HUT62871A - Process for producing 2-chlorothiazole derivatives - Google Patents
Process for producing 2-chlorothiazole derivativesInfo
- Publication number
- HUT62871A HUT62871A HU340291A HU340291A HUT62871A HU T62871 A HUT62871 A HU T62871A HU 340291 A HU340291 A HU 340291A HU 340291 A HU340291 A HU 340291A HU T62871 A HUT62871 A HU T62871A
- Authority
- HU
- Hungary
- Prior art keywords
- formula
- methyl
- iii
- give
- thiazole
- Prior art date
Links
Landscapes
- Thiazole And Isothizaole Compounds (AREA)
Abstract
Prepn. of 4-methyl-5-(2-chloroalkyl)-thiazole derivs. of formula (I) and their acid addn. salts comprises reacting a 3-thiocyanato-5-chloro- 2-alkanone of formula (II) either: with HCl gas in an organic solvent to give a 2-chloro-4-methyl-5-(2-chloroalky l)-thiazole of formula (III), or; with an aq. mineral acid to give a 2-hydroxy-4-methyl- 5-(2-chloroalkyl)-thiazole of formula (IV) which is treated with a halogenating agent to give (III); followed by hydrogenation of (III) in the presence of a metal catalyst in an organic solvent. In formulae R = 1-5C alkyl, 2-substd. by Cl. Intermediates (II) are new.
Priority Applications (30)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
HU3402/91A HU215840B (en) | 1991-10-30 | 1991-10-30 | Process for producing 2-chlorothiazole derivatives |
HR1125/92A HRP921128B1 (en) | 1991-10-30 | 1992-10-29 | Novel process for the preparation of 4-methyl-5(2-chloroethyl)-thiazole and analogues thereof |
IL103586A IL103586A (en) | 1991-10-30 | 1992-10-29 | Process for the preparation of 4-methyl-5- (2-chloroethyl)-thiazole and analogues thereof |
IS3937A IS1688B (en) | 1991-10-30 | 1992-10-29 | A novel process for the preparation of 4-methyl-5- (2-chloroethyl) thiazole and its analogues and novel intermediates in the preparation of the compounds |
DK92923097.7T DK0619815T3 (en) | 1991-10-30 | 1992-10-30 | Process for the preparation of 4-methyl-5- (2-chloroethyl) -thiazole and analogs thereof |
ES92923097T ES2100365T3 (en) | 1991-10-30 | 1992-10-30 | PROCEDURE TO PREPARE 4-METHYL-5- (2-CHLOROETHYL) -TIAZOL AND ITS ANALOGS. |
PL92303342A PL172013B1 (en) | 1991-10-30 | 1992-10-30 | Method of obtaining 4-methyl-5-(2-chloroalkyl)-thiazoles |
DE69219154T DE69219154T2 (en) | 1991-10-30 | 1992-10-30 | METHOD FOR PRODUCING 4-METHYL-5- (2-CHLORETHYL) THIAZOL AND ITS ANALOGS |
CA002121488A CA2121488A1 (en) | 1991-10-30 | 1992-10-30 | Novel process for the preparation of 4-methyl-5-(2-chloroethyl)-thiazole and analogues thereof |
HU9401262A HU217079B (en) | 1991-10-30 | 1992-10-30 | New process for producing 5-(2-chloroalkyl)-thiazole derivatives |
JP50829893A JP3190959B2 (en) | 1991-10-30 | 1992-10-30 | Novel process for producing 4-methyl-5- (2-chloroethyl) -thiazole and its homologues |
YU95292A YU95292A (en) | 1991-10-30 | 1992-10-30 | A NEW PROCEDURE FOR THE PREPARATION OF 4-METHYL-5 - (- 2-CHLORO-ETHYL) -THIAZOLE AND ITS ANALOGS |
EP92923097A EP0619815B1 (en) | 1991-10-30 | 1992-10-30 | Process for the preparation of 4-methyl-5-(2-chloroethyl)-thiazole and analogues thereof |
