GB669206A - Improvements in and relating to lubricating grease - Google Patents

Improvements in and relating to lubricating grease

Info

Publication number
GB669206A
GB669206A GB18474/49A GB1847449A GB669206A GB 669206 A GB669206 A GB 669206A GB 18474/49 A GB18474/49 A GB 18474/49A GB 1847449 A GB1847449 A GB 1847449A GB 669206 A GB669206 A GB 669206A
Authority
GB
United Kingdom
Prior art keywords
acids
oxidized
per cent
oil
fraction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB18474/49A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bataafsche Petroleum Maatschappij NV
Original Assignee
Bataafsche Petroleum Maatschappij NV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bataafsche Petroleum Maatschappij NV filed Critical Bataafsche Petroleum Maatschappij NV
Publication of GB669206A publication Critical patent/GB669206A/en
Expired legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M5/00—Solid or semi-solid compositions containing as the essential lubricating ingredient mineral lubricating oils or fatty oils and their use
    • C—CHEMISTRY; METALLURGY
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    • C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C—CHEMISTRY; METALLURGY
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    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
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    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/026—Butene
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    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/14—Synthetic waxes, e.g. polythene waxes
    • C—CHEMISTRY; METALLURGY
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    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
    • C—CHEMISTRY; METALLURGY
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    • C10M2205/17—Fisher Tropsch reaction products
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    • C10M2205/20—Natural rubber; Natural resins
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    • C10M2207/02—Hydroxy compounds
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    • C10M2207/026—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings with tertiary alkyl groups
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    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
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    • C10M2207/128—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids containing hydroxy groups; Ethers thereof
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    • C10M2207/129—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of thirty or more carbon atoms
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    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C10M2223/041—Triaryl phosphates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C10M2223/042—Metal salts thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C10M2223/047—Thioderivatives not containing metallic elements
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/12—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions obtained by phosphorisation of organic compounds, e.g. with PxSy, PxSyHal or PxOy
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/02—Groups 1 or 11
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/04—Groups 2 or 12
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/06—Groups 3 or 13
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/08—Groups 4 or 14
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/10—Groups 5 or 15
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/12—Groups 6 or 16
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/14—Group 7
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00—Metal present as such or in compounds
    • C10N2010/16—Groups 8, 9, or 10
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00—Form in which the lubricant is applied to the material being lubricated
    • C10N2050/10—Semi-solids; greasy
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2060/00—Chemical after-treatment of the constituents of the lubricating composition
    • C10N2060/04—Oxidation, e.g. ozonisation

