IE53415B1 - Vacuum packaging apparatus and process - Google Patents
Vacuum packaging apparatus and processInfo
- Publication number
- IE53415B1 IE53415B1 IE229282A IE229282A IE53415B1 IE 53415 B1 IE53415 B1 IE 53415B1 IE 229282 A IE229282 A IE 229282A IE 229282 A IE229282 A IE 229282A IE 53415 B1 IE53415 B1 IE 53415B1
- Authority
- IE
- Ireland
- Prior art keywords
- receptacle
- gas
- pressure
- chamber
- vacuum
- Prior art date
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- Vacuum Packaging (AREA)
Abstract
"VACUUM PACKAGING APPARATUS AND PROCESS" A vacuum packaging process and apparatus employ the novel step of deliberatety at least partically repressurizing the exterior of a packaging receptacle after commencement of the evacuation of the exterior and interior of the receptacle in a chamber. Two separate gas pressure restroation phases may be employed, separated by a resumption of the gas extraction, and the receptacle is closed during the second of these gas pressure restoration phases.
Description
The present invention relates to a process of and apparatus for packaging an article in a receptacle to obtain a vacuum pack.
Hitherto it has been known to package an article in a plastics envelope, such as a plastic bag, by loading the article in the envelope and then inserting the loaded envelope into a vacuum chamber for the atmosphere around the envelope to be reduced in pressure so that the air or other gas within the envelope is extracted and finally the envelope can be sealed under low pressure conditions. The resulting package is termed a vacuum package.
It is also known for the operation of the process to be such that during the reduction in pressure of the atmosphere around the envelope, the wall of the envelope baloons away from the enclosed article, so that the extraction of air from within the envelope can be more effectively carried out. Such a system has, for example, been disclosed in US-A-3 714 754 (Holcombe) using a nozzle to extract air from within the envelope while the pressure of the atmosphere around the envelope has
S3415 reduced to effect the necessary ballooning action. Ballooning has furthermore been disclosed in US-A-3 832 824 (Burrell) in which the vacuum chamber in which the envelope is closed has two portions of which a first portion encloses the envelope mouth and the second portion encloses the article-enclosing remainder of the envelope so that the pressure around the exterior of the envelope can initially be reduced more rapidly than the pressure within the envelope (in order to promote the desired ballooning effect). Such a process is suitable for a high vacuum pack when a long evacuation step can be tolerated. Furthermore, sealing the pack while it is in a ballooned condition will give rise to uncertainty of the volume of residual air still . in the pack at the time of sealing, leading to uncertainty of the air pressure within the sealed bag when the pack exterior is returned to atmospheric pressure outside the chamber.
When using such process for packing products having a porous structure the high vacuum applied can remove air out of the product so that the structure of the product will be destroyed or at least damaged.
It has further been found that, with these prior art arrangements, when a short evacuation step (for example for a
534»S so-called soft vacuum pack) is needed, there is a possibility for air to become trapped behind the product article and for pockets of such air to be trapped within the sealed pack.
It is an object of the present invention to provide an improved method and apparatus for packaging articles in a receptacle so as to overcome the disadvantages of the prior art.
Accordingly, the present invention provides a process for vacuum packaging an article in a flexible receptacle, comprising loading the article in the receptacle, extracting gas from around the exterior of the receptacle to lower the surrounding pressure, extracting gas from within the receptacle, and closing the receptacle in a gas-tight manner after the extraction of gas from its interior, wherein after the pressure surrounding the receptacle has been initially lowered, the pressure is raised in a pressure restoration phase before closing the receptacle, and after said pressure restoration phase the pressure surrounding the receptacle is lowered in a further pressure reduction step before the receptacle is closed.
By such additional pressure reduction step with a following pressure restoration phase a repeated inward and outward oscillation of the wall of the receptacle and therefore a pumping effect is achieved which causes removal of gas trapped in pockets in the pack.
A further aspect of the present invention provides apparatus for vacuum packaging, comprising a vacuum chamber having an extraction pump for extracting gas from within the interior of the chamber and a support for a loaded receptacle to be evacuated and sealed in the chamber; means for restoring pressure to the exterior of a receptacle disposed within the vacuum chamber after partial evacuation of the chamber by the extraction pump before the receptacle is closed; and means for closing a receptacle in the chamber; programming means being provided to ensure further pressure reduction in the chamber after operation of the pressure restoration means.
