GB845206A - Mixing apparatus - Google Patents
Mixing apparatusInfo
- Publication number
- GB845206A GB845206A GB9435/57A GB943557A GB845206A GB 845206 A GB845206 A GB 845206A GB 9435/57 A GB9435/57 A GB 9435/57A GB 943557 A GB943557 A GB 943557A GB 845206 A GB845206 A GB 845206A
- Authority
- GB
- United Kingdom
- Prior art keywords
- zone
- mixing
- reservoir
- fed
- ingredients
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000004615 ingredient Substances 0.000 abstract 7
- 239000005056 polyisocyanate Substances 0.000 abstract 7
- 229920001228 polyisocyanate Polymers 0.000 abstract 7
- 239000000463 material Substances 0.000 abstract 6
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 abstract 5
- 239000012190 activator Substances 0.000 abstract 4
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 abstract 4
- 230000004888 barrier function Effects 0.000 abstract 4
- 239000000203 mixture Substances 0.000 abstract 4
- 239000004814 polyurethane Substances 0.000 abstract 4
- 229920002635 polyurethane Polymers 0.000 abstract 4
- 239000000376 reactant Substances 0.000 abstract 4
- 229920000728 polyester Polymers 0.000 abstract 3
- RFFLAFLAYFXFSW-UHFFFAOYSA-N 1,2-dichlorobenzene Chemical compound ClC1=CC=CC=C1Cl RFFLAFLAYFXFSW-UHFFFAOYSA-N 0.000 abstract 2
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- 239000001361 adipic acid Substances 0.000 abstract 2
- 235000011037 adipic acid Nutrition 0.000 abstract 2
- 239000000110 cooling liquid Substances 0.000 abstract 2
- 239000012043 crude product Substances 0.000 abstract 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 2
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 abstract 2
- 229920001451 polypropylene glycol Polymers 0.000 abstract 2
- 239000000047 product Substances 0.000 abstract 2
- KZNICNPSHKQLFF-UHFFFAOYSA-N succinimide Chemical compound O=C1CCC(=O)N1 KZNICNPSHKQLFF-UHFFFAOYSA-N 0.000 abstract 2
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 abstract 1
- YPFZMPJXTBJRCP-UHFFFAOYSA-N 6-[2-(diethylamino)ethoxy]-6-oxohexanoic acid Chemical compound CCN(CC)CCOC(=O)CCCCC(O)=O YPFZMPJXTBJRCP-UHFFFAOYSA-N 0.000 abstract 1
- SVYKKECYCPFKGB-UHFFFAOYSA-N N,N-dimethylcyclohexylamine Chemical compound CN(C)C1CCCCC1 SVYKKECYCPFKGB-UHFFFAOYSA-N 0.000 abstract 1
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 abstract 1
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 abstract 1
- 230000004913 activation Effects 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000007859 condensation product Substances 0.000 abstract 1
- HPNMFZURTQLUMO-UHFFFAOYSA-N diethylamine Chemical compound CCNCC HPNMFZURTQLUMO-UHFFFAOYSA-N 0.000 abstract 1
- 125000005442 diisocyanate group Chemical group 0.000 abstract 1
- 239000003995 emulsifying agent Substances 0.000 abstract 1
- 239000012948 isocyanate Substances 0.000 abstract 1
- 150000002513 isocyanates Chemical class 0.000 abstract 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 abstract 1
- QYDYPVFESGNLHU-KHPPLWFESA-N methyl oleate Chemical class CCCCCCCC\C=C/CCCCCCCC(=O)OC QYDYPVFESGNLHU-KHPPLWFESA-N 0.000 abstract 1
- 229940049964 oleate Drugs 0.000 abstract 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 abstract 1
- 239000010452 phosphate Substances 0.000 abstract 1
- 229920000768 polyamine Polymers 0.000 abstract 1
- 229920001296 polysiloxane Polymers 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- 229960002317 succinimide Drugs 0.000 abstract 1
- 150000003512 tertiary amines Chemical class 0.000 abstract 1
- 125000005628 tolylene group Chemical group 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
- B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
- B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
- B29B7/40—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with single shaft
- B29B7/401—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with single shaft having a casing closely surrounding the rotor, e.g. with a plunger for feeding the material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
- B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
- B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
- B29B7/40—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with single shaft
- B29B7/405—Mixing heads
- B29B7/407—Mixing heads with a casing closely surrounding the rotor, e.g. with conical rotor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
- B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
- B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
- B29B7/40—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with single shaft
