GB906409A - Improvements in or relating to quaternary ammonium compounds - Google Patents

Improvements in or relating to quaternary ammonium compounds

Info

Publication number
GB906409A
GB906409A GB11132/59A GB1113259A GB906409A GB 906409 A GB906409 A GB 906409A GB 11132/59 A GB11132/59 A GB 11132/59A GB 1113259 A GB1113259 A GB 1113259A GB 906409 A GB906409 A GB 906409A
Authority
GB
United Kingdom
Prior art keywords
fragment
cellulose
trimethyloctadecyl
exchanger
quaternary ammonium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB11132/59A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Armour and Co
Original Assignee
Armour and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Armour and Co filed Critical Armour and Co
Publication of GB906409A publication Critical patent/GB906409A/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Investigating Or Analysing Biological Materials (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)

Abstract

Quaternary ammonium compounds are prepared, purified or assayed by fixing the cationic fragment on a cellulose cationic exchanger by contacting a solution with the exchanger, and eluting the fixed fragment from the ion exchanger with a solvent containing not more than 50% v/v of water, with an acid pH, and containing an anionic fragment of an ionisable compound. The quaternary ammonium compound may be saturated or unsaturated and may contain an aromatic group. Specified compounds are trimethyl "coco", dimethyldi "tallow", trimethyl "soya", trimethyloctadecyl, dimethyldioctadecyl, trimethyldodecyl, tris-2-hydroxyethyloctadecyl, ammonium chlorides, trimethyloctadecyl ammonium stearate, laurate, citrate and pelargonate, trimethylhexadecyl ammonium laurate and palmitate and the cationic fragment may also be derived from alkylamines, dialkylamines, dimethylalkylamines, bis (2-hydroxyethyl) alkylamines, N - alkyl - 1,3 - propanediamines, N-dodecyltrimethylenediamine and 1-alkyl pyridinium halides. The cation-exchanger has a cellulose base and preferred types are oxidised cellulose, carboxymethyl cellulose, cellulose phosphate and citrate and they may be contacted with the cationic fragment by a batch or column procedure. The solvent may be inorganic or organic and lists are given and the anionic fragment may be derived from lower fatty acids, polysulphonic, sulphuric, carboxylic, saccharinic phosphoric acids, non-polymeric polysulphonic acids, polyphosphoric esters and polysilicates. The process can be employed to purify quaternary ammonium compounds e.g. trimethyloctadecyl and tris-2-hydroxyethyloctadecylammonium chlorides, and assay the quantity e.g. of trimethyloctadecyl ammonium stearate, in animal feed, the eluate being estimated by titration or colorimetry.
GB11132/59A 1958-04-01 1959-04-01 Improvements in or relating to quaternary ammonium compounds Expired GB906409A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US725488A US3024283A (en) 1958-04-01 1958-04-01 Production of quaternary ammonium compounds

Publications (1)

Publication Number Publication Date
GB906409A true GB906409A (en) 1962-09-19

Family

ID=24914765

Family Applications (1)

Application Number Title Priority Date Filing Date
GB11132/59A Expired GB906409A (en) 1958-04-01 1959-04-01 Improvements in or relating to quaternary ammonium compounds

Country Status (2)

Country Link
US (1) US3024283A (en)
GB (1) GB906409A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3522296A (en) * 1966-04-26 1970-07-28 Kuhlmann Sa Ets Method for producing choline salts of organic acids from choline chloride
EP0149172A1 (en) * 1983-12-29 1985-07-24 Hoechst Aktiengesellschaft Fluorinated quaternary ammonium compounds, processes for their preparation and their use as drag reducing agents

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3295933A (en) * 1961-03-06 1967-01-03 Pennsalt Chemicals Corp Perchloramide compounds and process
US3314810A (en) * 1963-06-19 1967-04-18 Staley Mfg Co A E Amylosic material plasticized with quaternary ammonium salt
US3981937A (en) * 1966-06-03 1976-09-21 E. I. Du Pont De Nemours And Company Dehydrohalogenation of 3,4-dichloro-1-butene
US3867338A (en) * 1972-06-09 1975-02-18 Celanese Corp Thermal stabilization of polymers
US4140719A (en) * 1977-10-31 1979-02-20 Merck & Co., Inc. Solid-liquid phase transfer catalysis improved method of preparing 2,4-difluoroaniline
DE2964935D1 (en) * 1978-02-21 1983-04-07 Sumitomo Chemical Co A hydroxy-urea, process for producing the same and a process for producing a phenyl-substituted n-methoxy-n-methyl-urea
JPS58180463A (en) * 1982-04-19 1983-10-21 Toyama Chem Co Ltd Preparation of bischolinedisulfonate
US6376436B1 (en) 2000-03-22 2002-04-23 The United States Of America As Represented By The Secretary Of The Navy Chemical warfare agent decontamination foaming composition and method
AR051007A1 (en) * 2004-08-13 2006-12-13 Basf Ag PROCEDURE FOR THE PREPARATION OF ENVIRONMENTAL PRESSURE AMMONIUM COMPOUND COMPOUNDS
EP3160698A1 (en) * 2014-06-30 2017-05-03 Dow Global Technologies LLC Treated porous material
CN115181230B (en) * 2022-08-19 2023-10-31 盛鼎高新材料有限公司 Preparation method of segmented polyurethane elastomer
WO2024094669A1 (en) * 2022-11-03 2024-05-10 Blaser Swisslube Ag Production process for quaternary ammonium-carboxylate compounds and resultant additive for cooling lubricant emulsions

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE16721C (en) * L. GERECHTER in Berlin C, Georgenkirchplatz 11 Spring universal joint for the pedal mechanism on work machines
US2230641A (en) * 1938-06-09 1941-02-04 Us Rubber Co Ion exchange process
US2557109A (en) * 1948-11-13 1951-06-19 Du Pont Preparation of polymetaphosphate solutions
GB695968A (en) * 1950-09-15 1953-08-19 Ici Ltd Improvements in and relating to the production of organic quaternary ammonium hydroxides
US2806019A (en) * 1954-02-15 1957-09-10 Rohm & Haas Quaternary ammonium compounds of polymers of the cumarone-indene class
US2880239A (en) * 1955-02-23 1959-03-31 Ici Ltd New chemical compounds

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3522296A (en) * 1966-04-26 1970-07-28 Kuhlmann Sa Ets Method for producing choline salts of organic acids from choline chloride
EP0149172A1 (en) * 1983-12-29 1985-07-24 Hoechst Aktiengesellschaft Fluorinated quaternary ammonium compounds, processes for their preparation and their use as drag reducing agents

Also Published As

Publication number Publication date
US3024283A (en) 1962-03-06

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