IL74131A - Process for the preparation of tetronic acid - Google Patents
Process for the preparation of tetronic acidInfo
- Publication number
- IL74131A IL74131A IL74131A IL7413185A IL74131A IL 74131 A IL74131 A IL 74131A IL 74131 A IL74131 A IL 74131A IL 7413185 A IL7413185 A IL 7413185A IL 74131 A IL74131 A IL 74131A
- Authority
- IL
- Israel
- Prior art keywords
- preparation
- acid
- tetronic acid
- converted
- ester
- Prior art date
Links
- PGRHXDWITVMQBC-UHFFFAOYSA-N dehydroacetic acid Natural products CC(=O)C1C(=O)OC(C)=CC1=O PGRHXDWITVMQBC-UHFFFAOYSA-N 0.000 title abstract 3
- PEQJBOMPGWYIRO-UHFFFAOYSA-N n-ethyl-3,4-dimethoxyaniline Chemical compound CCNC1=CC=C(OC)C(OC)=C1 PEQJBOMPGWYIRO-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- 150000002148 esters Chemical class 0.000 abstract 3
- DJEJYZZJYYNADA-UHFFFAOYSA-N 3-chlorooxolane-2,4-dione Chemical compound ClC1C(=O)COC1=O DJEJYZZJYYNADA-UHFFFAOYSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000005660 chlorination reaction Methods 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 abstract 1
- 238000007669 thermal treatment Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D307/60—Two oxygen atoms, e.g. succinic anhydride
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Furan Compounds (AREA)
- Cephalosporin Compounds (AREA)
Abstract
1. Process for the preparation of tetronic acid from 4-chloroacetoacetic ester, characterized in that 4-chloroacetoacetic ester is converted into the 2,4-dichloroacetoacetic ester by chlorination, the latter is converted into 3-chlorotetronic acid by thermal treatment at temperatures of 110 to 1608C, and the latter acid is converted into tetronic acid by hydrogenation with hydrogen in the presence of a platinum metal catalyst.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH604/84A CH658056A5 (en) | 1984-02-09 | 1984-02-09 | METHOD FOR PRODUCING TETRONIC ACID. |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IL74131A0 IL74131A0 (en) | 1985-04-30 |
| IL74131A true IL74131A (en) | 1988-11-30 |
Family
ID=4190834
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL74131A IL74131A (en) | 1984-02-09 | 1985-01-22 | Process for the preparation of tetronic acid |
Country Status (12)
| Country | Link |
|---|---|
| EP (1) | EP0153615B1 (en) |
| JP (1) | JPS60184073A (en) |
| AT (1) | ATE42550T1 (en) |
| CA (1) | CA1225094A (en) |
| CH (1) | CH658056A5 (en) |
| DD (1) | DD229126A5 (en) |
| DE (1) | DE3569735D1 (en) |
| HU (1) | HU196066B (en) |
| IL (1) | IL74131A (en) |
| IN (1) | IN162567B (en) |
| MX (1) | MX156171A (en) |
| SU (1) | SU1436868A3 (en) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63112883U (en) * | 1987-01-13 | 1988-07-20 | ||
| CA2210821A1 (en) * | 1996-09-04 | 1998-03-04 | Lonza Ag | Process for the preparation of an arylazotetronic acid derivative |
| CA2211503A1 (en) * | 1996-09-04 | 1998-03-04 | Josef Schroer | Process for the preparation of tetronic acid derivatives |
| AUPQ841900A0 (en) * | 2000-06-28 | 2000-07-20 | Unisearch Limited | Synthesis of cyclic compounds |
| EP2039678A1 (en) | 2007-09-18 | 2009-03-25 | Bayer CropScience AG | Method for manufacturing 4-aminobut-2-enolids |
| EP2042496A1 (en) | 2007-09-18 | 2009-04-01 | Bayer CropScience AG | Method for manufacturing 4-aminobut-2-enolids |
| JP2010070460A (en) | 2008-09-16 | 2010-04-02 | Daicel Chem Ind Ltd | Method for producing tetronic acid |
| EP2230236A1 (en) | 2009-03-16 | 2010-09-22 | Bayer CropScience AG | New method for producing enaminocarbonyl compounds |
| EP2230237A1 (en) | 2009-03-16 | 2010-09-22 | Bayer CropScience AG | New method for producing enaminocarbonyl compounds |
| TW201111370A (en) | 2009-08-18 | 2011-04-01 | Bayer Cropscience Ag | Novel process for the preparation of 4-aminobut-2-enolides |
| CN103097378B (en) | 2009-12-23 | 2015-02-25 | 拜耳知识产权股份有限公司 | Novel method for preparing 4-aminobut-2-enolides starting from 4-alkoxyfuran-2(5H)-on or 4-arylalkoxyfuran-2-(5H)-on |
| CN106632081A (en) * | 2016-12-14 | 2017-05-10 | 四川同晟生物医药有限公司 | 5-chloro-6-(chloromethyl) uracil and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH529128A (en) * | 1970-09-04 | 1972-10-15 | Lonza Ag | Process for the production of tetronic acid |
| CH649996A5 (en) * | 1981-06-17 | 1985-06-28 | Lonza Ag | PROCESS FOR THE PRODUCTION OF TETRONIC ACID. |
| CH649294A5 (en) * | 1981-06-17 | 1985-05-15 | Lonza Ag | METHOD FOR PRODUCING TETRONIC ACID. |
-
1984
- 1984-02-09 CH CH604/84A patent/CH658056A5/en not_active IP Right Cessation
-
1985
- 1985-01-14 HU HU85132A patent/HU196066B/en not_active IP Right Cessation
- 1985-01-18 DD DD85272648A patent/DD229126A5/en not_active IP Right Cessation
- 1985-01-22 IL IL74131A patent/IL74131A/en unknown
- 1985-01-22 IN IN52/MAS/85A patent/IN162567B/en unknown
- 1985-02-04 AT AT85101150T patent/ATE42550T1/en not_active IP Right Cessation
- 1985-02-04 EP EP85101150A patent/EP0153615B1/en not_active Expired
- 1985-02-04 DE DE8585101150T patent/DE3569735D1/en not_active Expired
- 1985-02-06 MX MX204247A patent/MX156171A/en unknown
- 1985-02-07 CA CA000473780A patent/CA1225094A/en not_active Expired
- 1985-02-08 SU SU853853848A patent/SU1436868A3/en active
- 1985-02-08 JP JP60023386A patent/JPS60184073A/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| MX156171A (en) | 1988-07-19 |
| CH658056A5 (en) | 1986-10-15 |
| SU1436868A3 (en) | 1988-11-07 |
| HUT39441A (en) | 1986-09-29 |
| HU196066B (en) | 1988-09-28 |
| EP0153615A1 (en) | 1985-09-04 |
| CA1225094A (en) | 1987-08-04 |
| EP0153615B1 (en) | 1989-04-26 |
| JPS60184073A (en) | 1985-09-19 |
| DD229126A5 (en) | 1985-10-30 |
| DE3569735D1 (en) | 1989-06-01 |
| IL74131A0 (en) | 1985-04-30 |
| IN162567B (en) | 1988-06-11 |
| JPS6156232B2 (en) | 1986-12-01 |
| ATE42550T1 (en) | 1989-05-15 |
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