HUT47067A - Process for producing, purifying and stabilizing 2-/trifluoro-methyl/-phenol and 4-/trifluoro-methyl/-phenol
- Google Patents
Process for producing, purifying and stabilizing 2-/trifluoro-methyl/-phenol and 4-/trifluoro-methyl/-phenol
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Publication number
HUT47067A
HUT47067AHU315087AHU315087AHUT47067AHU T47067 AHUT47067 AHU T47067AHU 315087 AHU315087 AHU 315087AHU 315087 AHU315087 AHU 315087AHU T47067 AHUT47067 AHU T47067A
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Application filed by Budapesti VegyimuevekfiledCriticalBudapesti Vegyimuevek
Priority to HU315087ApriorityCriticalpatent/HU199099B/en
Publication of HUT47067ApublicationCriticalpatent/HUT47067A/en
Publication of HU199099BpublicationCriticalpatent/HU199099B/en
Organic Low-Molecular-Weight Compounds And Preparation Thereof
(AREA)
Abstract
2-(Tri-fluoro-methyl)-phenol and 4-(tri-fluoro-methyl)-phe nol respectively are prepd. by boiling a mixt. of either 2-(tri-fluoro-methyl)-chloro -benzene or 4-(tri-fluoro methyl)- chloro-benzene, benzyl-alcohol and of an alkali-hydroxide. A phenyl-benzyl ether intermediate is obtd. which is hydrogenated catalytically to the respective phenol. Water formed during boiling is removed by distillation. The product is purified by vacuum distillation at 50-150 deg.C in the presence of 0.001 pts. wt. silicone oil. A silicone oil additive is also used for products stabilisation.
HU315087A1987-07-101987-07-10Process for producing 2-/trifluoro-methyl/-phenol and 4-/trifluoro-methyl/-phenol
HU199099B
(en)
PROCESS FOR PREPARING 7-IMIDAZOLIDINYL ACIDS SUBSTITUTES 3-CHLORO-3-CEPHEM-4-CARBOXYLIC AND NEW PRODUCTS THUS OBTAINED, USED IN PARTICULAR AS ANTIBACTERIAL AGENTS
ALKYL 4-METHYL-3-FORMYL PENTENE ACID, THEIR PRODUCTION PROCESS, THEIR USE IN THE MANUFACTURE OF 4-METHYL-3-FORMYL-3-PENTENO ACID AND THE INTERMEDIATE PRODUCTS.