GB822573A - A method for the manufacture of black colouring matter - Google Patents
A method for the manufacture of black colouring matterInfo
- Publication number
- GB822573A GB822573A GB3078756A GB3078756A GB822573A GB 822573 A GB822573 A GB 822573A GB 3078756 A GB3078756 A GB 3078756A GB 3078756 A GB3078756 A GB 3078756A GB 822573 A GB822573 A GB 822573A
- Authority
- GB
- United Kingdom
- Prior art keywords
- iron
- added
- urushiol
- china
- melamine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000004040 coloring Methods 0.000 title abstract 6
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 14
- 239000003973 paint Substances 0.000 abstract 8
- 229910052742 iron Inorganic materials 0.000 abstract 7
- 239000000203 mixture Substances 0.000 abstract 7
- RMTXUPIIESNLPW-UHFFFAOYSA-N 1,2-dihydroxy-3-(pentadeca-8,11-dienyl)benzene Natural products CCCC=CCC=CCCCCCCCC1=CC=CC(O)=C1O RMTXUPIIESNLPW-UHFFFAOYSA-N 0.000 abstract 6
- QARRXYBJLBIVAK-UEMSJJPVSA-N 3-[(8e,11e)-pentadeca-8,11-dienyl]benzene-1,2-diol;3-[(8e,11e)-pentadeca-8,11,14-trienyl]benzene-1,2-diol;3-[(8e,11e,13e)-pentadeca-8,11,13-trienyl]benzene-1,2-diol;3-[(e)-pentadec-8-enyl]benzene-1,2-diol;3-pentadecylbenzene-1,2-diol Chemical compound CCCCCCCCCCCCCCCC1=CC=CC(O)=C1O.CCCCCC\C=C\CCCCCCCC1=CC=CC(O)=C1O.CCC\C=C\C\C=C\CCCCCCCC1=CC=CC(O)=C1O.C\C=C\C=C\C\C=C\CCCCCCCC1=CC=CC(O)=C1O.OC1=CC=CC(CCCCCCC\C=C\C\C=C\CC=C)=C1O QARRXYBJLBIVAK-UEMSJJPVSA-N 0.000 abstract 6
- IYROWZYPEIMDDN-UHFFFAOYSA-N 3-n-pentadec-8,11,13-trienyl catechol Natural products CC=CC=CCC=CCCCCCCCC1=CC=CC(O)=C1O IYROWZYPEIMDDN-UHFFFAOYSA-N 0.000 abstract 6
- 229920000877 Melamine resin Polymers 0.000 abstract 6
- VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 abstract 6
- 239000002904 solvent Substances 0.000 abstract 6
- DQTMTQZSOJMZSF-UHFFFAOYSA-N urushiol Natural products CCCCCCCCCCCCCCCC1=CC=CC(O)=C1O DQTMTQZSOJMZSF-UHFFFAOYSA-N 0.000 abstract 6
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 abstract 4
- -1 ferrous compound Chemical class 0.000 abstract 4
- 239000000470 constituent Substances 0.000 abstract 3
- MIHINWMALJZIBX-UHFFFAOYSA-N cyclohexa-2,4-dien-1-ol Chemical compound OC1CC=CC=C1 MIHINWMALJZIBX-UHFFFAOYSA-N 0.000 abstract 3
- 238000010438 heat treatment Methods 0.000 abstract 3
- 239000004312 hexamethylene tetramine Substances 0.000 abstract 3
- 235000010299 hexamethylene tetramine Nutrition 0.000 abstract 3
- 239000004922 lacquer Substances 0.000 abstract 3
- 229960004011 methenamine Drugs 0.000 abstract 3
- 239000000126 substance Substances 0.000 abstract 3
- 229920001875 Ebonite Polymers 0.000 abstract 2
- RRHGJUQNOFWUDK-UHFFFAOYSA-N Isoprene Chemical compound CC(=C)C=C RRHGJUQNOFWUDK-UHFFFAOYSA-N 0.000 abstract 2
- 239000004640 Melamine resin Substances 0.000 abstract 2
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 abstract 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 2
- 239000005864 Sulphur Substances 0.000 abstract 2
- 229920001807 Urea-formaldehyde Polymers 0.000 abstract 2
- 229920000180 alkyd Polymers 0.000 abstract 2
- 229920001971 elastomer Polymers 0.000 abstract 2
- 239000003822 epoxy resin Substances 0.000 abstract 2
- 235000021388 linseed oil Nutrition 0.000 abstract 2
- 239000000944 linseed oil Substances 0.000 abstract 2
- 239000000395 magnesium oxide Substances 0.000 abstract 2
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 abstract 2
- 229940098895 maleic acid Drugs 0.000 abstract 2
- 239000011976 maleic acid Substances 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 238000000465 moulding Methods 0.000 abstract 2
- 229920001568 phenolic resin Polymers 0.000 abstract 2
- 229920000647 polyepoxide Polymers 0.000 abstract 2
- 229920000915 polyvinyl chloride Polymers 0.000 abstract 2
- 239000004800 polyvinyl chloride Substances 0.000 abstract 2
- 239000000843 powder Substances 0.000 abstract 2
- 239000005060 rubber Substances 0.000 abstract 2
- 239000004753 textile Substances 0.000 abstract 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 abstract 2
- AAPLIUHOKVUFCC-UHFFFAOYSA-N trimethylsilanol Chemical compound C[Si](C)(C)O AAPLIUHOKVUFCC-UHFFFAOYSA-N 0.000 abstract 2
- 239000003981 vehicle Substances 0.000 abstract 2
- XNWFRZJHXBZDAG-UHFFFAOYSA-N 2-METHOXYETHANOL Chemical compound COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 abstract 1
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 abstract 1
- MCDLETWIOVSGJT-UHFFFAOYSA-N acetic acid;iron Chemical compound [Fe].CC(O)=O.CC(O)=O MCDLETWIOVSGJT-UHFFFAOYSA-N 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 229910021506 iron(II) hydroxide Inorganic materials 0.000 abstract 1
- NCNCGGDMXMBVIA-UHFFFAOYSA-L iron(ii) hydroxide Chemical compound [OH-].[OH-].[Fe+2] NCNCGGDMXMBVIA-UHFFFAOYSA-L 0.000 abstract 1
- 239000003921 oil Substances 0.000 abstract 1
- 235000019198 oils Nutrition 0.000 abstract 1
- 239000002966 varnish Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B63/00—Lakes
- C09B63/005—Metal lakes of dyes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
- C07C39/235—Metal derivatives of a hydroxy group bound to a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F15/00—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table
- C07F15/02—Iron compounds
- C07F15/025—Iron compounds without a metal-carbon linkage
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B57/00—Other synthetic dyes of known constitution
