GB694132A - Improvements in or relating to the production of gelatino silver halide photographicemulsions - Google Patents
Improvements in or relating to the production of gelatino silver halide photographicemulsionsInfo
- Publication number
- GB694132A GB694132A GB82051A GB82051A GB694132A GB 694132 A GB694132 A GB 694132A GB 82051 A GB82051 A GB 82051A GB 82051 A GB82051 A GB 82051A GB 694132 A GB694132 A GB 694132A
- Authority
- GB
- United Kingdom
- Prior art keywords
- anhydride
- parts
- glutamic
- acid
- photographicemulsions
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- -1 silver halide Chemical class 0.000 title abstract 2
- 229910052709 silver Inorganic materials 0.000 title 1
- 239000004332 silver Substances 0.000 title 1
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 abstract 4
- 229920000642 polymer Polymers 0.000 abstract 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 229920001577 copolymer Polymers 0.000 abstract 2
- 229920001184 polypeptide Polymers 0.000 abstract 2
- 108090000765 processed proteins & peptides Proteins 0.000 abstract 2
- 102000004196 processed proteins & peptides Human genes 0.000 abstract 2
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 abstract 2
- QBFQXAKABOKEHT-JTQLQIEISA-N (2s)-3-(4-acetyloxyphenyl)-2-azaniumylpropanoate Chemical compound CC(=O)OC1=CC=C(C[C@H](N)C(O)=O)C=C1 QBFQXAKABOKEHT-JTQLQIEISA-N 0.000 abstract 1
- JUAPMRSLDANLAS-UHFFFAOYSA-N 3,6-dibenzylpiperazine-2,5-dione Chemical compound O=C1NC(CC=2C=CC=CC=2)C(=O)NC1CC1=CC=CC=C1 JUAPMRSLDANLAS-UHFFFAOYSA-N 0.000 abstract 1
- JHWZWIVZROVFEM-UHFFFAOYSA-N 4-(2-methylpropyl)-1,3-oxazolidine-2,5-dione Chemical compound CC(C)CC1NC(=O)OC1=O JHWZWIVZROVFEM-UHFFFAOYSA-N 0.000 abstract 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 1
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 abstract 1
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 abstract 1
- 108010020346 Polyglutamic Acid Proteins 0.000 abstract 1
- 235000001014 amino acid Nutrition 0.000 abstract 1
- 150000001413 amino acids Chemical class 0.000 abstract 1
- 150000008064 anhydrides Chemical class 0.000 abstract 1
- 235000003704 aspartic acid Nutrition 0.000 abstract 1
- OQFSQFPPLPISGP-UHFFFAOYSA-N beta-carboxyaspartic acid Natural products OC(=O)C(N)C(C(O)=O)C(O)=O OQFSQFPPLPISGP-UHFFFAOYSA-N 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 230000000903 blocking effect Effects 0.000 abstract 1
- 229960004424 carbon dioxide Drugs 0.000 abstract 1
- 235000011089 carbon dioxide Nutrition 0.000 abstract 1
- 229960003067 cystine Drugs 0.000 abstract 1
- 235000013922 glutamic acid Nutrition 0.000 abstract 1
- 239000004220 glutamic acid Substances 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229920002643 polyglutamic acid Polymers 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/015—Apparatus or processes for the preparation of emulsions
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Polyamides (AREA)
Abstract
Synthetic polypeptides are prepared by esterifying the g -carboxylic group of glutamic or a like amino acid, converting to the carbonic anhydride, any free reactive group being blocked before such anhydride formation, allowing to polymerize in pyridine solution, and removing any blocking groups that have been introduced, e.g. by hydrolysis. The polypeptide may be polyglutamic acid, a copolymer of glutamic acid and another a -amino acid, or a corresponding compound in which aspartic acid is used. An optically active compound or racemic mixture may be used. The polymer may be dissolved in pyridine and precipitated with ether to free the polymer from polymers of lower molecular weight. Copolymers may be prepared from 3 parts of g -methyl-glutamic anhydride and 1 or 2 parts of leucine anhydride, 1 or 2 parts of phenylalanine anhydride, or 1 part of o-acetyltyrosine or cystine anhydride.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB82051A GB694132A (en) | 1951-01-11 | 1951-01-11 | Improvements in or relating to the production of gelatino silver halide photographicemulsions |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB82051A GB694132A (en) | 1951-01-11 | 1951-01-11 | Improvements in or relating to the production of gelatino silver halide photographicemulsions |
Publications (1)
Publication Number | Publication Date |
---|---|
GB694132A true GB694132A (en) | 1953-07-15 |
Family
ID=9711049
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB82051A Expired GB694132A (en) | 1951-01-11 | 1951-01-11 | Improvements in or relating to the production of gelatino silver halide photographicemulsions |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB694132A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2833650A (en) * | 1955-02-07 | 1958-05-06 | Du Pont | Photographic emulsions |
-
1951
- 1951-01-11 GB GB82051A patent/GB694132A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2833650A (en) * | 1955-02-07 | 1958-05-06 | Du Pont | Photographic emulsions |
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