GB865073A - Apparatus for simultaneously carrying out thermogravimetric, differential-thermal and derivative-thermogravimetric analysis - Google Patents
Apparatus for simultaneously carrying out thermogravimetric, differential-thermal and derivative-thermogravimetric analysisInfo
- Publication number
- GB865073A GB865073A GB3006457A GB3006457A GB865073A GB 865073 A GB865073 A GB 865073A GB 3006457 A GB3006457 A GB 3006457A GB 3006457 A GB3006457 A GB 3006457A GB 865073 A GB865073 A GB 865073A
- Authority
- GB
- United Kingdom
- Prior art keywords
- balance
- temperature
- crucible
- attached
- differential
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/14—Investigating or analyzing materials by the use of thermal means by using distillation, extraction, sublimation, condensation, freezing, or crystallisation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01G—WEIGHING
- G01G7/00—Weighing apparatus wherein the balancing is effected by magnetic, electromagnetic, or electrostatic action, or by means not provided for in the preceding groups
- G01G7/02—Weighing apparatus wherein the balancing is effected by magnetic, electromagnetic, or electrostatic action, or by means not provided for in the preceding groups by electromagnetic action
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/02—Investigating or analyzing materials by the use of thermal means by investigating changes of state or changes of phase; by investigating sintering
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N5/00—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
- G01N5/04—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by removing a component, e.g. by evaporation, and weighing the remainder
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Electromagnetism (AREA)
- Investigating Or Analyzing Materials Using Thermal Means (AREA)
- Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
Abstract
<PICT:0865073/III/1> <PICT:0865073/III/2> <PICT:0865073/III/3> Apparatus for analysing mixtures by the thermogravimetric, differential thermogravimetric and differential thermal methods comprises two crucibles in a furnace, one containing the test material and attached by an electrically-insulating carrier to one arm of a balance and the other fixed and containing an inert reference material, two thermoelements to register the instantaneous temperatures of the contents of the two crucibles respectively, and means for measuring the rate of movement of the balance arm. In Fig. 1 the sample is placed in a crucible 5 arranged in a furnace 1 together with the reference material 16. Each crucible contains a thermocouple to measure the temperature of the contents either directly or through the walls of the crucible. The instrument 8 reads the difference between the thermocouple voltages and the instrument 6 can be joined by links to a or d to measure the individual temperature of either crucible. By plotting the difference between the temperatures against the reference temperature a "differential thermmal analysis" (DTA) curve can be obtained. The crucible 5 is attached to the left-hand side of the beam of the balance by a steel hoop 10 and variations of weight can thus be determined. The thermocouple leads 4 are preferably brought out not as shown but via torsion-free coils, one pair in the plane of the stirrup knife-edge of the balance and one pair in the plane of the balance beam (Figs. 5 and 6, not shown), to avoid drag on the beam. If a torsion balance is used the torsion filaments themselves can be used as current leads. Attached to the right-hand side of the beam is a permanent magnet or electromagnet 13 which moves in a coil and induces an E.M.F. in it proportional to the rate of movement and hence representative of the rate of loss of weight of the sample. By plotting the readings of the meter 14 against temperature a "differential thermogravimetric analysis" (DTG) curve can be obtained. The positions of magnet and coil can be interchanged (Fig. 7-10, not shown). In an alternative arrangement (Figs. 11-13, not shown) a shutter having a wedge-shaped pointer is attached to the balance pointer 41 and varies the light passing from a lamp to a photo-cell. The output of the photo-cell is differentiated by a transformer or a CR network to give the required output. The curves can be obtained automatically as follows (Figs. 16 and 19):-the TG curve is produced on continuously-moving photographic paper 49 by focusing the image of a slit in a plate 48 attached to the balance beam or pointer. The DTA and DTG curves are obtained similarly from mirrors on the galvanometer 8 and 14 respectively. A "temperature" (T) curve is obtained from the galvanometer 6. The vertical calibration lines h are produced from lamps 55, 56 shining through slits in screens 53, 54 in front of the casing of the paper. Four further lamps 57 light up periodically by means of a clockwork switch to give the time markers i and from these are drawn the horizontal calibration lines j which facilitate the reading of the chart in terms of temperature instead of time. A direct recording in terms of temperature can be made if the drum is driven by a motor energized from the amplified output of the thermoelement.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1644261A GB924406A (en) | 1961-05-05 | 1961-05-05 | Apparatus for the themogravimetric determination of the distillation curve for liquids |
