GB2533244A - NMR Sample analysis - Google Patents

NMR Sample analysis Download PDF

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Publication number
GB2533244A
GB2533244A GB1603980.2A GB201603980A GB2533244A GB 2533244 A GB2533244 A GB 2533244A GB 201603980 A GB201603980 A GB 201603980A GB 2533244 A GB2533244 A GB 2533244A
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GB
United Kingdom
Prior art keywords
animal tissue
sample
sample analysis
nmr sample
characteristic data
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB1603980.2A
Other versions
GB2533244B (en
GB201603980D0 (en
Inventor
Williamson David
Kemsley Kate
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Oxford Instruments Industrial Products Ltd
Quadram Institute Bioscience
Original Assignee
Institute of Food Research Ltd
Oxford Instruments Industrial Products Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Institute of Food Research Ltd, Oxford Instruments Industrial Products Ltd filed Critical Institute of Food Research Ltd
Publication of GB201603980D0 publication Critical patent/GB201603980D0/en
Publication of GB2533244A publication Critical patent/GB2533244A/en
Application granted granted Critical
Publication of GB2533244B publication Critical patent/GB2533244B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00—Arrangements or instruments for measuring magnetic variables
    • G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/44—Arrangements or instruments for measuring magnetic variables involving magnetic resonance using nuclear magnetic resonance [NMR]
    • G01R33/46—NMR spectroscopy
    • G01R33/465—NMR spectroscopy applied to biological material, e.g. in vitro testing
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N24/00—Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
    • G01N24/08—Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance

Abstract

A method for identifying animal tissue using a bench top NMR spectrometer with a magnetic field strength between 1.0 and 2.5 Tesla is provided. Triglyceride molecules are dissolved from an animal tissue sample using a solvent to obtain a sample. The sample is then scanned using a bench top NMR spectrometer and the resulting signal is converted into a frequency spectrum. The spectrum is then analysed and characteristic data for the animal tissue is output, wherein said characteristic data indicates the identity of the animal tissue.
GB1603980.2A 2013-09-06 2014-09-05 NMR Sample analysis Active GB2533244B (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GBGB1315962.9A GB201315962D0 (en) 2013-09-06 2013-09-06 NMR sample analysis
PCT/GB2014/052695 WO2015033154A1 (en) 2013-09-06 2014-09-05 Nmr sample analysis

Publications (3)

Publication Number Publication Date
GB201603980D0 GB201603980D0 (en) 2016-04-20
GB2533244A true GB2533244A (en) 2016-06-15
GB2533244B GB2533244B (en) 2021-03-31

Family

ID=49486887

Family Applications (2)

Application Number Title Priority Date Filing Date
GBGB1315962.9A Ceased GB201315962D0 (en) 2013-09-06 2013-09-06 NMR sample analysis
GB1603980.2A Active GB2533244B (en) 2013-09-06 2014-09-05 NMR Sample analysis

Family Applications Before (1)

Application Number Title Priority Date Filing Date
GBGB1315962.9A Ceased GB201315962D0 (en) 2013-09-06 2013-09-06 NMR sample analysis

Country Status (4)

Country Link
DE (1) DE112014004052B4 (en)
GB (2) GB201315962D0 (en)
NZ (1) NZ717872A (en)
WO (1) WO2015033154A1 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102015226151A1 (en) * 2015-12-21 2017-06-22 Robert Bosch Gmbh Using a meter to examine a tooth or dentition
JP7100790B2 (en) * 2018-03-16 2022-07-14 静岡県公立大学法人 Species discrimination method

Non-Patent Citations (17)

