GB2474235A - Detection of fluid-bourne particles - Google Patents

Detection of fluid-bourne particles Download PDF

Info

Publication number
GB2474235A
GB2474235A GB0917444A GB0917444A GB2474235A GB 2474235 A GB2474235 A GB 2474235A GB 0917444 A GB0917444 A GB 0917444A GB 0917444 A GB0917444 A GB 0917444A GB 2474235 A GB2474235 A GB 2474235A
Authority
GB
United Kingdom
Prior art keywords
radiation
fluid
zone
detection zone
reflector
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB0917444A
Other versions
GB2474235B (en
GB0917444D0 (en
Inventor
Paul Henry Kaye
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
University of Hertfordshire
Original Assignee
University of Hertfordshire
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by University of Hertfordshire filed Critical University of Hertfordshire
Priority to GB0917444A priority Critical patent/GB2474235B/en
Publication of GB0917444D0 publication Critical patent/GB0917444D0/en
Publication of GB2474235A publication Critical patent/GB2474235A/en
Application granted granted Critical
Publication of GB2474235B publication Critical patent/GB2474235B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01Arrangements or apparatus for facilitating the optical investigation
    • G01N21/03Cuvette constructions
    • G01N21/05Flow-through cuvettes
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/02Investigating particle size or size distribution
    • G01N15/0205Investigating particle size or size distribution by optical means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/10Investigating individual particles
    • G01N15/14Optical investigation techniques, e.g. flow cytometry
    • G01N15/1434Optical arrangements
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/10Investigating individual particles
    • G01N15/14Optical investigation techniques, e.g. flow cytometry
    • G01N15/1456Optical investigation techniques, e.g. flow cytometry without spatial resolution of the texture or inner structure of the particle, e.g. processing of pulse signals
    • G01N15/1459Optical investigation techniques, e.g. flow cytometry without spatial resolution of the texture or inner structure of the particle, e.g. processing of pulse signals the analysis being performed on a sample stream
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01Arrangements or apparatus for facilitating the optical investigation
    • G01N21/03Cuvette constructions
    • G01N21/0303Optical path conditioning in cuvettes, e.g. windows; adapted optical elements or systems; path modifying or adjustment
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/47Scattering, i.e. diffuse reflection
    • G01N21/49Scattering, i.e. diffuse reflection within a body or fluid
    • G01N21/53Scattering, i.e. diffuse reflection within a body or fluid within a flowing fluid, e.g. smoke
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/47Scattering, i.e. diffuse reflection
    • G01N21/49Scattering, i.e. diffuse reflection within a body or fluid
    • G01N21/53Scattering, i.e. diffuse reflection within a body or fluid within a flowing fluid, e.g. smoke
    • G01N21/532Scattering, i.e. diffuse reflection within a body or fluid within a flowing fluid, e.g. smoke with measurement of scattering and transmission
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/10Investigating individual particles
    • G01N15/14Optical investigation techniques, e.g. flow cytometry
    • G01N2015/1486Counting the particles
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/10Investigating individual particles
    • G01N15/14Optical investigation techniques, e.g. flow cytometry
    • G01N2015/1493Particle size
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01Arrangements or apparatus for facilitating the optical investigation
    • G01N21/03Cuvette constructions
    • G01N21/05Flow-through cuvettes
    • G01N2021/052Tubular type; cavity type; multireflective
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2201/00Features of devices classified in G01N21/00
    • G01N2201/02Mechanical
    • G01N2201/022Casings
    • G01N2201/0221Portable; cableless; compact; hand-held

Landscapes

  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Dispersion Chemistry (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

An apparatus for the detection of a fluid-borne particle in an optically defined detection zone, comprises a scattering chamber 3, a fan 1 for providing a sample of fluid, containing the fluid-borne particle, in the form of a flow through the optically defined detection zone and a laser beam generator 5 for generating a beam of radiation through the optically defined detection zone 5. There is also a first reflector or refractor means 8a, a second reflector or refractor means 8b; a first detector means 11; a second detector means 12 and a means for deriving data from the radiation detected by the first and second detection means.