Publications (1)
Publication Number | Publication Date |
---|---|
GB865073A true GB865073A (en) | 1961-04-12 |
Family
ID=10077406
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB3006457A Expired GB865073A (en) | 1961-05-05 | 1957-09-25 | Apparatus for simultaneously carrying out thermogravimetric, differential-thermal and derivative-thermogravimetric analysis |
GB1644261A Expired GB924406A (en) | 1961-05-05 | 1961-05-05 | Apparatus for the themogravimetric determination of the distillation curve for liquids |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1644261A Expired GB924406A (en) | 1961-05-05 | 1961-05-05 | Apparatus for the themogravimetric determination of the distillation curve for liquids |
Country Status (3)
Country | Link |
---|---|
DE (2) | DE1178235B (en) |
FR (1) | FR1187070A (en) |
GB (2) | GB865073A (en) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1498822B1 (en) * | 1964-02-21 | 1971-05-06 | Inst Metallurg Im A A Baikowa | Measuring insert for the furnace of a device for differential thermal analysis |
US5484204A (en) * | 1994-09-21 | 1996-01-16 | Ta Instruments, Inc. | Mechanical cooling system |
RU2531064C2 (en) * | 2012-12-05 | 2014-10-20 | Федеральное государственное автономное образовательное учреждение высшего профессионального образования "Уральский федеральный университет имени первого Президента России Б.Н. Ельцина" | Method and apparatus for investigating parameters of molten mass |
CN111721657A (en) * | 2019-03-22 | 2020-09-29 | 北京恒久实验设备有限公司 | Array type magnetic core arrangement structure of analytical instrument |
CN113533114A (en) * | 2021-07-16 | 2021-10-22 | 北京工业大学 | Enameled wire pyrolysis method based on pyrolysis principle |
CN114814072A (en) * | 2022-05-05 | 2022-07-29 | 中冶赛迪工程技术股份有限公司 | System and method for direct reduction and comprehensive thermal analysis and determination of powdery iron ore and application of system and method |
CN115824874A (en) * | 2022-09-26 | 2023-03-21 | 南京航空航天大学 | Direct light-heat gravimetric high-precision analyzer and working method thereof |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3135107A (en) * | 1957-09-25 | 1964-06-02 | Paulik Ferenc | Apparatus for the determination of the evaporation curve for liquids by the thermogravimetric method |
DE102013102088B3 (en) * | 2013-03-04 | 2014-07-17 | Netzsch-Gerätebau GmbH | Method and device for material analysis |
-
1957
- 1957-09-25 GB GB3006457A patent/GB865073A/en not_active Expired
- 1957-09-28 DE DE1957P0019392 patent/DE1178235B/en active Pending
- 1957-10-02 FR FR1187070D patent/FR1187070A/en not_active Expired
-
1961
- 1961-05-03 DE DE1961P0027092 patent/DE1289999B/en active Pending
- 1961-05-05 GB GB1644261A patent/GB924406A/en not_active Expired
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1498822B1 (en) * | 1964-02-21 | 1971-05-06 | Inst Metallurg Im A A Baikowa | Measuring insert for the furnace of a device for differential thermal analysis |
US5484204A (en) * | 1994-09-21 | 1996-01-16 | Ta Instruments, Inc. | Mechanical cooling system |
RU2531064C2 (en) * | 2012-12-05 | 2014-10-20 | Федеральное государственное автономное образовательное учреждение высшего профессионального образования "Уральский федеральный университет имени первого Президента России Б.Н. Ельцина" | Method and apparatus for investigating parameters of molten mass |
CN111721657A (en) * | 2019-03-22 | 2020-09-29 | 北京恒久实验设备有限公司 | Array type magnetic core arrangement structure of analytical instrument |
CN113533114A (en) * | 2021-07-16 | 2021-10-22 | 北京工业大学 | Enameled wire pyrolysis method based on pyrolysis principle |
CN113533114B (en) * | 2021-07-16 | 2023-12-08 | 北京工业大学 | Enameled wire pyrolysis method based on pyrolysis principle |
CN114814072A (en) * | 2022-05-05 | 2022-07-29 | 中冶赛迪工程技术股份有限公司 | System and method for direct reduction and comprehensive thermal analysis and determination of powdery iron ore and application of system and method |
CN115824874A (en) * | 2022-09-26 | 2023-03-21 | 南京航空航天大学 | Direct light-heat gravimetric high-precision analyzer and working method thereof |
CN115824874B (en) * | 2022-09-26 | 2023-09-29 | 南京航空航天大学 | Direct photothermal heavy high-precision analyzer and working method thereof |
Also Published As
Publication number | Publication date |
---|---|
DE1178235B (en) | 1964-09-17 |
DE1289999B (en) | 1969-02-27 |
GB924406A (en) | 1963-04-24 |
FR1187070A (en) | 1959-09-07 |
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