GB574818A - Cyclical process for the manufacture of titanium dioxide pigments - Google Patents

Cyclical process for the manufacture of titanium dioxide pigments

Info

Publication number
GB574818A
GB574818A GB12506/43A GB1250643A GB574818A GB 574818 A GB574818 A GB 574818A GB 12506/43 A GB12506/43 A GB 12506/43A GB 1250643 A GB1250643 A GB 1250643A GB 574818 A GB574818 A GB 574818A
Authority
GB
United Kingdom
Prior art keywords
iron
solution
titanium
hydrochloric acid
chloride solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB12506/43A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
British Titan Products Co Ltd
Original Assignee
British Titan Products Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by British Titan Products Co Ltd filed Critical British Titan Products Co Ltd
Publication of GB574818A publication Critical patent/GB574818A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B1/00—Preliminary treatment of ores or scrap
    • C22B1/02—Roasting processes
    • C22B1/08—Chloridising roasting
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00—Obtaining refractory metals
    • C22B34/10—Obtaining titanium, zirconium or hafnium
    • C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1204—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 preliminary treatment of ores or scrap to eliminate non- titanium constituents, e.g. iron, without attacking the titanium constituent
    • C22B34/1209—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 preliminary treatment of ores or scrap to eliminate non- titanium constituents, e.g. iron, without attacking the titanium constituent by dry processes, e.g. with selective chlorination of iron or with formation of a titanium bearing slag
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00—Obtaining refractory metals
    • C22B34/10—Obtaining titanium, zirconium or hafnium
    • C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1218—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes
    • C22B34/1222—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes using a halogen containing agent
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00—Obtaining refractory metals
    • C22B34/10—Obtaining titanium, zirconium or hafnium
    • C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1236—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by wet processes, e.g. by leaching
    • C22B34/1259—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by wet processes, e.g. by leaching treatment or purification of titanium containing solutions or liquors or slurries

Abstract

574,818. Treating iron-bearing titanium ores. BRITISH TITAN PRODUCTS CO., Ltd. Aug. 3, 1943, No. 12506. Convention date, Aug. 1, 1942. Drawings to Specification. [Class 1 (iii)] [Also in Group XXXVI] Iron-bearing titanium ores such as ilmenite are treated with hydrochloric acid to bring the bulk of the iron into solution and leave a titanium dioxide concentrate, the latter is chlorinated to form and volatilise titanium tetrachloride, which is brought into solution and hydrolized to obtain hydrated titanium oxide which is calcined and hydrochloric acid for treating fresh ore; whilst the iron chloride solution is reduced and electrolysed to obtain metallic iron and chlorine which is used for chlorinating fresh titanium dioxide concentrate. In the first step elevated temperatures and relatively concentrated hydrochloric acid are used. In the chlorination step, the concentrate is preferably briquetted with carbonaceous material and a binder and ferric chloride passing off with the titanium tetrachloride is separated therefrom and added to the iron chloride solution to be electrolysed. The latter is usually acid and is neutralized before or during the reduction of ferric chloride present to ferrous chloride. Spent electrolyte from the electrolysis step may be used to form the titanium tetrachloride solution, and hydrolysis of the latter be effected in the presence of nuclei. Electrolysis may take place in a diaphragm cell having a carbon anode and iron cathode, using the iron chloride solution as catholyte and calcium chloride solution as anolyte, and current densities of 2-10 amps. per sq. decimetre. Specification 421,308 is referred to.
GB12506/43A 1942-08-01 1943-08-03 Cyclical process for the manufacture of titanium dioxide pigments Expired GB574818A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US574818XA 1942-08-01 1942-08-01

Publications (1)

Publication Number Publication Date
GB574818A true GB574818A (en) 1946-01-22

Family

ID=22010824

Family Applications (1)

Application Number Title Priority Date Filing Date
GB12506/43A Expired GB574818A (en) 1942-08-01 1943-08-03 Cyclical process for the manufacture of titanium dioxide pigments

Country Status (1)

Country Link
GB (1) GB574818A (en)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014008586A1 (en) * 2012-07-12 2014-01-16 Orbite Aluminae Inc. Processes for preparing titanium oxide and various other products
US9023301B2 (en) 2012-01-10 2015-05-05 Orbite Aluminae Inc. Processes for treating red mud
US9181603B2 (en) 2012-03-29 2015-11-10 Orbite Technologies Inc. Processes for treating fly ashes
US9260767B2 (en) 2011-03-18 2016-02-16 Orbite Technologies Inc. Processes for recovering rare earth elements from aluminum-bearing materials
US9353425B2 (en) 2012-09-26 2016-05-31 Orbite Technologies Inc. Processes for preparing alumina and magnesium chloride by HCl leaching of various materials
US9382600B2 (en) 2011-09-16 2016-07-05 Orbite Technologies Inc. Processes for preparing alumina and various other products
US9410227B2 (en) 2011-05-04 2016-08-09 Orbite Technologies Inc. Processes for recovering rare earth elements from various ores
US9534274B2 (en) 2012-11-14 2017-01-03 Orbite Technologies Inc. Methods for purifying aluminium ions

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9260767B2 (en) 2011-03-18 2016-02-16 Orbite Technologies Inc. Processes for recovering rare earth elements from aluminum-bearing materials
US9945009B2 (en) 2011-03-18 2018-04-17 Orbite Technologies Inc. Processes for recovering rare earth elements from aluminum-bearing materials
US9410227B2 (en) 2011-05-04 2016-08-09 Orbite Technologies Inc. Processes for recovering rare earth elements from various ores
US9382600B2 (en) 2011-09-16 2016-07-05 Orbite Technologies Inc. Processes for preparing alumina and various other products
US10174402B2 (en) 2011-09-16 2019-01-08 Orbite Technologies Inc. Processes for preparing alumina and various other products
US9023301B2 (en) 2012-01-10 2015-05-05 Orbite Aluminae Inc. Processes for treating red mud
US9556500B2 (en) 2012-01-10 2017-01-31 Orbite Technologies Inc. Processes for treating red mud
US9181603B2 (en) 2012-03-29 2015-11-10 Orbite Technologies Inc. Processes for treating fly ashes
WO2014008586A1 (en) * 2012-07-12 2014-01-16 Orbite Aluminae Inc. Processes for preparing titanium oxide and various other products
US9290828B2 (en) 2012-07-12 2016-03-22 Orbite Technologies Inc. Processes for preparing titanium oxide and various other products
US9353425B2 (en) 2012-09-26 2016-05-31 Orbite Technologies Inc. Processes for preparing alumina and magnesium chloride by HCl leaching of various materials
US9534274B2 (en) 2012-11-14 2017-01-03 Orbite Technologies Inc. Methods for purifying aluminium ions

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