GB842299A - A process involving the treatment of fluid material by contacting it with granular solid material - Google Patents

A process involving the treatment of fluid material by contacting it with granular solid material

Info

Publication number
GB842299A
GB842299A GB1621058A GB1621058A GB842299A GB 842299 A GB842299 A GB 842299A GB 1621058 A GB1621058 A GB 1621058A GB 1621058 A GB1621058 A GB 1621058A GB 842299 A GB842299 A GB 842299A
Authority
GB
United Kingdom
Prior art keywords
solids
passage
bed
chamber
regenerator
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB1621058A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WALTER PHILIP WILLIAMS
Original Assignee
WALTER PHILIP WILLIAMS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by WALTER PHILIP WILLIAMS filed Critical WALTER PHILIP WILLIAMS
Priority to GB1621058A priority Critical patent/GB842299A/en
Publication of GB842299A publication Critical patent/GB842299A/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/08Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
    • B01J8/12Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by gravity in a downward flow

Abstract

<PICT:0842299/IV(b)/1> <PICT:0842299/IV(b)/2> In processes involving the transfer of granular solid material to or from a contacting zone under pressure where the solid is contacted with a fluid material from or to a lower pressure zone, there is maintained a seal leg of compacted solids between the zones of a length such that at the pressure differential fluid material would flow at a rate sufficient to cause boiling of the solids in the lower pressure zone, above the end of the seal leg in the lower pressure zone there is maintained a compact bed of solids having a cross-sectional area greater than the seal leg and sufficient, at a level below the upper surface of the bed, to reduce the velocity of fluid material to below the boiling velocity, solids are continuously removed from the lower pressure zone so that there is continual flow of solids through the seal leg, and solids are supplied to the upper surface of the bed. In Fig. 1, the reactor 10, e.g. for the catalytic conversion of hydrocarbons, is fed with freshly regenerated catalyst from regenerator 11, operated at a lower pressure than the reactor, by surge hoppers 32 and 35 as described in Specification 732,605 [Group III]. The charge is fed to the centre of the reactor by line 12, together with hydrogen or recycle gas if required, and product removed at each end by lines 14 and 15. Catalyst is removed from the reactor by passage 16 which forms the seal leg; into this is fed a purge gas at a pressure slightly above that in the reactor to prevent loss of reactants by passage 16. The seal leg empties into chamber 18 (Fig. 2) which contains a bed of solids of a height sufficient to reduce the velocity of the escaping gases below the boiling velocity below the upper surface of the bed, gases leaving by passage 19 through a filter 42 through which gases but not solids may pass. Solids are fed onto the top of the bed by passage 25 as described below. A series of baffles in chamber 18 allow for preferential removal by passage 20 of solids supplied to the chamber by passage 16 while allowing for some movement of the bed above the end of passage 16. Solids removed are transported by conveyer 21, e.g. a bucket elevator or gas lift, to a level above the regenerator whence is falls by gravity through passage 22. Solids to be supplied to the top of the bed in chamber 18 may be unregenerated solids from passage 22 or regenerated solids from passage 33. In either case they pass by passage 23, chamber 24 and passage 25. Chamber 24 is a safety device containing a bed of solids so that should the bed in chamber 18 fail, the gas passes through line 25 and is reduced in velocity by the bed in chamber 24 before passing through exit 43 so that a "blowout" cannot occur. In an alternative (Fig. 4 not shown) the solids from the seal leg empty into a chamber above the regenerator. Solids for supply to the top of the bed may in such a case be obtained from the hopper 32 above the reactor or from a hopper positioned above the chamber and supplied by a conveyer from a partial stream withdrawn from the passage between the chamber and regenerator, such hopper having an overflow pipe emptying into the passage leading to the regenerator. The process may be used in operations where gases, vapours or liquids are contacted with catalytic or inert materials, e.g. in the catalytic reforming of gasolines using a silica-alumina moving bed catalyst under conditions which include; vapour inlet temperature 100-1100 DEG F., catalyst inlet temperature 100-1200 DEG F., space velocity 0,1-6,0 vol/vol/hr., recycle ratio 1-15 mols (1-8 mols H2) per mol. of reactant and pressure 15-600 p.s.i.a.; the regenerator may be operated at 600-1400 DEG F. and 15-600 p.s.i.a.ALSO:<PICT:0842299/III/1> In processes involving