GB499924A - Improvements in the distillation of pitch and like carbonaceous materials - Google Patents

Improvements in the distillation of pitch and like carbonaceous materials

Info

Publication number
GB499924A
GB499924A GB8831/38A GB883138A GB499924A GB 499924 A GB499924 A GB 499924A GB 8831/38 A GB8831/38 A GB 8831/38A GB 883138 A GB883138 A GB 883138A GB 499924 A GB499924 A GB 499924A
Authority
GB
United Kingdom
Prior art keywords
heated
steam
materials
parts
atomized
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB8831/38A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ruetgers Germany GmbH
Original Assignee
Ruetgerswerke AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ruetgerswerke AG filed Critical Ruetgerswerke AG
Publication of GB499924A publication Critical patent/GB499924A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10CWORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
    • C10C1/00Working-up tar
    • C10C1/04Working-up tar by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Working-Up Tar And Pitch (AREA)

Abstract

<PICT:0499924/III/1> In a process for the recovery of difficulty volatilizable products from pitches, tars, bitumens, coals, resins, waxes &c., of the ; kind in which the initial materials, preferably preheated, are atomized in a current of superheated steam or gas, the atomized materials are mixed with the steam or gas under pressure or vacuum in a locally very limited inlet zone, the length of which does not exceed a few centimetres, so that the materials are heated by the steam &c. only for a fraction of a second, whereupon the mixture is expanded into a non-heated expansion zone maintained at a lower pressure than the inlet zone where the products are cooled to a temperature below that at which decomposition can occur. The reaction temperature may be chosen so that slight decomposition of non - volatile fractions of the initial material takes place, whereby difficultly volatilizable decomposition products are obtained. The initial materials heated in a vessel F are fed through a nozzle D where they are atomized by heated gases passed through a coil A and a vaporizing tube C, the mixture being immediately expanded into a chamber E from which volatile constituents are withdrawn through a line H to condensation apparatus. The distance of the nozzle D from the inlet of the expansion chamber E is about 20 cms. so that with a flow of vapour of 5 metres per second the materials are in contact with the hot gases for 1/25 of a second. In examples: (1) coal-tar pitch was heated to 380 DEG C. and sprayed into a steam-jet heated to 600 DEG C.; 65 per cent viscous oil and 33 per cent pitch of high softening point were obtained; (6) 35 parts coal dispersed in 65 parts tar-oil were heated to 390 DEG C. and sprayed into steam heated to 600 DEG C., and on expansion the temperature of the mixture was reduced to 400 DEG C.; 29 parts residue and 70 parts distillate were obtained. Specification 169,763, [Class 32], is referred to.
GB8831/38A 1938-01-12 1938-03-22 Improvements in the distillation of pitch and like carbonaceous materials Expired GB499924A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE499924X 1938-01-12

Publications (1)

Publication Number Publication Date
GB499924A true GB499924A (en) 1939-01-31

Family

ID=6545541

Family Applications (1)

Application Number Title Priority Date Filing Date
GB8831/38A Expired GB499924A (en) 1938-01-12 1938-03-22 Improvements in the distillation of pitch and like carbonaceous materials

Country Status (1)

Country Link
GB (1) GB499924A (en)

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