In order that the present invention may more readily be understood the following description is given, merely by way of example, with reference to the accompanying drawings in
3 413 which:-
Figure 1 is a schematic side elevationai view of a first embodiment of vacuum packaging apparatus in accordance with the present invention; 5 Figure 2 is a view similar to Figure 1 but showing a second embodiment of apparatus in accordance with the invention; 10 Figure 3 is a cycle timing diagram showing the residual pressure P in the chamber plotted against time T of the cycle; Figure 4 is a view similar to Figure 1 but showing the apparatus during operation of the vacuum pump and with the air admission valve closed; 15 Figure 5 is a view similar to Figure 4 but showing the effect of the air admission valve in the open configuration; and Figure 6 is a view similar to Figure 5 but showing the
envelope-closing mechanism in operation
The vacuum chamber 1 shown in Figure 1 is of a conventional form and includes a vacuum enclosure comprising a cover 2 on a base 3 to which the cover is sealed along its rim
4. An air extraction duct 5 leads to an extraction pump 6 5 whose discharge duct 7 conveys away air which has been extracted from the chamber 1.
The chamber further includes a receptacle-closing unit 8 having a driven mechanism 9, here comprising a pair of opposed hot weld bars 10 which are driven towards one another to contact the neck region of the receptacle 11 (in this case a plastic bag of heat shrinkable thermoplastic material) and are energized with a pulse of electric energy to heat seal the neck region of the envelope before the chamber 1 opens. This closing unit is also associated with an optional yieldable bag holding means 21, here shown as a resilient blade 22 clamped along one edge (in this case the upper edge) and having its opposite, free edge (in this case the lower edge) disposed nearer to the bag mouth and nearer to an opposed anvil 23.
The embodiment of the present invention provides for the incorporation of an air admission valve 12 on the chamber cover 2 to admit air into the chamber while the extraction pump is in operation. This unexpected modification has the surprising advantage of being able to allow more effective extraction of air from within the receptacle 11 provided the air admission value is operated in accordance with the process of the present invention.
The air admission valve 12 includes an airflow regulator lever 13 allowing a throttle 14 to be adjusted to give 10 the desired rate of venting of the valve 12 when in its open configuration. Furthermore, the valve 12 is connected, by pneumatic control line 15, to a pneumatic control unit 16 which provides signal pulses to the valve 12 in response to the vacuum level in the chamber 1 as sensed by way of a sensing conduit
17. It is expected that the reate of admission of air through the throttle 14 will be grater than the rate of extraction by the pump 6.
The control unit 16 for the air admission valve 12 includes a selector control 19 allowing adjustment of the parti20 cular valve of the residual pressure within the chamber 1 at which the valve 12 is opened and closed.
83415
As will be indicated below, making the control unit 16 responsive to the chamber pressure is an optional feature, although this type of control does provide a particularly convenient way of controlling the operation of the air admission valve 12 when carrying out the process of the present invention.
To perform the process in accordance with the invention, the chamber cover 2 is closed over the open receptacle 11 with article 18 therein, and the extraction pump 6 is energized to begin extraction of air from within the chamber 1 and consequently from within the receptacel 11 (by virtue of the neck region being yieldable held by the holding means 21 in the region adjacent the two spaced welding bars 10 of the closing mechanism 8).
Ideally the welding bars 10 are, during extraction, spaced apart such that air is extracted at a controlled rate from within the receptacel 11 as the blade 22 yields, and this rate of extraction is less than the rate of pressure decrease in the atmosphere within the chamber 1 but around the exterior of the receptacle 11, with the result that the receptacle 11 balloons outwardly away from the article 18.
534 15
According to the invention, the air admission valve 12 should then be opened in order to vent air into the end of the chamber 1 where the article-enclosing part of the bag is located (preferably by simply opening the chamber 1 directly to atmosphere to allow atmospheric air to mix with the residual atmosphere around the exterior of the receptacle 11). Where the receptacel has already ballooned away from the article, this venting has the result that the receptacle 11 is pressed inwardly against the exterior of the article 18.
During this gas pressure restoration phase, the extraction of air from within the receptacle 11 will continue and in the case of a flexible bag 11 the thrusting of the flexible bag material 11 onto the product article helps to pump air from within the bag 11. The operation of the air admission valve and the extraction pump, as well as of the receptacle closing means 8 is controlled by a programmer 20 which maintains the pump 6 in operation even during gas pressure restoration phases.
