IE990654A1 - Method of Cleaning Metal Components - Google Patents

Method of Cleaning Metal Components

Info

Publication number
IE990654A1
IE990654A1 IE990654A IE990654A IE990654A1 IE 990654 A1 IE990654 A1 IE 990654A1 IE 990654 A IE990654 A IE 990654A IE 990654 A IE990654 A IE 990654A IE 990654 A1 IE990654 A1 IE 990654A1
Authority
IE
Ireland
Prior art keywords
components
hydrogen
elevated temperature
retort
fluoride
Prior art date
Application number
IE990654A
Inventor
Kenneth Gove
Original Assignee
Sifco Res & Dev Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from IES980638 external-priority patent/IES980638A2/en
Application filed by Sifco Res & Dev Ltd filed Critical Sifco Res & Dev Ltd
Priority to IE990654A priority Critical patent/IE990654A1/en
Publication of IE990654A1 publication Critical patent/IE990654A1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23GCLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
    • C23G5/00Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)

Abstract

A process of cleaning components, in particular nickel or cobalt based super alloys which are used for the manufacture of aircraft and land based gas turbine engines, is described. The cleaning of the superalloys usually takes place prior to repair of cracks or other defects in the components. The process involves the placing the components in a furnace retort, or some other similar sealed vessel, heating the components to an elevated temperature, and while at said elevated temperature introducing a geseous mixture of fluoride and chloride ions into the retort. Preferably, the halide gases introduced to the retort are hydrogen fluoride and hydrogen chloride.

Description

“METHOD OF CLEANING METAL COMPONENTS” A process of cleaning components, in particular nickel or cobalt based super alloys which are used for the manufacture of aircraft and land based gas turbine engines, is described. The cleaning of the superalloys usually takes place prior to repair of cracks or other defects in the components. The process involves the placing the components in a furnace retort, or some other similar sealed vessel, heating the components to an elevated temperature, and while at said elevated temperature introducing a geseous mixture of fluoride and chloride ions into the retort. Preferably, the halide gases introduced to the retort are hydrogen fluoride and hydrogen chloride.

Claims (12)

1. A process for cleaning cracks and other surface defects in components made from metallic based superalloys, prior to the repair of the crack by brazing and the like, comprising the steps of: a) placing the component in a furnace retort b) heating the furnace to an elevated temperature, and while at said elevated temperature, c) introducing a gaseous atmosphere into said retort, characterised in that the gaseous atmosphere comprises a mixture of hydrogen, a gaseous source of fluoride ions and a gaseous source of chloride ions.
2. The process as claimed in claim 1, wherein the gaseous source of fluoride ions is hydrogen fluoride and the gaseous source of chloride ions is hydrogen chloride
3. The process as claimed in any preceding claim, wherein the gaseous atmosphere comprises up to 20% hydrogen fluoride, a volume of hydrogen chloride comprising 1 to 2% of the volume of hydrogen fluoride and the balance comprising hydrogen.
4. The process as claimed in any preceding claim, wherein the elevated temperature is substantially in the range 950°C to 1000°C.
5. The process as claimed in any of the preceding claims where the elevated temperature is about 975°C.
6. The process as claimed in any preceding claim wherein the metallic based superalloys are selected from nickel and/ or cobalt based superalloys.
7. The process as claimed in any preceding claim comprising the additional preliminary step of removing any oxide material adhering to the components.
8. The process as claimed in any one of the preceding claims comprising the additional preliminary step of removing sulphide and/or oxy-sulphide deposits from the components by immersing the components in solutions comprising one or more of 5 the following compounds: a) nitric acid, b) acetic acid, c) phosporic acid, and d) ferric chloride.
9. The process as claimed in claim 4 wherein the heating process is carried out for a duration from about 15 to about 60 minutes.
10. A process for cleaning cracks and other surface defects in components made
11. 15 from metallic based superalloys substantially as described hereinbefore with reference to and/ or as illustrated in Figure 1.
12. 20 Tomkins & Co.
IE990654A 1998-07-30 1999-07-29 Method of Cleaning Metal Components IE990654A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
IE990654A IE990654A1 (en) 1998-07-30 1999-07-29 Method of Cleaning Metal Components

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
IES980638 IES980638A2 (en) 1998-07-30 1998-07-30 Method of cleaning metal components
IE990654A IE990654A1 (en) 1998-07-30 1999-07-29 Method of Cleaning Metal Components

Publications (1)

Publication Number Publication Date
IE990654A1 true IE990654A1 (en) 2000-04-05

Family

ID=27624393

Family Applications (1)

Application Number Title Priority Date Filing Date
IE990654A IE990654A1 (en) 1998-07-30 1999-07-29 Method of Cleaning Metal Components

Country Status (1)

Country Link
IE (1) IE990654A1 (en)

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