producing substantially anatase-free titanium dioxide with silicon halide addition |
| JP2004210586A (en) | 2002-12-27 | 2004-07-29 | Showa Denko Kk | Method for production of high bulk density titania-silica mixed crystal particle, titania-silica mixed crystal particle obtained by the method, and use thereof |
| EP1717203A1 (en) | 2005-04-26 | 2006-11-02 | Kerr-McGee Corporation | Production of titanium tetrachloride using a fluidized bed reactor |
| DE102006050336A1 (en) | 2006-10-25 | 2008-05-08 | Wacker Polymer Systems Gmbh & Co. Kg | Gemini surfactant-containing dispersion powder compositions |
-
2010
- 2010-09-02 CN CN201080049688.2A patent/CN102762753B/en active Active
- 2010-09-02 US US13/392,607 patent/US8748184B2/en active Active
- 2010-09-02 WO PCT/US2010/047660 patent/WO2011028892A1/en not_active Ceased
- 2010-09-02 AU AU2010289435A patent/AU2010289435B2/en active Active
- 2010-09-02 EP EP10752970.3A patent/EP2473642B1/en active Active
- 2010-09-02 IN IN1790DEN2012 patent/IN2012DN01790A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CN102762753A (en) | 2012-10-31 |
| AU2010289435B2 (en) | 2016-05-12 |
| AU2010289435A1 (en) | 2012-03-15 |
| CN102762753B (en) | 2014-03-05 |
| US8748184B2 (en) | 2014-06-10 |
| EP2473642B1 (en) | 2016-04-27 |
| WO2011028892A1 (en) | 2011-03-10 |
| EP2473642A1 (en) | 2012-07-11 |
| US20120156790A1 (en) | 2012-06-21 |
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