Where a yieldable bag holding means 21 is included, the blade 22 will remain in its yielded position (due to its elastic nature and its particular inclination) while air is being expelled from within the bag but will close off the bag neck
834 15 when air pressure outside the bag neck region has risen to a value which impedes air venting from the bag.
The air pressure restoration phase is of limited duration so that when the air admission valve 12 is reclosed the continuing operation of the extraction pump 6 will effect extraction of the now slightly higher pressure atmosphere around the bag 11, while still evacuating the lower pressure interior of the bag 11. This extraction of the external air from around the bag may shortly result in recurrence of the ballooning phenomenon, whereupon the air admission valve 12 is once again opened to build up gas pressure around the bag 11 to thrust the bag material onto the article 18 to achieve a pulsating reinforcement of the air extraction from within the bag 1.
It is envisaged that this pulsating action of success15 ful pressure reductions followed by pressure increases on the exterior of the receptacle can continue until a desired configuration has been obtained at which time the receptacle 11 is closed by operation of the closing means 8 when its actuating means 9 are energized. However, it is preferred for the cycle to continue for only two repressurization pulses, even though the use of more than two such pulses is within the scope of such process according to the present invention.
Figure 2 illustrates an alternative embodiment of the apparatus in accordance with the present invention, differing
only in that the air admission valve 12 is connected in the extraction duct 5 to the pump 6. The functional result will be 5 the same in that the successive opening and closing of the air admission valve 12 superimposed on the conti nuous operation of
the extraction pump 6 will achieve a pulsating pressure in the residual atmosphere around the receptacle 11 in both Figure 1 and Figure 2. It will of course be understood that the air admission valve 12 in Figure 1 need not be incorporated on the cover 2; air admission means of any suitable form could be used, for example a valve connected to an air admission port in the base 3 inwardly of the position occupied by the rim 4 of the cover 2 in the closed configuration of the chamber.
The embodiment of Figure 2 also includes an adjustable throttle valve 14 having a control lever 13, and an adjuster 19 on the control unit 16 for selecting a different pressure value at which the air admission valve 12 is to open or close.
Although, in Figure 1 and in Figure 2, the air admission valve 12 is operated in response to attainment of particular pressure valve in the chamber 1, as indicated above, it is not essential for the control of the air admission valve to be responsive to chamber pressure. For example, the control unit 16 may be a pulsing controller of a pneumatic type which Imposes pressure of suction pulses on the control line 15 to the air admission valve 12 at predetermined time intervals after commencemennt of the evacutation of the chamber 1. Alternatively, the control unit 16 may not be pneumatic but may be connected to the valve 12 by a mechanical linkage or by an electrical linkage, in which case the pressure- or time-responsive controller will be of a mechanical or an electrical type, respectively. Yet a further possibility suitable where the receptacle is a plastic envelope is for a mechanical feeler unit to be incorporated within the chamber 1 in order to detect when the flexible envelope such as bag 11 balloons, since the ballooned state of the bag 11 at the instant of the opening of the air admission valve 12 assists the extraction operation.
Throughout the following description, the mechanism of Figure 1 for use with plastics flexible bags 11 will be described in its detailed operating cycle, with reference to the cycle diagram of Figure 3 and with reference to Figures 4, 5 and 6 showing the apparatus of Figure 1 at different states in its operating cycle. It will of course be appreciated that the different locations Of the control line 15a and the sensing line
5341S
17a^ in Figures 4 to 6 with respect to the positions of the corresponding lines 15 and 17 in Figures 1 is of no functional significance but is simply to illustrate the fact that the routing of these lines is purely optional at the discretion of the machine designer.
Figure 3 shows that at the start of a typical operating cycle the pressure within the chamber is at a value Pp normally the atmospheric pressure in the packaging room.
The machine is set up by adjusting the throttle 10 control lever 13 to give the desired air admission rate, and also adjusting the pressure control 19 to select a particular pressure at which the control unit 16 operates to create a signal pulse in control line 15. This pressure Pg is shown in Figure .3.
