HUP0401666A2 - Method for producing arylsuphonic acid isocyanates - Google Patents
Method for producing arylsuphonic acid isocyanatesInfo
- Publication number
- HUP0401666A2 HUP0401666A2 HU0401666A HUP0401666A HUP0401666A2 HU P0401666 A2 HUP0401666 A2 HU P0401666A2 HU 0401666 A HU0401666 A HU 0401666A HU P0401666 A HUP0401666 A HU P0401666A HU P0401666 A2 HUP0401666 A2 HU P0401666A2
- Authority
- HU
- Hungary
- Prior art keywords
- phosgene
- arylsuphonic
- producing
- effective amount
- catalytically effective
- Prior art date
Links
- 239000002253 acid Substances 0.000 title abstract 2
- 239000012948 isocyanate Substances 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 150000002513 isocyanates Chemical class 0.000 title 1
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 abstract 3
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 125000004421 aryl sulphonamide group Chemical group 0.000 abstract 1
- -1 arylsulfonyl isocyanates Chemical class 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
- C07C303/40—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reactions not involving the formation of sulfonamide groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
A találmány tárgya eljárás arilszulfonil-izocianátok előállítására. Atalálmány szerint úgy járnak el, hogy egy arilszulfonamidot egykatalitikusan hatásos mennyiségű alkilizocianát jelenlétébenfoszgénnel reagáltatnak. A reakciót egy prótikus sav vagy sójakatalitikusan hatásos mennyiségének jelenlétében végzik és/vagy afoszgént úgy vezetik be, hogy a köztitermékként keletkező alkil-arilszulfonil-karbamid koncentrációja a reakciózónában a foszgénadagolási ideje alatt egy minimális érték alá ne csökkenjen. Atalálmány szerinti eljárás magas hozamot és terméktisztaságoteredményez. ÓThe subject of the invention is a process for preparing arylsulfonyl isocyanates. According to the invention, they proceed by reacting an arylsulfonamide with phosgene in the presence of a catalytically effective amount of alkylisocyanate. The reaction is carried out in the presence of a catalytically effective amount of a protic acid or salt and/or phosgene is introduced in such a way that the concentration of the intermediate alkyl arylsulfonylurea in the reaction zone does not fall below a minimum value during the phosgene dosing period. The process according to the invention results in a high yield and product purity. HE
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10150368A DE10150368A1 (en) | 2001-10-11 | 2001-10-11 | Process for the preparation of arylsulfonic acid isocyanates |
| DE10150368.7 | 2001-10-11 | ||
| PCT/EP2002/011379 WO2003033459A1 (en) | 2001-10-11 | 2002-10-10 | Method for producing arylsuphonic acid isocyanates |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| HUP0401666A2 true HUP0401666A2 (en) | 2004-12-28 |
| HU230232B1 HU230232B1 (en) | 2015-10-28 |
Family
ID=7702271
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| HU0401666A HU230232B1 (en) | 2001-10-11 | 2002-10-10 | Method for producing arylsuphonic acid isocyanates |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US6949672B2 (en) |
| EP (1) | EP1438286B1 (en) |
| JP (1) | JP3978181B2 (en) |
| KR (1) | KR100925573B1 (en) |
| CN (1) | CN1277814C (en) |
| AR (1) | AR036754A1 (en) |
| AT (1) | ATE466837T1 (en) |
| BR (1) | BR0213145A (en) |
| CA (1) | CA2462528C (en) |
| DE (2) | DE10150368A1 (en) |
| DK (1) | DK1438286T3 (en) |
| EA (1) | EA006399B1 (en) |
| ES (1) | ES2343680T3 (en) |
| HU (1) | HU230232B1 (en) |
| IL (2) | IL160999A0 (en) |
| MX (1) | MXPA04002761A (en) |
| PL (1) | PL207035B1 (en) |
| SI (1) | SI1438286T1 (en) |
| UA (1) | UA75471C2 (en) |
| WO (1) | WO2003033459A1 (en) |
| ZA (1) | ZA200403527B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102816043A (en) * | 2011-06-07 | 2012-12-12 | 安徽广信农化股份有限公司 | Production method for sulfonyl isocyanate |