Description

A Low Cost Apparatus and Method for the Detection of a Fluid-Borne Particle
Field of the Invention
The present invention relates to a low cost apparatus and method for the detection of a fluid-borne particle. It is particularly applicable for the detection of a fluid-borne particle in an optical detection zone.
Background
In many fields of environmental monitoring, workplace monitoring, pollution control, and occupational health monitoring, it is necessary to continuously measure the aerosol content of a local environment. Where real-time high-sensitivity measurements are desired, instruments are used that are capable of measuring the sizes of individual particles at high rates (thousands of particles per second) so that an accurate assessment of both the concentration of particles and their size distribution can be achieved.
The instruments that are commonly used for this purpose are optical particle counters' (OPC). These use an intense light source (usually a laser) to illuminate a narrow column of sample air drawn through a sensing chamber by an electrical air-pump. The air column is sufficiently narrow that the volume of air illuminated by the laser beam -often referred to as the sensing zone -rarely contains more than a single particle, and the pulse of light scattered by this particle as it crosses the laser beam is recorded as a particle count, the magnitude of the pulse being indicative of the particle size according to a calibration function, the calibration function depends on factors such as the laser wavelength and beam power and the solid angular range over which the scattered light from the particle is recorded.
There are many excellent commercial varieties of OPC manufactured by companies such as Met One Instruments (USA), Grimm Aerosol Technik GmbH (Germany), and Casella Measurement Ltd., (UK). In all these instruments, the air-pump provides the necessary suction to draw the ambient air through a narrow sample tube and deliver the resulting column of air through the laser beam. The pump itself must be powerful enough to generate the required pressure drop inside the sensing chamber to draw the external air in through the sample tube. Furthermore, since the pumps are normally required to be protected from particulate contamination in the air, they are generally preceded in the air-flow by a high efficiency particle filter and this too will present a flow impedance which the pump must overcome. These features of conventional OPC's result in several drawbacks; firstly, the pumps used must overcome the pressure drops in the sample tube and particle filter, and this has implications for pump size and current consumption (and, by extension, for battery-life in standalone of hand-held units); secondly, the particle filters need to be periodically replaced (incurring further cost to user); and thirdly, the air sample handling system comprising sample inlet tube, vent tube, interconnecting tubing and filter, etc.), can be relatively complex to manufacture and assemble, with implications for final unit cost.
W02008140816 (UNGER) describes a compact low cost particle sensor wherein the flow of fluid is directed to a detection zone via a series of baffles. The detection zone is basically a detector located directly under the laser beam which collects radiation scattered by particles passing through the beam. The problem with this device is that the detector is not able to distinguish the number or size of particles passing through the, rather large, detection zone. This device is only able to detect that at least one particle has passed through the detection zone, and in this regard it is little more than a portable smoke detector. This device cannot be used to accurately count the number of particles passing through the detection zone There is a need for an apparatus and method of aerosol monitoring, having single particle sensitivity, which requires no air-pump or particle filter, and which is mechanically very simple, thus offering the prospect of manufacture using a small number of parts.
Summary of the Invention
According to a first aspect of the present invention there is provided a detector assembly for the detection of fluid-borne particles comprising a tube through which fluid to be analysed flows in use; means for generating a radiation beam, the radiation beam being directed towards the tube in use, such that fluid to be analysed passes through the radiation beam in use, said tube being transparent to the radiation beam; a detector adapted to detect radiation scattered by a particle passing through the radiation beam.
According to a second aspect of the present invention there is provided an apparatus for the detection of a fluid-borne particle in an optically defined detection zone, the apparatus comprising: i) a scattering chamber; ii) a means for providing a sample of fluid, containing the fluid-borne particle, in the form of a flow through the optically defined detection zone; iii) a means for generating a beam of radiation through the optically defined detection zone; iv) a first reflector or refractor means; v) a second reflector or refractor means; vi) a first detector means; vii) a second detector means; and viii) a means for deriving data from the radiation detected by the first and second detection means wherein the first reflector or refractor means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the optically defined detection zone into the first detector means and wherein the second reflector or refractor means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the optically defined detection zone in to the second detector means.
Preferably the optically defined detection zone comprises a first zone and a second zone wherein the second zone is smaller than the first zone and wherein the second zone is located wholly inside the first zone.
