IN2012DN00705A - - Google Patents

Download PDF

Info

Publication number
IN2012DN00705A
IN2012DN00705A IN705DEN2012A IN2012DN00705A IN 2012DN00705 A IN2012DN00705 A IN 2012DN00705A IN 705DEN2012 A IN705DEN2012 A IN 705DEN2012A IN 2012DN00705 A IN2012DN00705 A IN 2012DN00705A
Authority
IN
India
Prior art keywords
continuous
monochloropropanediols
glycerine
dichloro
propanol
Prior art date
Application number
Inventor
Pavel Kubicek
Petr Sladek
Ivana Buricova
Original Assignee
Spolek
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=34256927&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=IN2012DN00705(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Spolek filed Critical Spolek
Publication of IN2012DN00705A publication Critical patent/IN2012DN00705A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/62—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by introduction of halogen; by substitution of halogen atoms by other halogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/34—Halogenated alcohols
    • C07C31/36—Halogenated alcohols the halogen not being fluorine

Abstract

A method of highly selective catalytic hydrochlorination of glycerine and/or monochloropropanediols to the dichloropropanol products 1,3-dichloro-2-propanol and 2,3-dichloro-l-propanol, carried out in at least one continuous reaction zone at reaction temperatures in the range of 70-140 °C and with continuous removing of the water of reaction, the liquid feed containing at least 50 % by weight of glycerine and/or monochloropropanediols. The method can be carried out in a continuously operating one-step circulation reactor or a cascade of continuous flow reactors of the liquid-gas type.
IN705DEN2012 2003-09-01 2004-08-23 IN2012DN00705A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CZ20032346A CZ294890B6 (en) 2003-09-01 2003-09-01 Process for preparing dichloropropanols from glycerin
PCT/CZ2004/000049 WO2005021476A1 (en) 2003-09-01 2004-08-23 Method of preparing dichloropropanols from glycerine

Publications (1)

Publication Number Publication Date
IN2012DN00705A true IN2012DN00705A (en) 2015-06-19

Family

ID=34256927

Family Applications (1)

Application Number Title Priority Date Filing Date
IN705DEN2012 IN2012DN00705A (en) 2003-09-01 2004-08-23

Country Status (22)

Country Link
US (2) US7473809B2 (en)
EP (1) EP1663924B1 (en)
JP (3) JP5752342B2 (en)
KR (1) KR101062792B1 (en)
CN (1) CN100439305C (en)
AT (1) ATE530513T1 (en)
BR (1) BRPI0413914B1 (en)
CA (1) CA2537131C (en)
CY (1) CY1112165T1 (en)
CZ (1) CZ294890B6 (en)
DK (1) DK1663924T3 (en)
ES (1) ES2373040T3 (en)
HK (1) HK1096081A1 (en)
IN (1) IN2012DN00705A (en)
MX (1) MXPA06002351A (en)
PL (1) PL1663924T3 (en)
PT (1) PT1663924E (en)
RU (1) RU2356878C2 (en)
SI (1) SI1663924T1 (en)
TW (1) TWI325417B (en)
UA (1) UA81971C2 (en)
WO (1) WO2005021476A1 (en)