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

Alkylene glycol and alkylene thioglycol polymers and their mono ester and ether derivatives are employed as stabilizers for certain lubricating grease compositions (see Group III). The polymers have the formula H-(OCnH2n-O-CmH2m)a-OH where a (n+m) is at least 6 and are prepared by polymerizing, in presence of iodine &c. as catalyst, ethylene, propylene, butylene or isobutylene oxide or by reacting a monohydric alcohol with an alkylene oxide. The average m.w. of the polymers is from 200-7000. The esters are prepared by esterifying the polymers with suitable acids especially higher fatty acids, naphthenic acids, sulphonic acids or oxidized tall oil acids. An example of a lubricating grease comprises 3.7 per cent hydrogenated fish oil acids, 3.7 per cent castor oil acids, 1.0 per cent lithium hydrate solution, 10 per cent paraffin oil 35-40 per cent, Coastal pale oil, 5-15 per cent oxidized Edeleanu extract and 0.1 per cent polyethylene glycol.ALSO:In the manufacture of a lubricating grease composition prepared from a mineral and/or synthetic oil and a minor proportion of a soap, there is added to the composition at any stage of its manufacture, from 1-20 per cent by weight of an oxidized petroleum fraction rich in aromatics, and/or an oxidized nitrogenous fraction and/or an oxidized sulphurous fraction, both the last two of which are derived from a petroleum fraction rich in aromatics. In a modification the aromatic fraction may be added to the grease composition in which it is then oxidized. The aromatic fractions are preferably obtained by the sulphur dioxide or furfural treatment of a petroleum distillate of S.U.V. about 60 at 210 DEG F. although other solvents are also mentioned and suitable fractions may also be obtained by catalytic conversion of petroleum hydrocarbons. The fraction may be oxidized before or after addition to the grease, by exposure to the air or blowing air through the fraction. The fractions may also be oxidized, prior to their addition to the grease, by means of hydrogen peroxide, manganese dioxide, permanganates, chlorates, perchlorates, perborates, chromates or chromic acid. The soap used to form the grease may be a metal or organic base soap of acids such as fatty acids derived from animal, vegetable, marine and fish oils or synthetic acids or mixtures thereof; various acids including hydrogenated, hydroxy and keto acids are mentioned, and also acids derived from the oxidation of petroleum, and naphthenic, rosin and tall oil acids. Synthetic lubricating oils referred to are the polymerized olefins, or organic esters such as 2-ethylhexyl sebacate, dioctyl phthalate and trioctyl phosphate, and polymeric tetra-hydrofurans; natural oils such as castor or lard oil may be mixed with the mineral or synthetic lubricating oil. Optional ingredients of the composition mentioned are stabilizing agents such as alkylene glycol or thioglycol polymers and their mono-ester and ether derivatives; additional soaps or salts; oxidation inhibitors such as various amines and phenols; corrosion inhibitors such as primary amines containing at least 6 carbon atoms and heterocyclic nitrogen compounds; extreme pressure agents such as phosphorous esters, aromatic sulphur and selenium compounds; sulphurized fatty oils or esters; sulphurized long-chain olefins; sulphurized or phosphorized compounds; chlorinated hydrocarbons and chlorinated esters; antiwear agents such as urea or thiourea derivatives; anti-foaming agents, viscosity index improvers, oiliness agents and pour point depressors. Specific examples of all these compounds are mentioned.
GB18474/49A 1948-07-26 1949-07-13 Improvements in and relating to lubricating grease Expired GB669206A (en)

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GB18474/49A Expired GB669206A (en) 1948-07-26 1949-07-13 Improvements in and relating to lubricating grease

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE926680C (en) * 1952-08-25 1955-04-21 Huels Chemische Werke Ag Additives for lubricants
DE926681C (en) * 1952-08-25 1955-04-21 Huels Chemische Werke Ag Additives for lubricants
DE927820C (en) * 1952-08-25 1955-05-16 Huels Chemische Werke Ag Additives for lubricants
DE929384C (en) * 1952-08-25 1955-06-27 Huels Chemische Werke Ag Additives for lubricants
DE1076299B (en) * 1956-08-18 1960-02-25 Basf Ag Lubricating oils
DE1086514B (en) * 1954-10-06 1960-08-04 Prod Chim Ind Et Organiques So N-polyglycol ether derivatives as corrosion protection agents

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE943487C (en) * 1952-06-21 1956-05-24 Deutsche Erdoel Ag Reversible universal grease
DE1075777B (en) * 1956-11-20 1960-02-18 Socony Mobil Oil Company, Inc., New York, N. Y. (V. St. A.) Mineral oil-based lubricating grease with a content of metal soaps of higher fatty acids
DE1128069B (en) * 1959-02-11 1962-04-19 Shell Int Research Grease
NL108694C (en) * 1959-02-11

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE926680C (en) * 1952-08-25 1955-04-21 Huels Chemische Werke Ag Additives for lubricants
DE926681C (en) * 1952-08-25 1955-04-21 Huels Chemische Werke Ag Additives for lubricants
DE927820C (en) * 1952-08-25 1955-05-16 Huels Chemische Werke Ag Additives for lubricants
DE929384C (en) * 1952-08-25 1955-06-27 Huels Chemische Werke Ag Additives for lubricants
DE1086514B (en) * 1954-10-06 1960-08-04 Prod Chim Ind Et Organiques So N-polyglycol ether derivatives as corrosion protection agents
DE1076299B (en) * 1956-08-18 1960-02-25 Basf Ag Lubricating oils

Also Published As

Publication number Publication date
DE832787C (en) 1952-02-28

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