GB684625A - Improvements in or relating to dyestuff intermediates - Google Patents
Improvements in or relating to dyestuff intermediatesInfo
- Publication number
- GB684625A GB684625A GB686350A GB686350A GB684625A GB 684625 A GB684625 A GB 684625A GB 686350 A GB686350 A GB 686350A GB 686350 A GB686350 A GB 686350A GB 684625 A GB684625 A GB 684625A
- Authority
- GB
- United Kingdom
- Prior art keywords
- bis
- general formula
- methiodide
- alkyl
- prepared
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000543 intermediate Substances 0.000 title abstract 2
- 239000000975 dye Substances 0.000 title 1
- 125000000217 alkyl group Chemical group 0.000 abstract 3
- INQOMBQAUSQDDS-UHFFFAOYSA-N iodomethane Chemical compound IC INQOMBQAUSQDDS-UHFFFAOYSA-N 0.000 abstract 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- 125000003710 aryl alkyl group Chemical group 0.000 abstract 2
- 125000000623 heterocyclic group Chemical group 0.000 abstract 2
- DXYYSGDWQCSKKO-UHFFFAOYSA-N methylbenzothiazole Natural products C1=CC=C2SC(C)=NC2=C1 DXYYSGDWQCSKKO-UHFFFAOYSA-N 0.000 abstract 2
- FECNOIODIVNEKI-UHFFFAOYSA-N 2-[(2-aminobenzoyl)amino]benzoic acid Chemical class NC1=CC=CC=C1C(=O)NC1=CC=CC=C1C(O)=O FECNOIODIVNEKI-UHFFFAOYSA-N 0.000 abstract 1
- 125000002373 5 membered heterocyclic group Chemical group 0.000 abstract 1
- 125000004070 6 membered heterocyclic group Chemical group 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 125000002768 hydroxyalkyl group Chemical group 0.000 abstract 1
- VUQUOGPMUUJORT-UHFFFAOYSA-N methyl 4-methylbenzenesulfonate Chemical compound COS(=O)(=O)C1=CC=C(C)C=C1 VUQUOGPMUUJORT-UHFFFAOYSA-N 0.000 abstract 1
- MOOSRNWDPWTOBF-UHFFFAOYSA-N methyl n-phenylcarbamodithioate Chemical compound CSC(=S)NC1=CC=CC=C1 MOOSRNWDPWTOBF-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
- Plural Heterocyclic Compounds (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
Abstract
Dye intermediates of the general formula <FORM:0684625/IV (b)/1> wherein R1 and R2 each represent an alkyl, hydroxyalkyl, or aralkyl group, D represents the residue of a 5- or 6-membered heterocyclic ring system, and n is 0 or 1, are prepared by reacting two molecular proportions of a heterocyclic base of the general formula <FORM:0684625/IV (b)/2> with an excess over one molecular proportion of a compound of the general formula <FORM:0684625/IV (b)/3> wherein R3 is alkyl, aralkyl, or aryl and R4 is or as R3, in the presence of an excess over three molecular proportions of an alkyl toluene-sulphonate of the general formula <FORM:0684625/IV (b)/4> The reaction of the heterocyclic base with the intermediate <FORM:0684625/IV (b)/5> is referred to. 2-b : b -Bis-methylthiovinylbenzthiazole methiodide is prepared by heating together 2 - methylbenzthiazole, methyl p - toluenesulphonate, and methyl phenyldithiocarbamate, dissolving in ethanol, and pouring into aqueous KI. 2-b : b -Bis-ethylthiovinylbenzthiazole ethiodide, 2-b : b -bis-methylthiovinylbenzoxazole methiodide and 2-b : b -bis-methylthiovinylbenzthiazole methiodide are similarly prepared. Specifications 549,201, 549,202, 549,203, 549,204, 623,990; 678,626, 681,736 and 684,622, [all in Group IV (c)], are referred to.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB686350A GB684625A (en) | 1950-03-20 | 1950-03-20 | Improvements in or relating to dyestuff intermediates |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB686350A GB684625A (en) | 1950-03-20 | 1950-03-20 | Improvements in or relating to dyestuff intermediates |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB684625A true GB684625A (en) | 1952-12-24 |
Family
ID=9822134
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB686350A Expired GB684625A (en) | 1950-03-20 | 1950-03-20 | Improvements in or relating to dyestuff intermediates |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB684625A (en) |
-
1950
- 1950-03-20 GB GB686350A patent/GB684625A/en not_active Expired
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