Families Citing this family (68)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CZ294890B6 (en) 2003-09-01 2005-04-13 Spolek Pro Chemickou A Hutní Výrobu,A.S. Process for preparing dichloropropanols from glycerin
CN100999442B (en) 2003-11-20 2012-04-11 索尔维公司 Pseudo-azeotropic composition containing dichloropropanol and process for producing same
KR101009858B1 (en) 2003-11-20 2011-01-19 솔베이(소시에떼아노님) Process for producing an organic compound
US7910781B2 (en) 2004-07-21 2011-03-22 Dow Global Technologies Llc Process for the conversion of a crude glycerol, crude mixtures of naturally derived multihydroxylated aliphatic hydrocarbons or esters thereof to a chlorohydrin
EP1771403B1 (en) 2004-07-21 2010-01-06 Dow Global Technologies Inc. Conversion of a multihydroxylated-aliphatic hydrocarbon or ester thereof to a chlorohydrin
US7906690B2 (en) 2004-07-21 2011-03-15 Dow Global Technologies Inc. Batch, semi-continuous or continuous hydrochlorination of glycerin with reduced volatile chlorinated hydrocarbon by-products and chloracetone levels
KR20080036555A (en) * 2005-05-20 2008-04-28 솔베이(소시에떼아노님) Method for making an epoxy starting from a chlorhydrine
TWI321129B (en) * 2005-05-20 2010-03-01 Solvay Process for preparing a chlorohydrin
EP1948583A2 (en) * 2005-11-08 2008-07-30 Solvay S.A. Process for the manufacture of dichloropropanol by chlorination of glycerol
EA200970011A1 (en) 2006-06-14 2009-06-30 Солвей (Сосьете Аноним) UNCLEANED PRODUCT ON THE BASIS OF GLYCERINE, THE METHOD OF ITS CLEANING AND ITS APPLICATION IN THE MANUFACTURE OF DICHLORPROPANOL
US7930651B2 (en) 2007-01-18 2011-04-19 Research In Motion Limited Agenda display in an electronic device
FR2913421B1 (en) 2007-03-07 2009-05-15 Solvay PROCESS FOR PRODUCING DICHLOROPROPANOL
FR2913684B1 (en) * 2007-03-14 2012-09-14 Solvay PROCESS FOR PRODUCING DICHLOROPROPANOL
TWI432407B (en) 2007-04-12 2014-04-01 Dow Global Technologies Llc Multi-stage process and apparatus for recovering dichlorohydrins
KR20100016453A (en) * 2007-04-12 2010-02-12 다우 글로벌 테크놀로지스 인크. Process and apparatus for reducing heavy byproduct formation during recovery of dichlorohydrins
WO2008128014A1 (en) * 2007-04-12 2008-10-23 Dow Global Technologies Inc. Process and apparatus for vapor phase purification during hydrochlorination of multi-hydroxylated aliphatic hydrocarbon compounds
JP2010523703A (en) 2007-04-12 2010-07-15 ダウ グローバル テクノロジーズ インコーポレイティド Method and apparatus for azeotropic recovery of dichlorohydrin
CN101657404B (en) 2007-04-12 2013-11-06 陶氏环球技术公司 Process and apparatus for recovery of dichlorohydrins via codistillation
TWI529155B (en) * 2007-04-12 2016-04-11 陶氏全球科技公司 Process and apparatus for producing chlorohydrin
TW200911740A (en) * 2007-06-01 2009-03-16 Solvay Process for manufacturing a chlorohydrin
TW200911773A (en) 2007-06-12 2009-03-16 Solvay Epichlorohydrin, manufacturing process and use
TW200911693A (en) 2007-06-12 2009-03-16 Solvay Aqueous composition containing a salt, manufacturing process and use
FR2918058A1 (en) * 2007-06-28 2009-01-02 Solvay GLYCEROL-BASED PRODUCT, PROCESS FOR ITS PURIFICATION AND USE IN THE MANUFACTURE OF DICHLOROPROPANOL
JP2010241689A (en) * 2007-08-17 2010-10-28 Kashima Chemical Kk Method for producing chlorohydrin
CN101397238B (en) * 2007-09-24 2011-08-17 如皋市双马化工有限公司 Method for producing dichloropropanol
WO2009041175A1 (en) * 2007-09-28 2009-04-02 Daiso Co., Ltd. Process for producing chlorohydrin
WO2009066327A1 (en) * 2007-11-19 2009-05-28 Conser S.P.A. Conversion of glycerine to dichlorohydrins and epichlorohydrin
KR100881344B1 (en) * 2007-12-12 2009-02-02 삼성정밀화학 주식회사 Method of preparing dichloropropanol from glycerol using heteropolyacid catalysts
FR2925045B1 (en) 2007-12-17 2012-02-24 Solvay GLYCEROL-BASED PRODUCT, PROCESS FOR OBTAINING THE SAME AND USE THEREOF IN THE MANUFACTURE OF DICHLOROPROPANOL
TWI478875B (en) 2008-01-31 2015-04-01 Solvay Process for degrading organic substances in an aqueous composition
DE102008007622A1 (en) 2008-02-04 2009-08-06 Biopetrol Industries Ag Process for the preparation of epichlorohydrin from glycerol
WO2009104961A2 (en) * 2008-02-21 2009-08-27 Bouwe De Jong Process for the preparation of a dichloropropanol product
PL2257537T3 (en) 2008-02-26 2013-03-29 Dow Global Technologies Llc Process for purifying epichlorohydrins
AR072446A1 (en) 2008-03-02 2010-09-01 Dow Global Technologies Inc IMPROVED HYDROGENATION PROCESS
EA201071157A1 (en) 2008-04-03 2011-04-29 Солвей (Сосьете Аноним) COMPOSITION CONTAINING GLYCERIN, METHOD OF ITS RECEPTION AND APPLICATION IN PRODUCTION OF DICHLORPROPANOL