- B29B7/44—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with single shaft with paddles or arms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/80—Component parts, details or accessories; Auxiliary operations
- B29B7/88—Adding charges, i.e. additives
- B29B7/94—Liquid charges
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/80—Component parts, details or accessories; Auxiliary operations
- B29B7/82—Heating or cooling
- B29B7/826—Apparatus therefor
Abstract
<PICT:0845206/IV(a)/1> A mixing apparatus comprises a reservoir zone into which some or all of the ingredients to be mixed are fed, and a mixing zone, said reservoir zone being separated from said mixing zone by a weir-like barrier over which the ingredients flow from the reservoir zone to the mixing zone, and said mixing zone being provided with inlet ports for any ingredients not fed into the reservoir zone and with mixing means and an exit port below the level of the weir-like barrier. The apparatus is useful in the p production of foamed or homogeneous polyurethanes. Polyester or other hydroxyl-containing polyurethane-forming material and polyisocyanate are fed separately into ports D and E and activator mixture is fed into F. Stirrer G mixes the reactants and the product is discharged through I, the rate of flow of reactants being such that there is no build up of material in mixing zone C tending to flow back over weir B. Then may also be an auxiliary stirrer H in the reservoir zone A. At the end of a run the flow of activator and polyisocyanate components is stopped first and the reservoir which is then filled with polyhydroxylic material alone prevents ingress of moisture to the polyisocyanate supply. The mixing head may have an outer jacket for the circulation of cooling liquid. Examples described the preparation of foamed polyurethanes in such an apparatus from starting materials selected from diethylene glycol/pentaerythritol/adipic acid or pentaerythritol/12:3-butylene glycol/adipic acid polyesters, a polyoxypropylene glycol and a prepolymer from polyoxypropylene glycol and trimethylol propane and tollylene diisocyanates. Tolylene 2:4 and 2:6- diisocyanates and the crude product obtained by phosgenating a formaldehydeaniline condensation product (see Group IV (b)) are the specified polyisocyanates. Tertiary amines, emulsifying agents such as sulphonated or sulphatedoils, silicones, flame-proofing agents (e.g., tri-b -chlorethyl phosphate) are other specified ingredients. Activation mixtures may contain dimethylcyclohexylamine, alkylphenolethylene oxide condensates, diethylaminoethyl adipate, diethylamine oleate, sulphated methyl oleate, N:N-diethylaminopropionamide or N:N-diethylaminopropyl succinimide. Specification 839,183 is referred to.ALSO:A diphenylmethane diisocyanate. for use in preparing polyurethanes (see Group IV(a)) is prepared by reacting one mole of formaldehyde, 4 moles of aniline and one mole of hydrochloric acid. The crude product of 2:41- and 4:41- diaminodiphenylmethane, containing 15% of polyamines (mainly triamines) is converted to a mixture of the corresponding isocyanates by treatment in o-dichlorobenzene with phosgene, firstly at 0 DEG C. and subsequently at 165 to 175 DEG C.ALSO:<PICT:0845206/III/1> A mixing apparatus comprises a reservoir zone into which some or all of the ingredients to be mixed are fed, and a mixing zone, said reservoir zone being separated from said mixing zone by a weir-like barrier over which the ingredients flow from the reservoir zone to the mixing zone, and said mixing zone being provided with inlet ports for any ingredients not fed into the reservoir zone, and with mixing means and an exit port below the level of the weir-like barrier. The apparatus is useful in the production of foamed or homogeneous polyurethanes. Polyester or other hydroxyl-containing polyurethane-forming material and polyisocyanate are fed separately into ports D and E and activator mixture is fed into F. Stirrer G mixes the reactants and the product is discharged through I, the rate of flow of reactants being such that there is no build up of material in mixing C tending to flow back over weir B. There may also be an auxiliary stirrer H in zone A. At the end of a run the flow of activator and polyisocyanate components is stopped first and the reservoir, which is then filled with polyhydroxylic material alone, prevents p ingress of moisture to the polyisocyanate. The mixing head may have an outer jacket for the circulation of cooling liquid. Specification 839,183 is referred to.
