GB457679A - Manufacture of azo-dyestuffs - Google Patents

Manufacture of azo-dyestuffs

Info

Publication number
GB457679A
GB457679A GB25933/35A GB2593335A GB457679A GB 457679 A GB457679 A GB 457679A GB 25933/35 A GB25933/35 A GB 25933/35A GB 2593335 A GB2593335 A GB 2593335A GB 457679 A GB457679 A GB 457679A
Authority
GB
United Kingdom
Prior art keywords
sulphone
acid
aminobenzene
methyl
group
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB25933/35A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF Schweiz AG
Original Assignee
Gesellschaft fuer Chemische Industrie in Basel CIBA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Gesellschaft fuer Chemische Industrie in Basel CIBA filed Critical Gesellschaft fuer Chemische Industrie in Basel CIBA
Publication of GB457679A publication Critical patent/GB457679A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Azo dyes; azo dyes, forming upon the material; cellulose esters and ethers, dyeing; acid wool dyes without mordants, dyeing with; printing.--Azo dyes are manufactured by coupling a diazocompound of an amine of the formula <FORM:0457679/IV/1> where R is an alkyl or aralkyl group and in which the p-position to the amino-group does not contain a nitro- or acylamino-group, with a component which contains as the group directing coupling a substituted or unsubstituted amino-group. The products dye animal fibres or cellulose esters and ethers, e.g. acetate artificial silk, yellow to red, blue-red or violet shades, those containing a sulphonic acid group being suitable for dyeing animal fibres, e.g. wool in acid baths, or for printing acetate artificial silk, whilst those free from sulphonic acid groups are suitable for dyeing acetate artificial silk, preferably after being brought into a finely dispersed condition, e.g. by grinding with dispersing agents such as sulphite cellulose lye or the sulphonated residue of the benzaldehyde manufacture. The products are particularly suitable for the production of combination dyeings. Examples describe the production of the following dyestuffs: (1) 1-aminobenzene-2-methyl-sulphone --> N-ethyl-N-p-sulphobenzylaniline; the product yields yellow-orange prints on acetate artificial silk and dyes wool orange shades; (2) 1-aminobenzene-2-methyl-sulphone --> 2-amino-8-naphthol-6-sulphonic acid; the product dyes wool red shades; the diazo-component may be replaced by 1-amino-5-chlorobenzene-2-methyl-sulphone, yielding a somewhat bluer red; (3) 1-aminobenzene-2-benzyl-sulphone --> 2 : 8 : 6-acid; the product dyes wool blue-red shades; (4) 1-aminobenzene-2-methyl-sulphone --> p-cresidine; the product dyes acetate artificial silk golden yellow shades; the diazo-component may be replaced by 1-aminobenzene-2-ethyl-sulphone and the coupling component by dimethylaniline; the dyeings may be diazotized on the fibre and developed, e.g. with 1 - phenyl - 3 - methyl - 5 - pyrazolone, resorcinol, p-cresotinic acid, b -naphthol, 2 : 3-oxynaphthoic acid, ethyl-a - or b - naphthylamine; (5) 1 - aminobenzene - 2 - methyl-sulphone-4-sulphonic acid --> b -naphthylamine; the product dyes wool orange red tints; if as coupling component there is used 2-ethylaminonaphthalene, the product yields blue - red dyeings; (6) 1 - aminobenzene - 2 - methyl-sulphone-4-sulphonic acid --> 2-amino-8-naphthol; the product dyes wool red-violet shades. In a further example: (7) wool is dyed with the product of (2) from a bath containing sodium sulphate and sulphuric acid. Other components specified are: diazo-components: 1-aminobenzene - 2 - propyl-, -butyl-and -chlorobenzyl-sulphones, 1-aminobenzene-2-ethyl- and -benzyl-sulphone-4-sulphonic acids and 1 - amino - 5 - chlorobenzene - 2 - methyl - sulphone-4-sulphonic acid; coupling components: a -naphthylamine, a - and b -naphthylamine-sulphonic acids, ethyl - b - naphthylaminesulphonic acids, aminonaphthols, e.g. 1 : 5-amino-naphthol and its sulphonic acids, N-alkyl and -aryl derivatives of 2 : 8-aminonaphthol and its 6-sulphonic acid, e.g. phenyl - 2 : 8 : 6 - acid, diphenylamine and its sulphonic acids, alkylanilines, e.g. ethylbenzylaniline, aniline, o- and m-toluidine, p-xylidine, 2 : 5-dioxyalkylaminobenzenes, amines which are alkylated or oxyalkylated in the amino-group and also oxyalkylated amines in which the oxy-group is capable of being etherified or esterified. Aminosulphones of the general formula given above are obtainable by reducing 2 : 2<1>-dinitrodiphenyl disulphide or a substitution product thereof, e.g. a halogen substitution product, to the o-nitrothiophenol, converting this into an alkyl or aralkyl thioether, e.g. by the action of an alkyl or aralkyl halide, oxidizing to the corresponding sulphone and reducing the nitro-group. Alternatively, the alkyl halide may be replaced by an a -halogen fatty acid, e.g. chloracetic or a -chloropropionic acid, in which case an additional step of splitting of carbon dioxide is effected after the oxidation to the sulphone. 1 - Aminobenzene - 2 - methyl - sulphone - 4 - sulphonic acid is obtainable by heating the acid sulphate of 1-aminobenzene-2-methyl-sulphone to 190--200 DEG C.
GB25933/35A 1934-09-28 1935-09-18 Manufacture of azo-dyestuffs Expired GB457679A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH457679X 1934-09-28

Publications (1)

Publication Number Publication Date
GB457679A true GB457679A (en) 1936-12-03

Family

ID=4515648

Family Applications (1)

Application Number Title Priority Date Filing Date
GB25933/35A Expired GB457679A (en) 1934-09-28 1935-09-18 Manufacture of azo-dyestuffs

Country Status (1)

Country Link
GB (1) GB457679A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5106960A (en) * 1980-03-28 1992-04-21 Ciba-Geigy Corporation Azo dyes and the production and use thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5106960A (en) * 1980-03-28 1992-04-21 Ciba-Geigy Corporation Azo dyes and the production and use thereof

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