| CN109824554B (en) * | 2017-11-23 | 2021-11-19 | 北京颖泰嘉和生物科技股份有限公司 | Process for preparing phenylsulfonyl isocyanates |
| CN108395383B (en) * | 2018-04-17 | 2020-10-16 | 湖南国发精细化工科技有限公司 | Synthesis method of tert-butyl isocyanate |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE790361A (en) | 1971-10-23 | 1973-04-20 | Bayer Ag | PROCESS FOR PREPARING ORGANIC SULFONYLISOCYANATES |
| DE2450083A1 (en) | 1974-10-22 | 1976-04-29 | Hoechst Ag | PROCESS FOR THE PRODUCTION OF AROMATIC SULFONYL ISOCYANATES |
| BR8003393A (en) | 1979-06-04 | 1980-12-30 | Du Pont | PROCESS TO PREPARE AN ARYLSULPHONYL ISOCIANATE |
| US4379769A (en) | 1979-06-04 | 1983-04-12 | E. I. Du Pont De Nemours And Company | Process for preparing arylsulfonyl isocyanates by phosgenation of arylsulfonamides |
| JP3810081B2 (en) * | 1994-08-29 | 2006-08-16 | イー・アイ・デユポン・ドウ・ヌムール・アンド・カンパニー | Improved process for the preparation of sulfonyl isocyanates |
| JP3742995B2 (en) * | 1995-06-09 | 2006-02-08 | 日本曹達株式会社 | Process for producing aromatic sulfonyl isocyanate |
-
2001
- 2001-10-11 DE DE10150368A patent/DE10150368A1/en not_active Withdrawn
-
2002
- 2002-10-07 AR ARP020103775A patent/AR036754A1/en active IP Right Grant
- 2002-10-10 DE DE50214417T patent/DE50214417D1/en not_active Expired - Lifetime
- 2002-10-10 CA CA2462528A patent/CA2462528C/en not_active Expired - Fee Related
- 2002-10-10 DK DK02801325.8T patent/DK1438286T3/en active
- 2002-10-10 WO PCT/EP2002/011379 patent/WO2003033459A1/en active Application Filing
- 2002-10-10 EA EA200400484A patent/EA006399B1/en not_active IP Right Cessation
- 2002-10-10 BR BR0213145-5A patent/BR0213145A/en not_active IP Right Cessation
- 2002-10-10 JP JP2003536200A patent/JP3978181B2/en not_active Expired - Fee Related
- 2002-10-10 UA UA20040503461A patent/UA75471C2/en unknown
- 2002-10-10 CN CNB028199065A patent/CN1277814C/en not_active Expired - Lifetime
- 2002-10-10 MX MXPA04002761A patent/MXPA04002761A/en active IP Right Grant
- 2002-10-10 IL IL16099902A patent/IL160999A0/en unknown
- 2002-10-10 KR KR1020047005229A patent/KR100925573B1/en active IP Right Grant
- 2002-10-10 SI SI200230910T patent/SI1438286T1/en unknown
- 2002-10-10 US US10/491,420 patent/US6949672B2/en not_active Expired - Lifetime
- 2002-10-10 EP EP02801325A patent/EP1438286B1/en not_active Expired - Lifetime
- 2002-10-10 PL PL368983A patent/PL207035B1/en unknown
- 2002-10-10 AT AT02801325T patent/ATE466837T1/en active
- 2002-10-10 ES ES02801325T patent/ES2343680T3/en not_active Expired - Lifetime
- 2002-10-10 HU HU0401666A patent/HU230232B1/en not_active IP Right Cessation
-
2004
- 2004-03-22 IL IL160999A patent/IL160999A/en active IP Right Grant
- 2004-05-10 ZA ZA200403527A patent/ZA200403527B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| HU230232B1 (en) | 2015-10-28 |
| IL160999A (en) | 2009-09-01 |
| PL368983A1 (en) | 2005-04-04 |
| JP2005505619A (en) | 2005-02-24 |
| US6949672B2 (en) | 2005-09-27 |
| UA75471C2 (en) | 2006-04-17 |
| EP1438286B1 (en) | 2010-05-05 |
| BR0213145A (en) | 2004-10-19 |
| KR20050035136A (en) | 2005-04-15 |
| IL160999A0 (en) | 2004-08-31 |
| SI1438286T1 (en) | 2010-08-31 |
| CN1277814C (en) | 2006-10-04 |
| KR100925573B1 (en) | 2009-11-06 |
| DE10150368A1 (en) | 2003-05-22 |
| JP3978181B2 (en) | 2007-09-19 |
| CN1564810A (en) | 2005-01-12 |
| ZA200403527B (en) | 2005-05-10 |
| CA2462528C (en) | 2010-09-28 |
| WO2003033459A1 (en) | 2003-04-24 |
| EA200400484A1 (en) | 2004-08-26 |
| PL207035B1 (en) | 2010-10-29 |
| EA006399B1 (en) | 2005-12-29 |
| MXPA04002761A (en) | 2004-06-29 |
| ATE466837T1 (en) | 2010-05-15 |
| AR036754A1 (en) | 2004-09-29 |
| ES2343680T3 (en) | 2010-08-06 |
| US20040199011A1 (en) | 2004-10-07 |
| EP1438286A1 (en) | 2004-07-21 |
| CA2462528A1 (en) | 2003-04-24 |
| DK1438286T3 (en) | 2010-08-16 |
| DE50214417D1 (en) | 2010-06-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | Lapse of definitive patent protection due to non-payment of fees |