AT92923097T ATE151761T1 (en) | 1991-10-30 | 1992-10-30 | METHOD FOR PRODUCING 4-METHYL-5-(2-CHLORETHYL)-THIAZOLE AND ANALOGUES THEREOF |
PCT/HU1992/000042 WO1993009107A1 (en) | 1991-10-30 | 1992-10-30 | Novel process for the preparation of 4-methyl-5-(2-chloroethyl)-thiazole and analogues thereof |
SK501-94A SK279665B6 (en) | 1991-10-30 | 1992-10-30 | Process for the preparation of 4-methyl-5-(2-chloroalkyl)thiazole |
UA94005498A UA34443C2 (en) | 1991-10-30 | 1992-10-30 | Process for the preparation of the thiazole derivatives or acid addition salts thereof, 3-thiocyanato-5-chloro-2-alkanone and a process for its preparation |
RU94022467A RU2103264C1 (en) | 1991-10-30 | 1992-10-30 | Method for producing derivatives of thiazole or their acid additive salts, 5-chloro-3-thiocyanate-2-alkanone and method for its production |
EP92118606A EP0546306B1 (en) | 1991-10-30 | 1992-10-30 | 5-(2-Chloroalkyl)-4-methylthiazoles, their preparation and their use, and intermediates for their preparation |
AU29123/92A AU664868B2 (en) | 1991-10-30 | 1992-10-30 | Novel process for the preparation of 4-methyl-5-(2-chloroethyl)-thiazole and analogues thereof |
SI9200292A SI9200292B (en) | 1991-10-30 | 1992-10-30 | Novel process for the preparation of 4-methyl-5-(2-chloroethyl)-thiazole and analogues derivatives |
CZ941034A CZ283402B6 (en) | 1991-10-30 | 1992-10-30 | Process for preparing 4-methyl-5-(2-chloroalkyl)thiazole derivative and 4-thiocyanato-5-chloro-2-alkanone employed as intermediate during said process |
US08/232,207 US5648498A (en) | 1991-10-30 | 1992-10-30 | Process for the preparation of 4-methyl-5-(2-chloroethyl)-thiazole and analogues thereof |
KR1019940701422A KR100218131B1 (en) | 1991-10-30 | 1992-10-30 | Novel process for the preparation of 4-methyl-5-(2-chloroethyl)-thiazole and analogues thereof |
NO940004A NO304650B1 (en) | 1991-10-30 | 1994-04-28 | New Process for Preparation of 4-Methyl-5- (2-Chloroethyl) Thiazole and Analogs thereof |
FI941996A FI105476B (en) | 1991-10-30 | 1994-04-29 | New Process for Preparation of 4-Methyl-5- (2-chloroethyl) -thiazole and its Analogs |
US08/464,308 US5534644A (en) | 1991-10-30 | 1995-06-05 | Process for the preparation of 4-methyl-5-(2-chloroethyl)-thiazole and analogues thereof |
GR970401480T GR3023842T3 (en) | 1991-10-30 | 1997-06-19 | Novel process for the preparation of 4-methyl-5-(2-chloroethyl)-thiazole and analogues thereof. |
HK93397A HK93397A (en) | 1991-10-30 | 1997-06-26 | Process for the preparation of 4-methyl-5-(2-chloroethyl)-thiazole and analogues thereof |
LVP-98-68A LV12130B (en) | 1991-10-30 | 1998-04-16 | 5-(2-chloroalkyl)-4-methylthiazoles, their preparation and their use, and intermediates for their preparation |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
HU3402/91A HU215840B (en) | 1991-10-30 | 1991-10-30 | Process for producing 2-chlorothiazole derivatives |
Publications (3)
Publication Number | Publication Date |
---|---|
HU913402D0 HU913402D0 (en) | 1992-01-28 |
HUT62871A true HUT62871A (en) | 1993-06-28 |
HU215840B HU215840B (en) | 1999-04-28 |
Family
ID=10963903