CN101998945B (en) * 2008-04-09 2014-04-09 陶氏环球技术公司 Process and apparatus for efficient recovery of dichlorohydrins
KR20100126603A (en) 2008-04-09 2010-12-01 다우 글로벌 테크놀로지스 인크. Multi-stage process and apparatus for recovering dichlorohydrins
CN101570471B (en) * 2008-04-29 2012-08-29 中国石油化工股份有限公司 Method for synthesizing dichloropropanol by glycerine
CN101570470B (en) * 2008-04-29 2012-08-29 中国石油化工股份有限公司 Method for preparing dichloropropanol by glycerin chlorination
AT507260B1 (en) * 2008-08-25 2010-10-15 Kanzler Walter PROCESS FOR THE PRODUCTION OF EPICHLORHYDRIN FROM GLYCERIN
ITMI20081535A1 (en) * 2008-08-26 2010-02-26 Biocompany Srl PROCESS FOR THE PREPARATION OF 1,3-DICHLORO-2-PROPANOL
FR2935968B1 (en) 2008-09-12 2010-09-10 Solvay PROCESS FOR THE PURIFICATION OF HYDROGEN CHLORIDE
CN101429099B (en) * 2008-11-25 2011-12-07 烟台万华聚氨酯股份有限公司 Method for producing dichlorohydrin with glycerol
KR101067494B1 (en) * 2008-12-31 2011-09-27 삼성정밀화학 주식회사 Method of preparing dichloropropanol using glycerol with improved selectivity of dichloropropanol
CN101774886B (en) * 2009-01-13 2013-10-16 德纳（南京）化工有限公司 Method for preparing dichlorohydrin and reaction device
BRPI0901399A2 (en) * 2009-03-11 2010-11-16 Ima Quimica S A process for obtaining dichloropropanols
WO2011092270A2 (en) 2010-02-01 2011-08-04 Akzo Nobel Chemicals International B.V. Process for preparing epichlorohydrin from dichlorohydrin
KR101705206B1 (en) * 2010-06-30 2017-02-09 롯데정밀화학 주식회사 Method of preparing chlorohydrins and method of preparing epichlorohydrin using chlorohydrins prepared by the same
KR101705205B1 (en) * 2010-06-30 2017-02-09 롯데정밀화학 주식회사 Method of preparing chlorohydrins and method of preparing epichlorohydrin using chlorohydrins prepared by the same
KR101705208B1 (en) * 2010-06-30 2017-02-09 롯데정밀화학 주식회사 Method of preparing composition of chlorohydrins and method of preparing epichlorohydrin using composition of chlorohydrins prepared by the same
KR101705209B1 (en) * 2010-06-30 2017-02-09 롯데정밀화학 주식회사 Method of preparing composition of chlorohydrins and method of preparing epichlorohydrin using composition of chlorohydrins prepared by the same
KR101705210B1 (en) * 2010-06-30 2017-02-09 롯데정밀화학 주식회사 Method of preparing composition of chlorohydrins and method of preparing epichlorohydrin using composition of chlorohydrins prepared by the same
KR101705207B1 (en) * 2010-06-30 2017-02-09 롯데정밀화학 주식회사 Method of preparing chlorohydrins and method of preparing epichlorohydrin using chlorohydrins prepared by the same
JP6182067B2 (en) 2010-09-03 2017-08-16 ステパン スペシャルティー プロダクツ、エルエルシー Removal of organic halo and oxirane species in carboxylic acid ester streams.
CN101979365B (en) * 2010-09-20 2013-11-06 华东理工大学 Method for continuously preparing dichlorohydrin
KR20140009163A (en) 2010-09-30 2014-01-22 솔베이(소시에떼아노님) Derivative of epichlorohydrin of natural origin
CN102010295B (en) * 2010-11-12 2013-05-01 珠海长先化学科技有限公司 Method for preparing dichloropropanol by glycerol method
PL215730B1 (en) 2011-01-10 2014-01-31 Inst Ciezkiej Syntezy Orga Process for the preparation of dichloropropanols from glycerine
PL218074B1 (en) 2011-04-11 2014-10-31 Inst Ciężkiej Syntezy Organicznej Blachownia Process for dry chloro-hydrogenation of the mass left after chloro-hydrogenation of glycerol with hydrochloric acid and a device for dry chloro-hydrogenation of the mass left after chloro-hydrogenation of glycerol with hydrochloric acid
CN102295529B (en) * 2011-07-11 2015-09-09 江西省化学工业研究所 A kind of method of glycerine and hydrochloric acid continuous production dichlorohydrine
PL2763944T3 (en) 2011-09-09 2016-05-31 Akzo Nobel Chemicals Int Bv Process for the chlorination of a hydroxylated organic compound
CZ306363B6 (en) 2013-06-10 2016-12-21 Spolek Pro Chemickou A Hutní Výrobu, Akciová Společnost Process for preparing epoxy-monomers and epoxides
CN103570498B (en) * 2013-08-06 2016-06-22 江苏大学 A kind of glycerin chlorination prepares the method for dichlorohydrin
CN104557442B (en) * 2013-10-18 2017-10-13 江苏扬农化工集团有限公司 The method of comprehensive utilization of carbon trichloride
CN104370857A (en) * 2014-11-11 2015-02-25 常州大学 Synthesis method of epoxy chloropropane
US11672258B2 (en) 2015-08-25 2023-06-13 Dsm Ip Assets B.V. Refined oil compositions and methods for making
TWI547470B (en) 2015-12-18 2016-09-01 長春人造樹脂廠股份有限公司 Process for Preparing Dichloropropanol
CN111018665A (en) * 2019-12-17 2020-04-17 山东民基化工有限公司 Method for recycling trichloropropane in epichlorohydrin heavy component

