HUP9802542A2 - Process for the preparation of 4-bromo-1,1-difluorobut-1-ene and 2,4-dibromo-1,1,1-trifluorobutane - Google Patents
Process for the preparation of 4-bromo-1,1-difluorobut-1-ene and 2,4-dibromo-1,1,1-trifluorobutaneInfo
- Publication number
- HUP9802542A2 HUP9802542A2 HU9802542A HUP9802542A HUP9802542A2 HU P9802542 A2 HUP9802542 A2 HU P9802542A2 HU 9802542 A HU9802542 A HU 9802542A HU P9802542 A HUP9802542 A HU P9802542A HU P9802542 A2 HUP9802542 A2 HU P9802542A2
- Authority
- HU
- Hungary
- Prior art keywords
- trifluorobutane
- dibromo
- bromo
- difluorobut
- ene
- Prior art date
Links
- OTMJZYBDBAVGET-UHFFFAOYSA-N 2,4-dibromo-1,1,1-trifluorobutane Chemical compound FC(F)(F)C(Br)CCBr OTMJZYBDBAVGET-UHFFFAOYSA-N 0.000 title abstract 3
- WSIDFIREQDHYPW-UHFFFAOYSA-N 4-bromo-1,1-difluorobut-1-ene Chemical compound FC(F)=CCCBr WSIDFIREQDHYPW-UHFFFAOYSA-N 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 238000009835 boiling Methods 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 2
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 abstract 1
- AFVFQIVMOAPDHO-UHFFFAOYSA-M Methanesulfonate Chemical compound CS([O-])(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-M 0.000 abstract 1
- 229950002475 mesilate Drugs 0.000 abstract 1
- 239000012429 reaction media Substances 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/26—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfonic acids
- C07C303/28—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfonic acids by reaction of hydroxy compounds with sulfonic acids or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/23—Preparation of halogenated hydrocarbons by dehalogenation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
- C07C19/14—Acyclic saturated compounds containing halogen atoms containing fluorine and bromine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
- C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
- C07C29/143—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of ketones
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
- C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
- C07C29/147—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
A találmány tárgya eljárás 4-bróm-1,1-diflűőr-1-bűtén előállításáraőly módőn, hőgy 2,4-dibróm-1,1,1-triflűőr-bűtánt főlyékőnyreakcióközegben egy diflűőrbrómőzó szerrel kezelnek, majd a kívántterméket elkülönítik. A találmány tárgyát képezi a kiindűlási anyagként fehasznált 2,4-dibróm-1,1,1-triflűőr-bűtán előállítása is őly módőn, hőgy egy 1,1,1-triflűőr-bűtán-2,4-szűlfőnátőt (előnyösen mezilátőt vagy tőzilátőt)brőmidfőrrással reagáltatnak. ŕThe subject of the invention is a process for the production of 4-bromo-1,1-difluoro-1-butene, in which 2,4-dibromo-1,1,1-trifluorobutane is treated with a difluorobrominating agent in a boiling reaction medium, and then the desired product is isolated. The subject of the invention is also the production of 2,4-dibromo-1,1,1-trifluorobutane used as a starting material in the same way, i.e. a 1,1,1-trifluorobutane-2,4-sulfonate (preferably mesilate or ) are reacted with bromide boiling. ŕ
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GBGB9518111.1A GB9518111D0 (en) | 1995-09-06 | 1995-09-06 | Chemical process |
Publications (2)
Publication Number | Publication Date |
---|---|
HUP9802542A2 true HUP9802542A2 (en) | 1999-02-01 |
HUP9802542A3 HUP9802542A3 (en) | 1999-03-29 |
Family
ID=10780231
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HU9802542A HUP9802542A3 (en) | 1995-09-06 | 1996-08-23 | Process for the preparation of 4-bromo-1,1-difluorobut-1-ene and 2,4-dibromo-1,1,1-trifluorobutane |
Country Status (10)
Country | Link |
---|---|
EP (1) | EP0850211A1 (en) |
JP (1) | JPH11512110A (en) |
KR (1) | KR19990044419A (en) |
CN (1) | CN1200717A (en) |
AU (1) | AU6828896A (en) |
GB (1) | GB9518111D0 (en) |
HU (1) | HUP9802542A3 (en) |
IL (1) | IL123460A0 (en) |
WO (1) | WO1997009292A1 (en) |
ZA (1) | ZA967262B (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ATE537133T1 (en) * | 2006-11-01 | 2011-12-15 | Daikin Ind Ltd | METHOD FOR PRODUCING OLEFIN |
CN107652162A (en) * | 2017-11-29 | 2018-02-02 | 常州沃腾化工科技有限公司 | A kind of preparation method of cyclohexyl bromide methane |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB9219635D0 (en) * | 1992-09-16 | 1992-10-28 | Ici Plc | Heterocyclic compounds |
AU7193094A (en) * | 1993-08-05 | 1995-02-28 | Zeneca Limited | Process for the preparation of fluoroathenylthio heterocyclic derivatives |
-
1995
- 1995-09-06 GB GBGB9518111.1A patent/GB9518111D0/en active Pending
-
1996
- 1996-08-23 IL IL12346096A patent/IL123460A0/en unknown
- 1996-08-23 KR KR1019980701663A patent/KR19990044419A/en not_active Application Discontinuation
- 1996-08-23 EP EP96928560A patent/EP0850211A1/en not_active Withdrawn
- 1996-08-23 AU AU68288/96A patent/AU6828896A/en not_active Abandoned
- 1996-08-23 WO PCT/GB1996/002072 patent/WO1997009292A1/en not_active Application Discontinuation
- 1996-08-23 CN CN96197873A patent/CN1200717A/en active Pending
- 1996-08-23 HU HU9802542A patent/HUP9802542A3/en unknown
- 1996-08-23 JP JP9510925A patent/JPH11512110A/en active Pending
- 1996-08-27 ZA ZA967262A patent/ZA967262B/en unknown
Also Published As
Publication number | Publication date |
---|---|
AU6828896A (en) | 1997-03-27 |
GB9518111D0 (en) | 1995-11-08 |
ZA967262B (en) | 1997-03-06 |
CN1200717A (en) | 1998-12-02 |
KR19990044419A (en) | 1999-06-25 |
IL123460A0 (en) | 1998-09-24 |
EP0850211A1 (en) | 1998-07-01 |
JPH11512110A (en) | 1999-10-19 |
WO1997009292A1 (en) | 1997-03-13 |
HUP9802542A3 (en) | 1999-03-29 |
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