GB685719A - Improvements in or relating to distillation processes and apparatus - Google Patents
Improvements in or relating to distillation processes and apparatusInfo
- Publication number
- GB685719A GB685719A GB12234/50A GB1223450A GB685719A GB 685719 A GB685719 A GB 685719A GB 12234/50 A GB12234/50 A GB 12234/50A GB 1223450 A GB1223450 A GB 1223450A GB 685719 A GB685719 A GB 685719A
- Authority
- GB
- United Kingdom
- Prior art keywords
- liquid
- circulator
- compartment
- compartments
- central
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
- C11C1/08—Refining
- C11C1/10—Refining by distillation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Microbiology (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
High boiling liquids are distilled or deodorized by passing the liquid successively through two or more compartments arranged in series in a single vessel, each compartment being provided with a circulator, such as a riser-tube dipping in the liquid and having an inlet for a propellant vapour, which raises the liquid in the compartment and causes it to impinge against <PICT:0685719/III/1> <PICT:0685719/III/2> <PICT:0685719/III/3> a baffle disposed in the vapour space of the vessel, the liquid being heated (distilling) or cooled (deodorizing) during its passage through the circulator by a heat exchanger disposed in the circulator. The distillation of mineral oils, glycerine and fatty acids, and the deodorization of oils, fats, waxes and resins (natural or synthetic), are referred to. The process is preferably carried out under reduced pressure. The annular space between cylinder 2 and the wall of distillation-still 1 is divided into eight compartments 4 by partitions 3; and the cylinder and the compartments each contain a circulator 5. Each circulator comprises a dip-pipe 6, and a riser-tube 7 which is supplied with steam or hydrocarbon vapour through line 10, and which contains heating-tubes 8. The distilland is introduced into the central circulator through line 15, and is lifted to, and dispersed in the vapour space of the central compartment where partial vaporization takes place. Part of the remaining liquid, which collects in the lower part of the still, re-enters the central circulator through opening 9; and the rest flows through opening 16 into the first compartment 4 where it is lifted by the circulator in that compartment. The unvaporized liquid passes through the succeeding compartments 4 via openings 17, and is finally discharged from the last compartment through line 18. The liquid is circulated separately in each compartment. The distillation-temperature may be kept higher in the first compartments than in the last ones. In order that the residence-time of the liquid in the still may be as short as possible (so as to avoid thermal decomposition), the liquid-content and the liquid-level are both kept low, and the bottom 19 of the central chamber is disposed higher than the bottom 20 of the still. The mixture of distilland-vapours and lift-vapours, is withdrawn through outlet 28 into a vacuum plant. If a plurality of fractions is required, the vapour space of the still is subdivided into compartments each of which is provided with a separate conduit leading to a separate condenser; and the compartments may be subjected to different degrees of vacuum. A similar apparatus designed for holding greater depths of liquid, which is suitable for the deodorization of oils, is also described. In this apparatus the central chamber is separated from the annular chambers by a double wall. The oil is introduced into one of the annular chambers, and is withdrawn from the central chamber. The heating tubes may be the double type wherein the heating steam flows up the inner tube (which is open at the top) and then flows down the annular space between the inner and the outer tube (which is closed at the top). The heating element shown in Fig. 6 comprises a central tube 26 provided with several branch tubes 27. Heating steam is supplied through line 13 and the condensate is discharged through line 14, or vice versa. Specifications 225,552, [Class 32], 546,416 and 608,595 are referred to.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE685719X | 1949-05-16 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB685719A true GB685719A (en) | 1953-01-07 |
Family
ID=6597922
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB12234/50A Expired GB685719A (en) | 1949-05-16 | 1950-05-16 | Improvements in or relating to distillation processes and apparatus |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB685719A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2994647A (en) * | 1958-03-31 | 1961-08-01 | American Mach & Foundry | Flash evaporator |
US4767502A (en) * | 1986-05-26 | 1988-08-30 | Oy Santasalo-Sohlberg Ab | Steam generator in a multi-stage distilling apparatus |
-
1950
- 1950-05-16 GB GB12234/50A patent/GB685719A/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2994647A (en) * | 1958-03-31 | 1961-08-01 | American Mach & Foundry | Flash evaporator |
US4767502A (en) * | 1986-05-26 | 1988-08-30 | Oy Santasalo-Sohlberg Ab | Steam generator in a multi-stage distilling apparatus |
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