- C09B57/10—Metal complexes of organic compounds not being dyes in uncomplexed form
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
A black colouring matter is prepared by heating a ferrous compound with urushiol to produce iron urushiolate and dissolving the product in a solvent. The term urushiol includes the chief constituents of lacquers from China, Japan, Korea, Burma, Indo-China and Java which are of slightly different chemical composition. The iron may be present in the stoichiometric proportion, or in lesser amount, in which case the addition product of hexamethylene tetramine and a monohydric phenol is condensed with the product. Examples are given of producing both types. The colouring matter may be dissolved in solvent naphtha and ethylene glycol monomethyl ether to form a printing ink; it may be added to a varnish consisting of polymerized drying oils and thinners; it may be added to paints consisting of modified or unmodified alkyd resins and suitable vehicles; it may be added to tri-methyl silanol and solvent naphtha to form a silicoresin paint; it may be added to a paint consisting of an epoxy resin, a melamine-formaldehyde resin and solvent naphtha; these paint compositions are hardened by baking after application; it may be incorporated into moulding powders containing phenol-, urea- or melamine-formaldehyde resin or polyvinyl chloride; and it may be included in the mixture of rubber, sulphur and magnesia used in the production of ebonite. It may also be mixed with a melamine resin or with maleic-acid modified linseed oil to form a printing paste for textiles; the printed material must be heated to harden the print.ALSO:A black colouring matter comprises a solution of iron urushiolate, prepared by heating a ferrous compound with urushiol. The term urushiol includes the chief constituents of lacquers from China, Japan, Korea, Burma, Indo-China and Java which are of slightly different chemical composition. The iron may be present in the stoichiometric proportion, or in lesser amount in which case the addition product of hexamethylene tetramine and a monohydric phenol is condensed with the product. Examples are given of producing both types. The ferrous compound may be ferrous hydroxide or ferrous acetate (pyrolignite of iron).ALSO:A black colouring matter comprises a solution of iron urushiolate, prepared by heating a ferrous compound with urushiol. The term urushiol includes the chief constituents of lacquers from China, Japan, Korea, Burma, Indo-China and Java which are of slightly different chemical composition. The iron may be present in the stoichiometric proportion, or in lesser amount, in which case the addition product of hexamethylene tetramine and a monohydric phenol is condensed with the product. Examples are given of producing both types. The colouring matter may be added to paints consisting of modified or unmodified alkyd resins and suitable vehicles; it may be added to trimethyl silanol and solvent naphtha to form a silicoresin paint; it may be added to a paint consisting of an epoxy resin, a melamine-formaldehyde resin and solvent naphtha; these paint compositions are hardened by baking after application; it may be incorporated into moulding powders containing phenol-, urea-, or melamine-formaldehyde resin or polyvinyl chloride; and it may be included in the mixture of rubber, sulphur and magnesia used in the production of ebonite. It may also be mixed with a melamine resin or with maleic-acid modified linseed oil to form a printing paste for textiles; the printed material must be heated to harden the print.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3078756A GB822573A (en) | 1956-10-09 | 1956-10-09 | A method for the manufacture of black colouring matter |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3078756A GB822573A (en) | 1956-10-09 | 1956-10-09 | A method for the manufacture of black colouring matter |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB822573A true GB822573A (en) | 1959-10-28 |
Family
ID=10313134
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3078756A Expired GB822573A (en) | 1956-10-09 | 1956-10-09 | A method for the manufacture of black colouring matter |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB822573A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102285869A (en) * | 2011-06-23 | 2011-12-21 | 福建师范大学 | Method for preparing urushiol-metal polymer through direct grinding |
| CN114853114A (en) * | 2022-05-25 | 2022-08-05 | 福建师范大学 | Magnetic urushiol iron nanoparticle with photo-thermal effect and preparation method thereof |
-
1956
- 1956-10-09 GB GB3078756A patent/GB822573A/en not_active Expired
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102285869A (en) * | 2011-06-23 | 2011-12-21 | 福建师范大学 | Method for preparing urushiol-metal polymer through direct grinding |
| CN102285869B (en) * | 2011-06-23 | 2013-08-21 | 福建师范大学 | Method for preparing urushiol-metal polymer through direct grinding |
| CN114853114A (en) * | 2022-05-25 | 2022-08-05 | 福建师范大学 | Magnetic urushiol iron nanoparticle with photo-thermal effect and preparation method thereof |
| CN114853114B (en) * | 2022-05-25 | 2023-08-18 | 福建师范大学 | Magnetic urushiol iron nanoparticle with photo-thermal effect and preparation method thereof |
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