the transfer of granular solid material to or from a contacting zone under pressure, where the solid is contacted with a fluid material, from or to a lower pressure zone, there is maintained a seal leg of compacted solids between the zones of a length such that at the pressure differential fluid material would flow at a rate sufficient to cause boiling of the solids in the lower pressure zone, above the end of the seal leg in the lower pressure zone there is maintained a compact bed of solids having a cross-sectional <PICT:0842299/III/2> area greater than the seal leg and sufficient, at a level below the upper surface of the bed, to reduce the velocity of fluid material to below the boiling velocity, solids are continuously removed from the lower pressure zone so that there is continual flow of solids through the seal leg, and solids are supplied to the upper surface of the bed. In Fig. 1, the reactor 10, e.g. for the catalytic conversion of hydrocarbons, is fed with freshly regenerated catalyst from regenerator 11, operated at a lower pressure than the reactor, by surge hoppers 32 and 35 as described in Specification 732,605. The charge is fed to the centre of the reactor by line 12, together with hydrogen or recycle gas if required, and product removed at each end by lines 14 and 15. Catalyst is removed from the reactor by passage 16 which forms the seal leg; into this is fed a purge gas at a pressure slightly above that in the reactor to prevent loss of reactants by passage 16. The seal leg empties into chamber 18 (Fig. 2) which contains a bed of solids of a height sufficient to reduce the velocity of the escaping gases below the boiling velocity below the upper surface of the bed, gases leaving by passage 19 through a filter 42 through which gases but not solids may pass. Solids are fed on to the top of the bed by passage 25 as described below. A series of baffles in chamber 18 allow for preferential removal by passage 20 of solids supplied to the chamber by passage 16 while allowing for some movement of the bed above the end of passage 16. Solids removed are transported by conveyer 21, e.g. a bucket elevator or gas lift, to a level above the regenerator whence it falls by gravity through passage 22. Solids to be supplied to the top of the bed in chamber 18 may be unregenerated solids from passage 22 or regenerated solids from passage 33. In either case they pass by passage 23, chamber 24 and passage 25. Chamber 24 is a safety device containing a bed of solids so that should the bed in chamber 18 fail, the gas passes through line 25 and are reduced in velocity by the bed in chamber 24 before passing through exit 43 so that a "blow-out" cannot occur. In an alternative (Fig. 4 not shown) the solids from the seal leg empty into a chamber above the regenerator. Solids for supply to the top of the bed may in such a case be obtained from the hopper 32 above the reactor or from a hopper positioned above the chamber and supplied by a conveyer from a partial stream withdrawn from the passage between the chamber and regenerator, such hopper having an overflow pipe emptying into the passage leading to the regenerator. The process may be used in operations where gases, vapours or liquids are contacted with catalytic or inert materials, e.g. in the catalytic reforming of gasolines using a silica-alumina moving bed catalyst under conditions which include; vapour inlet temperature 100-1100 DEG F. catalyst inlet temperature 100-1200 DEG F. space velocity 0.1-6.0 vol/vol/hr., recycle ratio 1-15 mols (1-8 mols H2) per mol. of reactant and pressure 15-600 p.s.i.a. The regenerator may be operated at 600-1400 DEG F. and 15-600 p.s.i.a.
GB1621058A 1958-05-20 1958-05-20 A process involving the treatment of fluid material by contacting it with granular solid material Expired GB842299A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB1621058A GB842299A (en) 1958-05-20 1958-05-20 A process involving the treatment of fluid material by contacting it with granular solid material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB1621058A GB842299A (en) 1958-05-20 1958-05-20 A process involving the treatment of fluid material by contacting it with granular solid material

Publications (1)

Publication Number Publication Date
GB842299A true GB842299A (en) 1960-07-27

Family

ID=10073152

Family Applications (1)

Application Number Title Priority Date Filing Date
GB1621058A Expired GB842299A (en) 1958-05-20 1958-05-20 A process involving the treatment of fluid material by contacting it with granular solid material

Country Status (1)

Country Link
GB (1) GB842299A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110465246A (en) * 2019-09-11 2019-11-19 上海电气电站环保工程有限公司 A kind of three phase separator

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110465246A (en) * 2019-09-11 2019-11-19 上海电气电站环保工程有限公司 A kind of three phase separator

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