GB601539A - Improvements in or relating to the preparation of n-disubstituted melamines - Google Patents

Improvements in or relating to the preparation of n-disubstituted melamines

Info

Publication number
GB601539A
GB601539A GB24812/45A GB2481245A GB601539A GB 601539 A GB601539 A GB 601539A GB 24812/45 A GB24812/45 A GB 24812/45A GB 2481245 A GB2481245 A GB 2481245A GB 601539 A GB601539 A GB 601539A
Authority
GB
United Kingdom
Prior art keywords
dicyanoguanidine
heating
potassium
melamine
secondary amine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB24812/45A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wyeth Holdings LLC
Original Assignee
American Cyanamid Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by American Cyanamid Co filed Critical American Cyanamid Co
Publication of GB601539A publication Critical patent/GB601539A/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B44DECORATIVE ARTS
    • B44BMACHINES, APPARATUS OR TOOLS FOR ARTISTIC WORK, e.g. FOR SCULPTURING, GUILLOCHING, CARVING, BRANDING, INLAYING
    • B44B3/00Artist's machines or apparatus equipped with tools or work holders moving or able to be controlled substantially two- dimensionally for carving, engraving, or guilloching shallow ornamenting or markings
    • B44B3/06Accessories, e.g. tool or work holders
    • B44B3/063Tool holders
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23BTURNING; BORING
    • B23B27/00Tools for turning or boring machines; Tools of a similar kind in general; Accessories therefor
    • B23B27/14Cutting tools of which the bits or tips or cutting inserts are of special material
    • B23B27/18Cutting tools of which the bits or tips or cutting inserts are of special material with cutting bits or tips or cutting inserts rigidly mounted, e.g. by brazing
    • B23B27/20Cutting tools of which the bits or tips or cutting inserts are of special material with cutting bits or tips or cutting inserts rigidly mounted, e.g. by brazing with diamond bits or cutting inserts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23QDETAILS, COMPONENTS, OR ACCESSORIES FOR MACHINE TOOLS, e.g. ARRANGEMENTS FOR COPYING OR CONTROLLING; MACHINE TOOLS IN GENERAL CHARACTERISED BY THE CONSTRUCTION OF PARTICULAR DETAILS OR COMPONENTS; COMBINATIONS OR ASSOCIATIONS OF METAL-WORKING MACHINES, NOT DIRECTED TO A PARTICULAR RESULT
    • B23Q1/00Members which are comprised in the general build-up of a form of machine, particularly relatively large fixed members
    • B23Q1/25Movable or adjustable work or tool supports
    • B23Q1/44Movable or adjustable work or tool supports using particular mechanisms
    • B23Q1/48Movable or adjustable work or tool supports using particular mechanisms with sliding pairs and rotating pairs
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23QDETAILS, COMPONENTS, OR ACCESSORIES FOR MACHINE TOOLS, e.g. ARRANGEMENTS FOR COPYING OR CONTROLLING; MACHINE TOOLS IN GENERAL CHARACTERISED BY THE CONSTRUCTION OF PARTICULAR DETAILS OR COMPONENTS; COMBINATIONS OR ASSOCIATIONS OF METAL-WORKING MACHINES, NOT DIRECTED TO A PARTICULAR RESULT
    • B23Q17/00Arrangements for observing, indicating or measuring on machine tools
    • B23Q17/24Arrangements for observing, indicating or measuring on machine tools using optics or electromagnetic waves
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B44DECORATIVE ARTS
    • B44BMACHINES, APPARATUS OR TOOLS FOR ARTISTIC WORK, e.g. FOR SCULPTURING, GUILLOCHING, CARVING, BRANDING, INLAYING
    • B44B3/00Artist's machines or apparatus equipped with tools or work holders moving or able to be controlled substantially two- dimensionally for carving, engraving, or guilloching shallow ornamenting or markings
    • B44B3/06Accessories, e.g. tool or work holders
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B44DECORATIVE ARTS
    • B44BMACHINES, APPARATUS OR TOOLS FOR ARTISTIC WORK, e.g. FOR SCULPTURING, GUILLOCHING, CARVING, BRANDING, INLAYING
    • B44B3/00Artist's machines or apparatus equipped with tools or work holders moving or able to be controlled substantially two- dimensionally for carving, engraving, or guilloching shallow ornamenting or markings
    • B44B3/06Accessories, e.g. tool or work holders
    • B44B3/061Tool heads
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B44DECORATIVE ARTS
    • B44BMACHINES, APPARATUS OR TOOLS FOR ARTISTIC WORK, e.g. FOR SCULPTURING, GUILLOCHING, CARVING, BRANDING, INLAYING
    • B44B2700/00Machines, apparatus, tools or accessories for artistic work
    • B44B2700/12Accessories; Tool or work holders

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Phenolic Resins Or Amino Resins (AREA)

Abstract

N1-Di-substituted melamines are prepared by reacting a secondary amine with 1,3-dicyanoguanidine. The secondary amine may have the same or different aliphatic, cycloaliphatic or aromatic radicals. Preferably, the reaction takes place between a mineral acid salt of a secondary amine and an alkali metal salt of 1,3-dicyanoguanidine, for example, by mixing and heating to at least 60 DEG C. In examples: (1) N1-diethyl melamine is obtained by heating diethylamine hydrochloride and mono-potassium 1,3-dicyanoguanidine; (2) N1-dibutyl melamine is obtained by heating dibutylamine hydrochloride and mono-potassium 1,3-dicyanoguanidine; and (3) N1-methyl-N1-phenyl melamine is obtained by heating methylaniline hydrochloride and potassium dicyanoguanidine. Other secondary amines specified are dimethylamine, di-isopropylamine, didodecylamine, dioctadecylamine, dicyclohexylamine, nitro - N - methylanilines, ethylanilines and diphenylamine. 1,3-Dicyanoguanidine is prepared by mixing together dicyandiamide, a water-soluble alkali metal or alkaline earth metal hydroxide in the presence of acetone and then adding cyanogen chloride.
GB24812/45A 1944-09-14 1945-09-25 Improvements in or relating to the preparation of n-disubstituted melamines Expired GB601539A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US601539XA 1944-09-14 1944-09-14

Publications (1)

Publication Number Publication Date
GB601539A true GB601539A (en) 1948-05-07

Family

ID=22027708

Family Applications (1)

Application Number Title Priority Date Filing Date
GB24812/45A Expired GB601539A (en) 1944-09-14 1945-09-25 Improvements in or relating to the preparation of n-disubstituted melamines

Country Status (1)

Country Link
GB (1) GB601539A (en)

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