Referring now to the operating cycle depicted in 15 Figure 3, once that chamber 1 is closed the pressure P reduces
from initial value P^ at point 1 to a value Pg which has been preset on the control 19, and at which the control unit 16 sends a signal pulse - to the valve 12. As this pulse is being
transmitted to the valve 12, the pressure P is till reducing 20 below the value Pg between points II and point III on the pressure/time curve. The opening of the air admission valve 12
83415 will, however, result in a reduction in the rate of extraction of air by the pump 6 and consequently the pressure P bottoms out at a value P^ at point III, and then begins to rise towards the value which is attained at point IV on the curve. At this point the control unit 16 emits another signal pulse closing the air admission valve 12, but nevertheless there remains an upward swing in the pressure value towards the point V on the curve. This upward swing flattens out at point V at pressure value Pg, and the pressure then begins to reduce towards point
VI on the curve. The above-described sequence of events between points II, III, IV and V is repeated between points VI, VII, VIII and IX. However, somewhere between points VII and IX the receptacle-closing unit 8 is operated to seal the bag 11 while the pressure around the bag is increasing and pumping out residual air from within the envelope. This is a preferred aspect of the invention and ensures optimum elimination of trapped bubbles of air or other gas from within the bag 1.
It is particularly preferable for the programmer 20 to trigger the closing action to occur between points VIII and
IX, so that the repressurization pulse on the envelope has had a chance to build up momentum.
It will readily be appreciated that the flexible bag
3 415 balloons at some stage between points 1 and III, collapses between points 111 and V, balloons again between points \l and VII and collapses between points VII and IX.
Where a particularly high vacuum (low residual pressure) is required within the bag 11, it may be envisaged that the receptacle-closing means 8 are operated between points VI and VII or between corresponding points on a further descending half cycle of the curve after point IX.
The process described above has been performed successfully for the packaging of cheese where a relatively soft vacuum is advantageous but where the size of the cheese pack may be such that conventionally the air extraction operation takes a considerable time. It has been found that the extraction time is reduced wtih such process in accordance with the present invention and the occurrence of trapped gas pockets in the pack (particularly likely in the case of Emmental cheese having cavities formed in the surface of the cheese block) is reduced. Although the present invention is not to be limited by any speculation on the functional advantages of the process, it is thought that the inward and outward oscillation of the wall of the receptacle (in the case of a flexible bag 11) due to the pulsating pressure on its exterior results in a pumping action which urges escape of gas (e.g. air) through the neck of the bag 11 with great momentum while the bag is still ballooned, and that this assists in persuading trapped gas pockets to escape. Furthermore, this ensures that the residual pressure right through the pack Is more uniform than is possible with prior art vacuum packaging processes.
It is envisaged that the process described will be equally applicable to high vacuum (low residual pressure) packaging as to soft vacuum packaging (with relatively higher residual pressure values).
Figure 4 illustrates the condition of the apparatus between points I, II and III of the cycle diagram of Figure 3. This same configuration applies between points V, VI and VII. The extraction, pump 6 is in operation but the air admission valve 12 is closed.
Figure 5 illustrates the configuration between points III, IV and V in the cycle diagram of Figure 3. This configuration is repeated between points VII, VIII and IX. The air admission valve receives a signal along the signal line 15a end opens to admit air into the chamber 1.
$3413
Figure 6 illustrates the configuration at one instant during the interval between points VIII and IX, shortly before point IX, when the control unit 16 transmits a signal pulse along the signal line 15a and closes the air admission valve 12 while the receptacle-closing means 8 are actuated to seal the envelope.
If desired, the sealed receptacle 11 may be subjected to a shrinking operation to cause the receptacle material to contact the article 18 intimately.
Although it is envisaged that the apparatus in accordance with the present invention may be equipped from the outset with repressurization means such as the air admission valve 12, it is also within the scope of the present invention for an existing vacuum chamber machine to be modified, simply by the addition of repressurization means such as the air admission valve 12 (and suitable control means therefor) either on the chamber 1 or on the extraction conduit 5, so as to modify that existing machine to operate in accordance with the processes of the present invention. '
Although, in the above description, the envelope5 closing means 8 comprises a heat sealing bar arrangement, other suitable closing mechanisms may be provided, for example radiant heat fusion sealing means operating in conjuction with the yieldable holding means 21 to allow escape of air from within the receptacle 11 before the emission of a radiant heat
IQ pulse to cause the receptacle to fuse upon pressing contact with itself by the increasing pressure in the chamber 1 between points VII and IX of Figure 3.