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE197308C (en) *
DE1075103B (en) 1960-02-11 VEB Leuna-Werke "Walter Ulbricht", Leuna (Kr. Merseburg) Process for the continuous production of epichlorohydrin from glycerine
US2198600A (en) 1936-09-10 1940-04-30 Dow Chemical Co Glycerol dichlorohydrin
US2144612A (en) * 1936-09-10 1939-01-24 Dow Chemical Co Preparation of glycerol dichlorohydrin
JPH0643353B2 (en) 1989-07-25 1994-06-08 ダイソー株式会社 Continuous production method of 2,3-dichloro-1-propanol and its apparatus
JP3846926B2 (en) * 1995-12-27 2006-11-15 日本ジーイープラスチックス株式会社 Process for continuous production of aromatic carbonates
DE19604253A1 (en) * 1996-02-06 1997-08-07 Basf Ag Process for the continuous production of alkyl esters of (meth) acrylic acid
JP2002020333A (en) * 2000-07-06 2002-01-23 Toagosei Co Ltd Method for substituting hydroxyl group by chlorine
DE10063175A1 (en) 2000-12-18 2002-06-20 Basf Ag Process for the preparation of higher (meth) acrylic acid esters
JP4721311B2 (en) * 2001-04-26 2011-07-13 昭和電工株式会社 Process for producing 2,3-dichloro-1-propanol and epichlorohydrin
CZ294890B6 (en) * 2003-09-01 2005-04-13 Spolek Pro Chemickou A Hutní Výrobu,A.S. Process for preparing dichloropropanols from glycerin

