GB822933A - Improved process and device for the distillation of fatty acids, glycerine and similar high-boiling substances - Google Patents
Improved process and device for the distillation of fatty acids, glycerine and similar high-boiling substancesInfo
- Publication number
- GB822933A GB822933A GB29193/56A GB2919356A GB822933A GB 822933 A GB822933 A GB 822933A GB 29193/56 A GB29193/56 A GB 29193/56A GB 2919356 A GB2919356 A GB 2919356A GB 822933 A GB822933 A GB 822933A
- Authority
- GB
- United Kingdom
- Prior art keywords
- dephlegmator
- liquid
- evaporator
- vapours
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
- C11C1/08—Refining
- C11C1/10—Refining by distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/26—Multiple-effect evaporating
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Wood Science & Technology (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
<PICT:0822933/III/1> In the distillation of liquid mixtures of high boiling-range, e.g. mixtures containing fatty acids and glycerine, the liquid is passed through a film evaporator of the liquid-downflow type; the vapours evolved in the evaporator are condensed, e.g. in a dephlegmator, and the condensate is distilled in a further film evaporator of the liquid-downflow type. A fatty acid mixture is fed through inlet 1 into preheater 2, where it is heated to about 150 DEG C. About 1 to 3% by weight of steam, supplied through pipe 4, is injected into the preheated acid mixture, and it then passes up through tube-evaporator 3, where 20 to 50% of the mixture is vaporized. The liquid-vapour mixture is discharged into vessel 6 where a separation of the two phases is effected. The separated liquid flows down film evaporator 7, where further vaporization takes place. The residual liquid then enters still 9 which is divided into two or more chambers, by baffles (not shown), each of which is provided with a heater-coil and a tube 10 for the injection of steam. The unevaporated residue is withdrawn through outlet 11. The vapours formed in evaporator 7 and still 9 flow up into vessel 6. The vapours which leave the top of vessel 6 flow to dephlegmator 13, and the condensate formed therein is led to film evaporator 14 and its associated still 15. The vapours which are not condensed in dephlegmator 13 and the re-evaporated light fractions from evaporator 14 and still 15 are mixed, and the vapour-mixture is subjected to two further stages of dephlegmation and partial re-evaporation. Dephlegmator 16 is maintained at a lower temperature than dephlegmator 13, and dephlegmator 19 is maintained at a lower temperature than dephlegmator 16. Product-fractions are withdrawn from stills 15, 18 and 21 via outlets 22, 23 and 24 respectively; while steam and odorous components are withdrawn via pipe 25.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE822933X | 1955-09-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB822933A true GB822933A (en) | 1959-11-04 |
Family
ID=6744713
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB29193/56A Expired GB822933A (en) | 1955-09-24 | 1956-09-24 | Improved process and device for the distillation of fatty acids, glycerine and similar high-boiling substances |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB822933A (en) |
-
1956
- 1956-09-24 GB GB29193/56A patent/GB822933A/en not_active Expired
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US2224984A (en) | Fatty acid distillation | |
| US3496159A (en) | Esterification of fatty acids of tall oil in a horizontal distillation column and condenser | |
| US2260072A (en) | Distillation and fractionation of mixtures of hydrocarbons | |
| GB304756A (en) | Improvements relating to the separation of liquids by distillation | |
| US2679472A (en) | Separation of hydrocarbons by azeotropic distillation | |
| GB900457A (en) | Improvements in the separation of liquid mixtures into their components | |
| US2224925A (en) | Fractional distillation of fatty acid materials | |
| US2462444A (en) | Production of maleic anhydride from maleic acid | |
| US2371010A (en) | Preparation of stable binary motor fuel | |
| US2716630A (en) | Distillation of tall oil | |
| US1862706A (en) | Continuous process for separating organic liquids | |
| GB822933A (en) | Improved process and device for the distillation of fatty acids, glycerine and similar high-boiling substances | |
| US2147306A (en) | Fatty acid distillation | |
| US2795538A (en) | Fractional distillation of coal tar | |
| US3496071A (en) | Process for the separation of organic materials by continuous horizontal evaporation and horizontal condensation | |
| US2322056A (en) | Treating fatty acid-containing stock | |
| GB901079A (en) | Purifying furfural | |
| US2785114A (en) | Schmalenbach | |
| US1826302A (en) | Method for the dehydration of formic acid | |
| GB1065178A (en) | An improved process and apparatus for extractive distillation | |
| US2171549A (en) | Process for azeotropic distillation of aliphatic acids | |
| US2299283A (en) | Treatment of enriched benzol wash oil or the like | |
| US2400370A (en) | Process and apparatus for producing in the pure state, butyl alcohol, acetone, and ethyl alcohol from watery solutions | |
| US1559218A (en) | Process of continuous rectification of spirits, petroleums, and benzols | |
| US2184164A (en) | Production of butadiene from 1, 3-butylene glycol |