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE565981D BE565981A (en) | 1957-03-22 | ||
| NL226126D NL226126A (en) | 1957-03-22 | ||
| NL102765D NL102765C (en) | 1957-03-22 | ||
| GB9435/57A GB845206A (en) | 1957-03-22 | 1957-03-22 | Mixing apparatus |
| FR1203647D FR1203647A (en) | 1957-03-22 | 1958-03-22 | Mixing device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB9435/57A GB845206A (en) | 1957-03-22 | 1957-03-22 | Mixing apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB845206A true GB845206A (en) | 1960-08-17 |
Family
ID=9871925
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB9435/57A Expired GB845206A (en) | 1957-03-22 | 1957-03-22 | Mixing apparatus |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE565981A (en) |
| FR (1) | FR1203647A (en) |
| GB (1) | GB845206A (en) |
| NL (2) | NL226126A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0151652A2 (en) * | 1983-08-23 | 1985-08-21 | Synergistics Industries Limited/Les Industries Synergistics Limitee | Improved process for producing foamed plastic articles |
| GB2257150A (en) * | 1991-07-04 | 1993-01-06 | Hennecke Gmbh Maschf | A process for the production of elastomeric polyurethanes, particularly in the form of shoe soles |
| US5662753A (en) * | 1994-12-05 | 1997-09-02 | Loos; James H. | Installation of moldings |
| CN111479663A (en) * | 2017-12-19 | 2020-07-31 | 汉高股份有限及两合公司 | Device and method for producing plastic parts, in particular for applying adhesive |
| CN113442363A (en) * | 2021-07-14 | 2021-09-28 | 清远市番亿聚氨酯有限公司 | Polyurethane foaming equipment with accurate raw material mixing proportion |
-
0
- NL NL102765D patent/NL102765C/xx active
- NL NL226126D patent/NL226126A/xx unknown
- BE BE565981D patent/BE565981A/xx unknown
-
1957
- 1957-03-22 GB GB9435/57A patent/GB845206A/en not_active Expired
-
1958
- 1958-03-22 FR FR1203647D patent/FR1203647A/en not_active Expired
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0151652A2 (en) * | 1983-08-23 | 1985-08-21 | Synergistics Industries Limited/Les Industries Synergistics Limitee | Improved process for producing foamed plastic articles |
| EP0151652A3 (en) * | 1983-08-23 | 1985-10-16 | Synergistics Chemicals Limited | Improved process for producing foamed plastic articles |
| GB2257150A (en) * | 1991-07-04 | 1993-01-06 | Hennecke Gmbh Maschf | A process for the production of elastomeric polyurethanes, particularly in the form of shoe soles |
| GB2257150B (en) * | 1991-07-04 | 1995-02-08 | Hennecke Gmbh Maschf | A process for the production of elastomeric polyurethanes, more particularly in the form of shoe soles |
| US5662753A (en) * | 1994-12-05 | 1997-09-02 | Loos; James H. | Installation of moldings |
| CN111479663A (en) * | 2017-12-19 | 2020-07-31 | 汉高股份有限及两合公司 | Device and method for producing plastic parts, in particular for applying adhesive |
| CN111479663B (en) * | 2017-12-19 | 2022-06-24 | 汉高股份有限及两合公司 | Device and method for producing plastic parts, in particular for applying adhesive |
| US11780117B2 (en) | 2017-12-19 | 2023-10-10 | Henkel Ag & Co., Kgaa | Device and method for the production of plastic parts with drying and dessicant feed devices |
| CN113442363A (en) * | 2021-07-14 | 2021-09-28 | 清远市番亿聚氨酯有限公司 | Polyurethane foaming equipment with accurate raw material mixing proportion |
Also Published As
| Publication number | Publication date |
|---|---|
| FR1203647A (en) | 1960-01-20 |
| BE565981A (en) | |
| NL102765C (en) | |
| NL226126A (en) |
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