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HU3402/91A HU215840B (en) | 1991-10-30 | 1991-10-30 | Process for producing 2-chlorothiazole derivatives |
Country Status (1)
Country | Link |
---|---|
HU (1) | HU215840B (en) |
-
1991
- 1991-10-30 HU HU3402/91A patent/HU215840B/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
HU215840B (en) | 1999-04-28 |
HU913402D0 (en) | 1992-01-28 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US3399192A (en) | 1-oxa-2-oxo 3, 8-diaza spiro (4, 5) decanes | |
NZ333379A (en) | Process of preparing a 3-phenyl-4-(methylsulphonyl)-phenyl-furan-2-one derivative which is useful as COX-2 inhibitor | |
SE0104346L (en) | Process for continuous quaternization of tertiary amines with an alkyl halide | |
GB1598278A (en) | 5-(4-(diarylmethyl)-1-piperazinylakyl) benzimidazole derivatives | |
HUT62871A (en) | Process for producing 2-chlorothiazole derivatives | |
HUT62856A (en) | Process for producing thiocyanatoketones | |
SU513624A3 (en) | Method for preparing 2-piperazinyl thiazole derivatives | |
Njoya et al. | Efficient synthesis of new 6-nitrobenzothiazoles using microwave irradiation | |
Mangeney et al. | Enantioselective synthesis of indoloquinolizidines | |
Khripach et al. | Highly stereoselective synthesis of 20-isosteroidal side chain by dehydration of (20R)-20-hydroxy-20-isoxazolinylsteroids | |
Mylari et al. | 2-Chloro-1, 1, 1-triethoxyethane and its use in a versatile synthesis of substituted, 2-chloromethyl heterocycles including benzothiazole and benzoxazole | |
US5614536A (en) | Substituted N-aminoalkylmethane sulfanilide as antispasmodica | |
KR940005570A (en) | Method for preparing pyrrolidinylacetamide derivative | |
US3631042A (en) | Quinazoline compounds | |
Tanaka et al. | N-Acyl-1-chloro-2, 2, 2-trifluoroethylamine as a 2, 2, 2-Trifluoroethylamine-Building Block. | |
ES2158896T3 (en) | NEW INTERMEDIATE COMPOUND FOR USE IN SYNTHESIS AND PROCEDURE TO PRODUCE AN AMINOPIPERAZINE DERIVATIVE. | |
BR9405498A (en) | Process for producing carboxylic acid derivatives | |
PT87480A (en) | PROCESS FOR THE PREPARATION OF HISTAMINE H2-ANTAGONISTS FROM NOVEL INTERMEDIATES | |
ES2154632T3 (en) | PROCEDURE FOR THE PRODUCTION OF DERIVATIVES OF AZACICLOALCANOS. | |
JPH0539276A (en) | Production of iminothiazoline derivative | |
Tanaka et al. | Studies on Bacimethrin, A New Antibiotic from B. Megatherium. II The Chemical Structure of Bacimethrin | |
JPH01299256A (en) | Preparation of alpha-substituted beta-hydroxycarboxylic acid ester | |
HU9401262D0 (en) | New process for producing 4-methyl-5-(2-chloroethyl)-thiazole derivatives | |
Turro et al. | Additions and Corrections-Photosensitized Cycloaddition of Haloethylenes and 1, 3-Dienes | |
Gordon | Additions and Corrections-Fused Organic Salts. III. Chemical Stability of Molten Tetra-n-alkylammonium Salts. Medium Effects on Thermal R4N+ X--Decomposition. RBr+ I-= RI+ Br-Equilibrium Constant in Fused Salt Medium |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
DGB9 | Succession in title of applicant |
Owner name: AKTIEBOLAGET ASTRA, SE |
|
HMM4 | Cancellation of final prot. due to non-payment of fee |