Also Published As

Publication number Publication date
JP2007504101A (en) 2007-03-01
JP5752342B2 (en) 2015-07-22
DK1663924T3 (en) 2012-01-30
CZ20032346A3 (en) 2005-04-13
US20090082601A1 (en) 2009-03-26
RU2006110099A (en) 2007-10-10
PT1663924E (en) 2011-12-27
ATE530513T1 (en) 2011-11-15
CN100439305C (en) 2008-12-03
JP5554816B2 (en) 2014-07-23
CZ294890B6 (en) 2005-04-13
ES2373040T3 (en) 2012-01-30
KR20070015902A (en) 2007-02-06
TW200510284A (en) 2005-03-16
CN1845888A (en) 2006-10-11
EP1663924A1 (en) 2006-06-07
PL1663924T3 (en) 2012-03-30
WO2005021476A1 (en) 2005-03-10
CA2537131A1 (en) 2005-03-10
RU2356878C2 (en) 2009-05-27
TWI325417B (en) 2010-06-01
US7473809B2 (en) 2009-01-06
SI1663924T1 (en) 2012-02-29
CY1112165T1 (en) 2015-12-09
HK1096081A1 (en) 2007-05-25
JP2013006876A (en) 2013-01-10
MXPA06002351A (en) 2006-08-31
EP1663924B1 (en) 2011-10-26
CA2537131C (en) 2011-01-18
JP2013006875A (en) 2013-01-10
US20070167659A1 (en) 2007-07-19
BRPI0413914B1 (en) 2014-12-09
KR101062792B1 (en) 2011-09-06
JP5554815B2 (en) 2014-07-23
UA81971C2 (en) 2008-02-25
BRPI0413914A (en) 2006-10-24

Similar Documents

Publication Publication Date Title
IN2012DN00705A (en)
FI20185652A1 (en) Purification of recycled and renewable organic material
MY177306A (en) Process for producing dichloropropanol
UA88906C2 (en) Method and device for producing 1,2-dichlorethane
PL1752435T3 (en) Process for producing epichlorhydrin
BRPI0519200A2 (en) process for the production of 1,2 dichloroethane using direct chlorination
BRPI0519856A2 (en) food purification at room temperature
BRPI0408669A (en) continuous process and system for producing polyether polyols
WO2007134415A3 (en) Process for production of ethylene from ethyl alcohol
TW200714639A (en) Process and equipment for the decomposition and recovery of isocyanate compounds
ES8301841A1 (en) Process for the removal of urea, ammonia and carbon dioxide from dilute aqueous solutions.
MY114496A (en) Process for the production of n-propanol
BRPI0510183A (en) method for the stable production of an aromatic polycarbonate
DE60106091D1 (en) PRODUCTION OF POTASSIUM FORMAT
IN2012DN00704A (en)
DE3660803D1 (en) Process for the production of cyclohexyl compounds
MY160853A (en) Process for the production of chlorine dioxide
EA200700628A1 (en) CONTINUOUS METHOD FOR OBTAINING PHENOL FROM BENZENE IN A REINFORCED LAYER
GB2593207B (en) A continuous type process method to increase the rate of reaction between solids, liquids, and gasses per area of the land occupied by two reactors
BR9911999A (en) Process for hydroformylation of a substrate
CA2106089C (en) Catalysed hypochlorite decomposition process
김종호 Evolution of Human Chemistry and Its Future
GB202004408D0 (en) A continuous type process method to increase the rate of reaction between solids, liquids, and gasses per area of the land occupied by two reactors.
Janecki et al. Catalytic wet air oxidation of phenol in the trickle-bed reactor operating under steady and periodically changing liquid flow
Shi et al. KINETICS AND MECBANISM OF BENZOTHIOPHENE HYDRODESULFURIZATION OVER NiO-MoO/y-Al 2 0 3 COMMERCIAL CATALYST