* Cited by examiner, † Cited by third party
Title
A. DI LUCCIA, A. SATRIANI, C.M.A. BARONE, P. COLATRUGLIO, S. GIGLI, M. OCCIDENTE, E. TRIVELLONE, A. ZULLO, D. MATASSINO: "Effect of dietary energy content on the intramuscular fat depots and triglyceride composition of river buffalo meat", MEAT SCIENCE, APPLIED SCIENCE PUBLISHERS., vol. 65, no. 4, 1 December 2003 (2003-12-01), pages 1379 - 1389, XP055153563, ISSN: 03091740, DOI: 10.1016/S0309-1740(03)00060-3 *
AL-JOWDER O., ET AL.: "High resolution NMR studies of meat composition and authenticity", MAGNETIC RESONANCE IN FOOD SCIENCE : A VIEW TO THE FUTURE (FIFTH INTERNATIONAL CONFERENCE ON APPLICATIONS OF MAGNETIC RESONANCE IN FOOD SCIENCE WAS HELD AT THE UNIVERSITY OF AVEIRO, PORTUGAL, BETWEEN THE 18TH AND 20TH SEPTEMBER 2000), 18 September 2000 (2000-09-18) - 20 September 2000 (2000-09-20), pages 232 - 238, XP009181303, ISBN: 978-0-85404-870-0 *
ANONYMOUS: "Benchtop NMR breakthrough | News from the Institute of Food Research", 2 May 2013 (2013-05-02), XP055153581, Retrieved from the Internet <URL:http://news.ifr.ac.uk/2013/05/benchtop-nmr-breakthrough/> [retrieved on 20141118] *
ANONYMOUS: "Pulsar, Benchtop NMR for Food Authenticity Screening", OXFORD INSTRUMENTS, 1 October 2013 (2013-10-01), XP055153337, Retrieved from the Internet <URL:http://www.oxford-instruments.com/OxfordInstruments/media/industrial-analysis/magnetic-resonance-pulsar-applications/Pulsar-high-resolution-benchtop-NMR-Meat-Oil-Flyer-Oct-2013.pdf> [retrieved on 20141117] *
ANONYMOUS: "Specification of Meat, Application Note - Pulsar 006", OXFORD INSTRUMENTS, 1 April 2004 (2004-04-01), XP055153332, Retrieved from the Internet <URL:http://www.oxford-instruments.com/OxfordInstruments/media/industrial-analysis/magnetic-resonance-pdfs/Pulsar-Speciation-of-Meat-Application-Note-006.pdf?width=0&height=0&ext=.pdf> [retrieved on 20141117] *
INGER BEATE STANDAL: "Use of NMR spectroscopy in combination with pattern recognition techniques for elucidation of origin and adulteration of foodstuffs, Thesis for the degree of Philosophiae Doctor", 1 June 2009 (2009-06-01), XP055153555, Retrieved from the Internet <URL:http://ntnu.diva-portal.org/smash/get/diva2:232500/FULLTEXT02.pdf> [retrieved on 20141118] *
JEAN-PIERRE RENOU, GUY BIELICKI, CHRISTINE DEPONGE, PIERRE GACHON, DIDIER MICOL, PATRICK RITZ: "Characterization of animal products according to geographic origin and feeding diet using nuclear magnetic resonance and isotope ratio mass spectrometry. Part II: Beef meat", FOOD CHEMISTRY, ELSEVIER SCIENCE, vol. 86, no. 2, 1 June 2004 (2004-06-01), pages 251 - 256, XP055153549, ISSN: 03088146, DOI: 10.1016/j.foodchem.2003.08.021 *
LUNDBOM, J. ; HEIKKINEN, S. ; FIELDING, B. ; HAKKARAINEN, A. ; TASKINEN, M.R. ; LUNDBOM, N.: "PRESS echo time behavior of triglyceride resonances at 1.5T: Detecting @w-3 fatty acids in adipose tissue in vivo", JOURNAL OF MAGNETIC RESONANCE., ACADEMIC PRESS, ORLANDO, FL., US, vol. 201, no. 1, 1 November 2009 (2009-11-01), US, pages 39 - 47, XP026685063, ISSN: 1090-7807, DOI: 10.1016/j.jmr.2009.07.026 *
MADELEINE BONNET, C. DENOYER, J. P. RENOU: "High resolution 13C NMR spectroscopy of rendered animal fats: degree of saturation of fatty acid chains and position on glycerol", INTERNATIONAL JOURNAL OF FOOD SCIENCE AND TECHNOLOGY, vol. 25, no. 4, 1 August 1990 (1990-08-01), pages 399 - 408, XP055153562, ISSN: 09505423, DOI: 10.1111/j.1365-2621.1990.tb01097.x *
