IE37865B1 - Recovery of formic acid in the manufacture of polyols - Google Patents
Recovery of formic acid in the manufacture of polyolsInfo
- Publication number
- IE37865B1 IE37865B1 IE1099/73A IE109973A IE37865B1 IE 37865 B1 IE37865 B1 IE 37865B1 IE 1099/73 A IE1099/73 A IE 1099/73A IE 109973 A IE109973 A IE 109973A IE 37865 B1 IE37865 B1 IE 37865B1
- Authority
- IE
- Ireland
- Prior art keywords
- formic acid
- polyol
- solvent
- aqueous solution
- manufacture
- Prior art date
Links
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 title abstract 20
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 title abstract 10
- 235000019253 formic acid Nutrition 0.000 title abstract 10
- 229920005862 polyol Polymers 0.000 title abstract 7
- 150000003077 polyols Chemical class 0.000 title abstract 7
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 238000011084 recovery Methods 0.000 title abstract 2
- 239000002904 solvent Substances 0.000 abstract 7
- 239000007864 aqueous solution Substances 0.000 abstract 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- 239000012071 phase Substances 0.000 abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- HTSABYAWKQAHBT-UHFFFAOYSA-N 3-methylcyclohexanol Chemical compound CC1CCCC(O)C1 HTSABYAWKQAHBT-UHFFFAOYSA-N 0.000 abstract 2
- MQWCXKGKQLNYQG-UHFFFAOYSA-N 4-methylcyclohexan-1-ol Chemical compound CC1CCC(O)CC1 MQWCXKGKQLNYQG-UHFFFAOYSA-N 0.000 abstract 2
- -1 aliphatic ketones Chemical class 0.000 abstract 2
- 239000012535 impurity Substances 0.000 abstract 2
- 238000005406 washing Methods 0.000 abstract 2
- AVMSWPWPYJVYKY-UHFFFAOYSA-N 2-Methylpropyl formate Chemical compound CC(C)COC=O AVMSWPWPYJVYKY-UHFFFAOYSA-N 0.000 abstract 1
- NDVWOBYBJYUSMF-UHFFFAOYSA-N 2-methylcyclohexan-1-ol Chemical compound CC1CCCCC1O NDVWOBYBJYUSMF-UHFFFAOYSA-N 0.000 abstract 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 abstract 1
- 150000001299 aldehydes Chemical class 0.000 abstract 1
- 239000008346 aqueous phase Substances 0.000 abstract 1
- FRCHCYFLGZRELU-UHFFFAOYSA-N butan-2-one;cyclohexanone Chemical compound CCC(C)=O.O=C1CCCCC1 FRCHCYFLGZRELU-UHFFFAOYSA-N 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 150000003997 cyclic ketones Chemical class 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 150000004675 formic acid derivatives Chemical class 0.000 abstract 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
- 239000001117 sulphuric acid Substances 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0488—Flow sheets
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2420/00—Metallocene catalysts
- C08F2420/09—Cyclic bridge, i.e. Cp or analog where the bridging unit linking the two Cps or analogs is part of a cyclic group
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Extraction Or Liquid Replacement (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7224619A FR2192088B1 (enrdf_load_stackoverflow) | 1972-07-07 | 1972-07-07 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IE37865L IE37865L (en) | 1974-01-07 |
| IE37865B1 true IE37865B1 (en) | 1977-10-26 |
Family
ID=9101515
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IE1099/73A IE37865B1 (en) | 1972-07-07 | 1973-07-02 | Recovery of formic acid in the manufacture of polyols |
Country Status (12)
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101942035B (zh) * | 2010-09-07 | 2012-03-28 | 天津强微特生物科技有限公司 | 一种根瘤菌胞外多糖的提取及精制方法 |
-
1972
- 1972-07-07 FR FR7224619A patent/FR2192088B1/fr not_active Expired
-
1973
- 1973-06-18 AT AT533773A patent/AT323712B/de not_active IP Right Cessation
- 1973-06-22 NL NL7308690A patent/NL7308690A/xx unknown
- 1973-06-22 LU LU67855A patent/LU67855A1/xx unknown
- 1973-06-25 DE DE2332137A patent/DE2332137A1/de active Pending
- 1973-06-28 ES ES416442A patent/ES416442A1/es not_active Expired
- 1973-07-02 GB GB3135273A patent/GB1429237A/en not_active Expired
- 1973-07-02 IE IE1099/73A patent/IE37865B1/xx unknown
- 1973-07-04 IT IT68978/73A patent/IT991656B/it active
- 1973-07-06 CA CA175,898A patent/CA1039751A/fr not_active Expired
- 1973-07-06 SE SE7309586A patent/SE407404B/xx unknown
- 1973-07-06 BE BE133227A patent/BE802038A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE2332137A1 (de) | 1974-01-24 |
| FR2192088A1 (enrdf_load_stackoverflow) | 1974-02-08 |
| LU67855A1 (enrdf_load_stackoverflow) | 1973-08-30 |
| AT323712B (de) | 1975-07-25 |
| SE407404B (sv) | 1979-03-26 |
| IE37865L (en) | 1974-01-07 |
| BE802038A (fr) | 1974-01-07 |
| CA1039751A (fr) | 1978-10-03 |
| NL7308690A (enrdf_load_stackoverflow) | 1974-01-09 |
| IT991656B (it) | 1975-08-30 |
| FR2192088B1 (enrdf_load_stackoverflow) | 1980-07-25 |
| ES416442A1 (es) | 1976-05-01 |
| GB1429237A (en) | 1976-03-24 |
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