GB947396A - Process for the production of cyclododecadiene-mononitrosochlorides - Google Patents
Process for the production of cyclododecadiene-mononitrosochloridesInfo
- Publication number
- GB947396A GB947396A GB19259/60A GB1925960A GB947396A GB 947396 A GB947396 A GB 947396A GB 19259/60 A GB19259/60 A GB 19259/60A GB 1925960 A GB1925960 A GB 1925960A GB 947396 A GB947396 A GB 947396A
- Authority
- GB
- United Kingdom
- Prior art keywords
- trans
- nitroso
- solution
- cyclododecadiene
- cyclododeca
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- MNIXHKDMEYKNBQ-UHFFFAOYSA-N N(=O)Cl.C1=CC=CCCCCCCCC1 Chemical class N(=O)Cl.C1=CC=CCCCCCCCC1 MNIXHKDMEYKNBQ-UHFFFAOYSA-N 0.000 title abstract 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 4
- VPCDQGACGWYTMC-UHFFFAOYSA-N nitrosyl chloride Chemical compound ClN=O VPCDQGACGWYTMC-UHFFFAOYSA-N 0.000 abstract 4
- 239000004157 Nitrosyl chloride Substances 0.000 abstract 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 abstract 3
- 235000019392 nitrosyl chloride Nutrition 0.000 abstract 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- 229960000583 acetic acid Drugs 0.000 abstract 2
- 239000012362 glacial acetic acid Substances 0.000 abstract 2
- RZUNIXAGSKNOIB-HSFFGMMNSA-N (1z,3e)-cyclododeca-1,3-diene Chemical compound C1CCCC\C=C/C=C/CCC1 RZUNIXAGSKNOIB-HSFFGMMNSA-N 0.000 abstract 1
- ZOLLIQAKMYWTBR-UDIJVJLMSA-N (1z,5e,9z)-cyclododeca-1,5,9-triene Chemical compound C/1C\C=C/CC\C=C/CC\C=C\1 ZOLLIQAKMYWTBR-UDIJVJLMSA-N 0.000 abstract 1
- ZOLLIQAKMYWTBR-UHFOHBBQSA-N (5e)-cyclododeca-1,5,9-triene Chemical compound C1CC=CCC\C=C\CCC=C1 ZOLLIQAKMYWTBR-UHFOHBBQSA-N 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 125000001309 chloro group Chemical group Cl* 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- ZOLLIQAKMYWTBR-UHFFFAOYSA-N cyclododeca-1,5,9-triene Chemical compound C1CC=CCCC=CCCC=C1 ZOLLIQAKMYWTBR-UHFFFAOYSA-N 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
- SCRFXJBEIINMIC-UHFFFAOYSA-N n-cyclododecylidenehydroxylamine Chemical compound ON=C1CCCCCCCCCCC1 SCRFXJBEIINMIC-UHFFFAOYSA-N 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B25/00—Compositions containing a nitrated organic compound
- C06B25/34—Compositions containing a nitrated organic compound the compound being a nitrated acyclic, alicyclic or heterocyclic amine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
A mono - nitroso - chloride of cyclododecadiene is produced by the action of nitrosyl chloride on a solution of cyclododeca- 1, 5, 9-triene. The nitrosyl chloride may be reacted in the form of vapour, or as a solution in a solvent. In example 1, a solution of trans, trans, ciscyclododeca-1, 5, 9-triene in glacial acetic acid is mixed with a solution of nitrosyl chloride in glacial acetic acid. Crystals of 1- nitroso-2-chloro-cyclododeca-trans-cis 5, 9-diene are formed; these are filtered off, dried, and recrystallized from ethanol or hexane. Example 2 describes the preparation of 1-nitroso-chlorocyclododeca - trans - trans - 5, 9 - diene from all trans - cyclododeca - 1, 5, 9-triene. The Specification states that cyclododecanone oxime may be prepared from the cyclododecadiene - mono - nitroso - chlorides by hydrogenation of the two double bonds and removal of the chlorine atom. Specifications 848,951, 849,236 and 867,016 are referred to.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEST15225A DE1094741B (en) | 1959-06-11 | 1959-06-11 | Process for the preparation of cyclododecadiene mononitrosochlorides |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB947396A true GB947396A (en) | 1964-01-22 |
Family
ID=7456609
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB19259/60A Expired GB947396A (en) | 1959-06-11 | 1960-05-31 | Process for the production of cyclododecadiene-mononitrosochlorides |
Country Status (2)
| Country | Link |
|---|---|
| DE (1) | DE1094741B (en) |
| GB (1) | GB947396A (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1196649B (en) * | 1962-12-05 | 1965-07-15 | Organico Sa | Process for the preparation of 1-oximino-2-chlorocyclododecadiene-5, 9 |
-
1959
- 1959-06-11 DE DEST15225A patent/DE1094741B/en active Pending
-
1960
- 1960-05-31 GB GB19259/60A patent/GB947396A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE1094741B (en) | 1960-12-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CH432851A (en) | Process for the preparation of cis-1,4-polybutadiene | |
| GB947396A (en) | Process for the production of cyclododecadiene-mononitrosochlorides | |
| CH383977A (en) | Process for the production of new azepine derivatives | |
| CA581615A (en) | Process for the manufacture of organic acid chlorides | |
| CH438737A (en) | Process for the production of stable, aqueous polymer dispersions | |
| CA611121A (en) | Process for the electrolytic production of tantalum and resultant product | |
| CH410967A (en) | Process for the production of new reserp acid derivatives | |
| CA628865A (en) | Process for the production of aromatic carboxylic acid amides | |
| CH430717A (en) | Process for the preparation of new (3,2-b) thiazole derivatives of androstane compounds | |
| AT220332B (en) | Process for the production of frames and frames produced by the process | |
| CH392503A (en) | Process for the production of new corticohormone derivatives | |
| AU253456B2 (en) | Process of preparing cyclohexanone from cyclohexanol | |
| CA614395A (en) | Process for the production of terephthalic acid | |
| CA528897A (en) | Process of continuously sulfonating organic products by the use of sulfuric chloridrine | |
| CA521926A (en) | Process for the production of oximes | |
| CA570037A (en) | Process for the production of butane-1,2,4-tricarboxylic acid | |
| AU214537B2 (en) | Process for production of 5-nitro-2-furaldehyde semicarbazone | |
| AT225930B (en) | Process for the production of crystalline 1,3-butadiene polymers | |
| AT195934B (en) | Process for the production of the new p, p'-bis- [2,4-dimethyl-pyrimidyl- (5) -aminosulfonyl] -azobenzene and the 5-sulfanilamido-2,4-dimethyl-pyrimidine obtainable therefrom by reduction | |
| CH383366A (en) | Process for the production of new 18,21-cycloacetals of the pregnane series | |
| AU454561A (en) | Process of preparing cyclohexanone from cyclohexanol | |
| AU245991B2 (en) | Process forthe manufacture of cyclohexanol and cyclohexanone by oxidation of cyclohexane | |
| CA588865A (en) | Process for the production of organic hydroxylamine compounds | |
| CH388938A (en) | Process for the production of cyclododecanone | |
| AU235594B2 (en) | 3 hydroxybutyric acid cyclohexylamide anda process for preparing it |