MANNINA L., ET AL: "NMR metabolic profiling of organic and aqueous sea bass extracts: Implications in the discrimination of wild and cultured sea bass", TALANTA, ELSEVIER, AMSTERDAM, NL, vol. 77, no. 1, 19 October 2008 (2008-10-19), NL, pages 433 - 444, XP002608836, ISSN: 0039-9140, DOI: 10.1016/j.talanta.2008.07.006 *
MANNINA LUISA; SOBOLEV ANATOLY P.; VIEL STÉPHANE: "Liquid state1H high field NMR in food analysis", PROGRESS IN NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY., PERGAMON PRESS, OXFORD., GB, vol. 66, 1 January 1900 (1900-01-01), GB, pages 1 - 39, XP028937898, ISSN: 0079-6565, DOI: 10.1016/j.pnmrs.2012.02.001 *
MARIT AURSAND, INGER B. STANDAL, ANGELIKA PRAËL, LESLEY MCEVOY, JOE IRVINE, DAVID E. AXELSON: "13 C NMR Pattern Recognition Techniques for the Classification of Atlantic Salmon (Salmo salar L.) According to Their Wild, Farmed, and Geographical Origin", JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, ¬AMERICAN CHEMICAL SOCIETY, BOOKS AND JOURNALS DIVISION|, vol. 57, no. 9, 13 May 2009 (2009-05-13), pages 3444 - 3451, XP055153557, ISSN: 00218561, DOI: 10.1021/jf8039268 *
RAYNA STEFANOVA; STOYAN TOSHKOV; NIKOLA V. VASILEV; NIKOLAY G. VASSILEV; ILKO N. MAREKOV;: "Effect of gamma-ray irradiation on the fatty acid profile of irradiated beef meat", FOOD CHEMISTRY, ELSEVIER LTD., NL, vol. 127, no. 2, 31 December 2010 (2010-12-31), NL, pages 461 - 466, XP028365638, ISSN: 0308-8146, DOI: 10.1016/j.foodchem.2010.12.155 *
ROBERTA MANZANO MARIA, LUIZ ALBERTO COLNAGO, LUCIMARA APARECIDA FORATO, DONALD BOUCHARD: "Fast and Simple Nuclear Magnetic Resonance Method To Measure Conjugated Linoleic Acid in Beef", JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, ¬AMERICAN CHEMICAL SOCIETY, BOOKS AND JOURNALS DIVISION|, vol. 58, no. 11, 9 June 2010 (2010-06-09), pages 6562 - 6564, XP055153545, ISSN: 00218561, DOI: 10.1021/jf100345e *
SERGE REZZI, IVAN GIANI, KÁROLY HÉBERGER, DAVID E. AXELSON, VITTORIO M. MORETTI, FABIANO RENIERO, CLAUDE GUILLOU: "Classification of Gilthead Sea Bream ( Sparus aurata ) from 1 H NMR Lipid Profiling Combined with Principal Component and Linear Discriminant Analysis", JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, ¬AMERICAN CHEMICAL SOCIETY, BOOKS AND JOURNALS DIVISION|, vol. 55, no. 24, 1 November 2007 (2007-11-01), pages 9963 - 9968, XP055153546, ISSN: 00218561, DOI: 10.1021/jf070736g *
SICILIANO CARLO; BELSITO EMILIA; DE MARCO ROSARIA; DI GIOIA MARIA LUISA; LEGGIO ANTONELLA; LIGUORI ANGELO: "Quantitative determination of fatty acid chain composition in pork meat products by high resolution1H NMR spectroscopy", FOOD CHEMISTRY, ELSEVIER LTD., NL, vol. 136, no. 2, 1 January 1900 (1900-01-01), NL, pages 546 - 554, XP028955803, ISSN: 0308-8146, DOI: 10.1016/j.foodchem.2012.08.058 *
VIDAL NATALIA P.; MANZANOS MARIA J.; GOICOECHEA ENCARNACIÓN; GUILLÉN MARIA D.: "Quality of farmed and wild sea bass lipids studied by1H NMR: Usefulness of this technique for differentiation on a qualitative and a quantitative basis", FOOD CHEMISTRY, ELSEVIER LTD., NL, vol. 135, no. 3, 1 January 1900 (1900-01-01), NL, pages 1583 - 1591, XP028935703, ISSN: 0308-8146, DOI: 10.1016/j.foodchem.2012.06.002 *

Also Published As

Publication number Publication date
DE112014004052T5 (en) 2016-06-02
GB2533244B (en) 2021-03-31
NZ717872A (en) 2020-06-26
WO2015033154A1 (en) 2015-03-12
GB201603980D0 (en) 2016-04-20
GB201315962D0 (en) 2013-10-23
DE112014004052B4 (en) 2021-03-18

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