Other closing systems such as a gathering and clipping mechanism may instead be provided. Likewise, although the apparatus illustrated In Figures 1, 2, 4, 5 and 6 shows a single, open chamber, it is of course possible for the processes of the present invention to be carried out using the in-chamber nozzle disclosed in the above mentioned US-A-3 714 754, or in the double chamber construction disclosed in the above mentioned US-A-3 832 824.
As mentioned above, the operation of the air admission valve 12 may be controlled simply on the basis of time elapsed since the start of the cycle, or in response to operation of a mechanical feeler, and both of these control mechanisms can be incorporated as modifications to existing vacuum chamber packaging equipment.
Claims (21)
1. A process for vacuum packaging an article in a flexible receptacle, comprising loading the article in the receptacle, extracting gas from around the 5 exterior of the receptacle to lower the surrounding pressure, extracting gas from within the receptacle, and closing the receptacle in a gas-tight manner after the extraction of gas from its interior, wherein after the pressure surrounding the 10 receptacle has been initially lowered, the pressure is raised in a pressure restoration phase, before the receptacle is closed, and after said pressure restoration phase the pressure surrounding the receptacle is lowered in a further pressure reduction 15 step before the receptacle is closed. 5 3 415
2. A process according to claim 1, wherein there are only two phases during which pressure is restored surrounding the exterior of the receptacle, these pressure restoration phases being separated by a pressure reduction 5 step in which gas is extracted from the exterior of the receptacle, and the receptacle being closed during the second of said pressure restoration phases.
3. A process according to claim' 1 or 2, wherein the loaded receptacle is placed in a vacuum 10 chamber and the closing of the receptacle is also carried out within the vacuum chamber.
4. A process according to claim 3, wherein the vacuum chamber is connected to an extraction pump, and the restoration of gas to the exterior of the 15 receptacle is carried out by opening a valve which allows gas to enter the chamber at a rate which is greater than the rate of extraction by the extraction pump.
5. A process according to claim 4, wherein the extraction pump operates continuously and the venting 20 valve, which opens while the gas extraction pump is in operation, is capable of introducing gas into the chamber at a rate faster than the rate of extraction by the extraction pump.
6. A process according to any one of claims 1 to 5, wherein the receptacle is a flexible envelope which balloons away from the article during said pressure reduction step and becomes pressed down against the product article during said gas pressure restoration phase.
7. A process according to any one of claims 1 to 6, wherein the receptacle is yieldably held closed during 10 the gas extraction escape of air from, receptacle. and gas restoration periods, to allow into, the but to impede re-entry of air 8. Apparatus for vacuum packaging, comprising a vacuum chamber having an extraction pump for extracting gas from 15 within the interior of the chamber and a support for a loaded flexible receptacle to be evacuated and sealed in the chamber; means for restoring pressure to the exterior of a receptacle disposed within the vacuum chamber after partial evacuation of the chamber by the 20 extracticn pump before the receptacle is closed; and means for closing a receptacle in the chamber; 2d programming means being provided to ensure further pressure reduction in the chamber after operation of the pressure restoration means» 91 Apparatus according to claim 8, wherein the 5 programming means ensure that the pressure restoration means carry out at least two pressure restoration phases separated by a pressure reduction step during which gas is extracted from within the chamber by the extraction pump.
8. 10 10. Apparatus according to claim 8 or 9, wherein said pressure restoration means comprises a gas admission valve connected to the space evacuated by the extraction pump.
9. 11. Apparatus according to claim 10, wherein said lb gas admission valve is connected to a wall of the vacuum chamber.
10. 12. Apparatus according to claim 10, wherein said gas admission valve is connected to an extraction duct between the vacuum chamber and the extraction pump.
11. 13. Apparatus according to any one of claims 10 to 12, wherein said gas admission valve includes a variable throttle valve for adjusting the rate of admission of gas to the chamber 5
12. 14. Apparatus according to any one of claims 10 to 13, wherein said gas admission valve is controlled in response to the vacuum level in the vacuum chamber by a control unit and a vacuum sensing line. 10 15. Apparatus according to claim 14, wherein said vacuum level-responsive control unit includes means for selecting a particular vacuum level at which the control unit sends a signal to open or close the gas admission valve,
13. 15
14. 16. Apparatus according to any one of claims 10 to 13, wherein the gas admission valve is controlled by a timer according to a predetermined program of gas admission phases when the valve is open and pressure reduction steps when the valve is 20 closed and the extraction pump is in operation.
