IE41103B1 - Method for preparing bis-(2-pyridyl-1-oxide) disulfide - Google Patents

Method for preparing bis-(2-pyridyl-1-oxide) disulfide

Info

Publication number
IE41103B1
IE41103B1 IE716/75A IE71675A IE41103B1 IE 41103 B1 IE41103 B1 IE 41103B1 IE 716/75 A IE716/75 A IE 716/75A IE 71675 A IE71675 A IE 71675A IE 41103 B1 IE41103 B1 IE 41103B1
Authority
IE
Ireland
Prior art keywords
oxide
pyridyl
disulfide
preparing bis
chloropyridine
Prior art date
Application number
IE716/75A
Other versions
IE41103L (en
Original Assignee
Olin Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Olin Corp filed Critical Olin Corp
Publication of IE41103L publication Critical patent/IE41103L/en
Publication of IE41103B1 publication Critical patent/IE41103B1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/89—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members with hetero atoms directly attached to the ring nitrogen atom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pyridine Compounds (AREA)
  • Cosmetics (AREA)

Abstract

An improved integrated route to bis-(2-pyridyl-1-oxide) disulfide is provided by oxidizing 2-chloropyridine with permaleic acid to form 2-chloropyridine-1-oxide followed by mercaptization with a selected alkali metal sulfide to form the alkali metal salt of 2-mercaptopyridine-1-oxide and then oxidation with hydrogen peroxide under selected pH conditions. [US3892760A]
IE716/75A 1974-05-02 1975-04-02 Method for preparing bis-(2-pyridyl-1-oxide) disulfide IE41103B1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US466328A US3892760A (en) 1974-05-02 1974-05-02 Bis-(2-pyridyl-1-oxide) disulfide

Publications (2)

Publication Number Publication Date
IE41103L IE41103L (en) 1975-11-02
IE41103B1 true IE41103B1 (en) 1979-10-24

Family

ID=23851343

Family Applications (1)

Application Number Title Priority Date Filing Date
IE716/75A IE41103B1 (en) 1974-05-02 1975-04-02 Method for preparing bis-(2-pyridyl-1-oxide) disulfide

Country Status (17)

Country Link
US (1) US3892760A (en)
JP (1) JPS5421344B2 (en)
AR (1) AR208546A1 (en)
BE (1) BE828695A (en)
BR (1) BR7502591A (en)
CA (1) CA1052792A (en)
CH (1) CH597190A5 (en)
DK (1) DK143650C (en)
FI (1) FI58917C (en)
FR (1) FR2269525B1 (en)
GB (1) GB1469907A (en)
IE (1) IE41103B1 (en)
IL (1) IL46996A (en)
IT (1) IT1035419B (en)
NL (1) NL7504696A (en)
SE (1) SE401508B (en)
ZA (1) ZA752024B (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4585871A (en) * 1982-03-26 1986-04-29 Olin Corporation Process for oxidizing halopyridines to halopyridine-N-oxides
US4504667A (en) * 1983-06-24 1985-03-12 Olin Corporation Process for oxidizing halopyridines to halopyridine-N-oxides
JP2002265310A (en) * 2001-03-06 2002-09-18 Nagase Chemtex Corp Antimicrobial agent composition
US6664280B2 (en) 2001-07-25 2003-12-16 The United States Of America As Represented By The Secretary Of The Army Antivesicant compounds and methods of making and using thereof

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2686786A (en) * 1953-01-09 1954-08-17 Olin Mathieson Nu-hydroxy-2-pyridinethiones and method of preparing same
US2742476A (en) * 1953-10-26 1956-04-17 Olin Mathieson Derivatives of 2-mercaptopyridine 1-oxide
DE1224744B (en) * 1956-04-13 1966-09-15 Olin Mathieson Process for the preparation of bactericidal and fungicidal sulfur-containing pyridine compounds
US2951844A (en) * 1958-11-05 1960-09-06 Olin Mathieson Cyclic process for manufacture of 2-chloropyridine-1-oxide
US3759932A (en) * 1972-08-25 1973-09-18 Olin Corp Method for preparing mercaptopyridines using alkali metal polysulfides

Also Published As

Publication number Publication date
US3892760A (en) 1975-07-01
AU7996875A (en) 1976-10-14
DE2519715B2 (en) 1977-03-31
AR208546A1 (en) 1977-02-15
NL7504696A (en) 1975-11-04
SE7505136L (en) 1975-11-03
SE401508B (en) 1978-05-16
JPS50149680A (en) 1975-11-29
DE2519715A1 (en) 1975-11-06
FI751253A (en) 1975-11-03
DK143650B (en) 1981-09-21
ZA752024B (en) 1976-02-25
IT1035419B (en) 1979-10-20
CA1052792A (en) 1979-04-17
BE828695A (en) 1975-11-03
CH597190A5 (en) 1978-03-31
JPS5421344B2 (en) 1979-07-30
BR7502591A (en) 1976-03-16
IL46996A (en) 1977-12-30
DK168275A (en) 1975-11-03
GB1469907A (en) 1977-04-06
DK143650C (en) 1982-02-15
FI58917B (en) 1981-01-30
FI58917C (en) 1981-05-11
FR2269525B1 (en) 1979-10-05
FR2269525A1 (en) 1975-11-28
IE41103L (en) 1975-11-02
IL46996A0 (en) 1975-06-25

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