GB785410A - Improvements in and relating to substituted tetrahydronaphthalenes - Google Patents
Improvements in and relating to substituted tetrahydronaphthalenesInfo
- Publication number
- GB785410A GB785410A GB168/56A GB16856A GB785410A GB 785410 A GB785410 A GB 785410A GB 168/56 A GB168/56 A GB 168/56A GB 16856 A GB16856 A GB 16856A GB 785410 A GB785410 A GB 785410A
- Authority
- GB
- United Kingdom
- Prior art keywords
- lower alkyl
- relating
- trimethyl
- tetrahydronaphthalenes
- substituted tetrahydronaphthalenes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- CXWXQJXEFPUFDZ-UHFFFAOYSA-N tetralin Chemical class C1=CC=C2CCCCC2=C1 CXWXQJXEFPUFDZ-UHFFFAOYSA-N 0.000 title 1
- 125000000217 alkyl group Chemical group 0.000 abstract 3
- ZIDUJCHAYXSXNA-UHFFFAOYSA-N 5-(4-methylphenyl)hexan-2-one Chemical compound CC(=O)CCC(C)C1=CC=C(C)C=C1 ZIDUJCHAYXSXNA-UHFFFAOYSA-N 0.000 abstract 1
- 238000003747 Grignard reaction Methods 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- WETWJCDKMRHUPV-UHFFFAOYSA-N acetyl chloride Chemical compound CC(Cl)=O WETWJCDKMRHUPV-UHFFFAOYSA-N 0.000 abstract 1
- 239000012346 acetyl chloride Substances 0.000 abstract 1
- -1 alkyl magnesium iodide Chemical compound 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 abstract 1
- 229910001641 magnesium iodide Inorganic materials 0.000 abstract 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
- 239000001117 sulphuric acid Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0042—Essential oils; Perfumes compounds containing condensed hydrocarbon rings
- C11B9/0046—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings
- C11B9/0049—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings the condensed rings sharing two common C atoms
- C11B9/0053—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings the condensed rings sharing two common C atoms both rings being six-membered
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention comprises 6-acetyl-1 : 4 : 7-trimethyl - 1 - lower alkyl - 1 : 2 : 3 : 4 - tetrahydronaphthalenes, where "lower alkyl" means methyl and ethyl. The compounds are prepared by a Grignard reaction between 5-p-tolylhexan-2-one and a lower alkyl magnesium iodide to give 2-lower alkyl-5-p-tolyl-hexan-2-ol, which is then treated with concentrated sulphuric acid to yield 1 : 4 : 7 - trimethyl - 1 - lower alkyl - 1 : 2 : 3 : 4 - tetrahydronaphthalene which is acetylated with acetyl chloride. Examples are given.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US785410XA | 1955-01-28 | 1955-01-28 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB785410A true GB785410A (en) | 1957-10-30 |
Family
ID=22144692
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB168/56A Expired GB785410A (en) | 1955-01-28 | 1956-01-03 | Improvements in and relating to substituted tetrahydronaphthalenes |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB785410A (en) |
-
1956
- 1956-01-03 GB GB168/56A patent/GB785410A/en not_active Expired
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