15. 17. Apparatus according to any one of claims 10 to 16 wherein the programming means are effective to open and. close the gas admission valve according to a predetermined program, to maintain operation of the extraction pump during gas extraction phases and gas 5 restoration phases, and to operate the bag closing means during a pressure restoration phase while the gas admission valve is open.
16. 18. Apparatus according to any one of claims 8 to 17, wherein the bag closing means comprises 10 opposed heat seating bars which, for bag closing, are driven together and energized electrically to impart sealing heat to clamped wall portions of the receptacle.
17. 19. Apparatus according to any one of claims 8 to 18, including yieldable holding means for holding 15 the receptacle substantially closed while allowing air to vent from the interior of the receptacle.
18. 20. Apparatus according to claim 19, wherein the yieldable holding means includes an elastic blade and an anvil to hold a portion of the receptacle 20 therebetween.
19. 21. A process according to claim 1 for vacuum packaging an article in a flexible receptacle, such process being substantially as hereinbefore described with reference to the accompanying drawings. 5
20. 22. Apparatus according to claim 8 for vacuum packaging, such apparatus being constructed and adapted to operate substantially as hereinbefore described with reference to, and as illustrated in the accompanying drawings·
21. 23. An article in a flexible receptacle whenever vacuum 10 packaged by a process claimed in a preceding claim.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IT24538/81A IT1139239B (en) | 1981-10-16 | 1981-10-16 | VACUUM PACKAGING EQUIPMENT AND PROCEDURE |
EP82108140A EP0077458B1 (en) | 1981-10-16 | 1982-09-03 | Vacuum packaging apparatus and process |
Publications (2)
Publication Number | Publication Date |
---|---|
IE822292L IE822292L (en) | 1984-03-03 |
IE53415B1 true IE53415B1 (en) | 1988-11-09 |
Family
ID=26084275
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
IE229282A IE53415B1 (en) | 1981-10-16 | 1982-09-21 | Vacuum packaging apparatus and process |
Country Status (9)
Country | Link |
---|---|
AR (1) | AR228686A1 (en) |
AT (1) | ATE17213T1 (en) |
AU (1) | AU549772B2 (en) |
CA (1) | CA1291412C (en) |
DK (1) | DK456382A (en) |
FI (1) | FI72474C (en) |
IE (1) | IE53415B1 (en) |
NO (1) | NO156562C (en) |
NZ (1) | NZ202174A (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1989001440A1 (en) * | 1987-08-18 | 1989-02-23 | Alfa-Laval Engineering Pty. Limited | Improved vacuum packaging technique and devices |
-
1982
- 1982-09-03 AT AT82108140T patent/ATE17213T1/en not_active IP Right Cessation
- 1982-09-21 IE IE229282A patent/IE53415B1/en unknown
- 1982-10-14 AU AU89366/82A patent/AU549772B2/en not_active Ceased
- 1982-10-14 FI FI823503A patent/FI72474C/en not_active IP Right Cessation
- 1982-10-14 NO NO823431A patent/NO156562C/en unknown
- 1982-10-14 DK DK456382A patent/DK456382A/en not_active Application Discontinuation
- 1982-10-14 NZ NZ20217482A patent/NZ202174A/en unknown
- 1982-10-14 AR AR29096682A patent/AR228686A1/en active
- 1982-10-15 CA CA000413519A patent/CA1291412C/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
NO156562C (en) | 1987-10-14 |
ATE17213T1 (en) | 1986-01-15 |
AU549772B2 (en) | 1986-02-13 |
AU8936682A (en) | 1983-04-21 |
NO156562B (en) | 1987-07-06 |
AR228686A1 (en) | 1983-03-30 |
CA1291412C (en) | 1991-10-29 |
FI72474B (en) | 1987-02-27 |
NZ202174A (en) | 1986-05-09 |
FI72474C (en) | 1987-06-08 |
FI823503A0 (en) | 1982-10-14 |
IE822292L (en) | 1984-03-03 |
DK456382A (en) | 1983-04-17 |
FI823503L (en) | 1983-04-17 |
NO823431L (en) | 1983-04-18 |
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