This is particularly advantageous as it provides for the a low cost apparatus for counting and sizing particles which operates by providing an optical rather than physical detection zone in which particles are detected. The optical detection zone allowing not only for particles to be detected but also to be counted and sized accurately. The apparatus being able to operated without the need of a pump to draw a sample through a narrow chamber. Given that there is no pump and that the parts are simple, light and cheap to construct this apparatus provides a low cost hand held device with single particle sensitivity, for the first time.
Preferably the first zone is defined by a first aperture located between the first reflector or refractor means and the first detector means and wherein the second zone is defined by a second aperture located between the second reflector or refractor means and the second detector means.
Preferably the second aperture is smaller than the first aperture.
Preferably the apparatus further comprises focussing means adapted to focus the beam of radiation such that the beam of radiation has an elliptical cross-section. More preferably the major axis of the elliptical cross-section is orthogonal/perpendicular to the direction of fluid flow.
Preferably the beam of radiation is generated using a diode laser.
Preferably the means for providing a sample of fluid in the form of a flow through the optically defined detection zone comprises an open ended tube of a diameter large compared to the optically defined detection zone in the scattering chamber through which fluid can freely flow. By selecting a scattering chamber diameter which is larger than the diameter of the optical sensing zone, the air, or other fluid sample, can freely flow through the scattering chamber. There is therefore no need for the air, or other fluid sample, to be sucked through the scattering chamber as in prior art devices, but whilst still retaining the desired single particle sensitivity without a pump.
Preferably the means for providing a sample of fluid in the form of a flow through the optically defined detection zone comprises a fan. This is advantageous as a flow of air can be provided cheaply and with low weight and low power usage to help draw air, or other fluid sample, through the device when there is no natural air or fluid flow in the environment. Alternatively the apparatus could be "waved" (i.e. moved through the air, for example manually by the user or attached to a moving vehicle) through the air to generate a flow of air or other fluid. Alternatively the apparatus can be placed in an environment wherein the fluid sample will flow through the optically defined detection zone, such as an environment of sample air moving relative to the apparatus by convection.
Preferably the first and second reflector or refractor means comprise mirrors. More preferably the mirrors comprise concave mirrors. This allows the mirrors to be used to not only reflect the scattered radiation towards the detector, but also to focus the radiation so that a greater sample of scattered radiation is detected from the particle.
This is also advantageous as mirrors are much cheaper than lenses to produce, again resulting in a lower cost apparatus. Preferably the mirrors are of the same size and the same curvature.
Preferably the first and second reflector or refractor means are arranged above and below the beam of radiation; more preferably the first and second reflector or refractor means are arranged above and below the plane containing the major axis of the cross-section of the beam of radiation. This is advantageous since the reflector or refractor means being above and below the plane containing the major axis of the cross-section of the beam of radiation means that they can be used to define an optical detection zone that lies entirely within the beam of radiation.
Preferably the first and second reflector means are integrally formed in the scattering chamber. This is advantageous as there are less parts to produce and producing less parts is cheaper resulting in a lower cost apparatus.
Preferably the scattering chamber is formed from an injection moulded plastics material. This is advantageous as injection moulding of plastics is a cheap process to run to mass produce identical items, resulting in a lower cost apparatus.
Preferably a first and second concave surface are formed integrally within the scattering chamber.
Preferably the first and second concave surfaces are provided with a reflective material to form the first and second reflector or refractor means. This is advantageous as the mirrors are formed internally to the scattering chamber, in the correct positions, in a single step and coated with a reflective material. This results in a lower cost apparatus due to reduced parts and also because the mirrors are automatically positioned correctly.
According to a third aspect of the present invention there is provided a method for the detection of a fluid-borne particle in an optically defined detection zone, the method comprising: i) providing a sample of fluid, containing the fluid-borne particle, in the form of a flow through the optically defined detection zone; ii) directing a beam of radiation that illuminates the optically defined detection zone and with uniform intensity of radiation; iii) detecting radiation scattered by the fluid-borne particle as it passes through the beam of radiation in the optically defined detection zone.
Preferably the method employs an apparatus for the detection of a fluid-borne particle in an optically defined detection zone, the apparatus comprising: i) a scattering chamber; ii) a means for providing a sample of fluid, comprising the fluid-borne particle, in the form of a flow through the optically defined detection zone; iii) a means for generating a beam of radiation through the optically defined detection zone; iv) a first reflector or refractor means; v) a second reflector or refractor means; vi) a first detector means; vii) a second detector means; and viii) a means for deriving data from the radiation detected by the first and second detection means.
wherein the first reflector or refractor means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the optically defined detection zone into the first detector means and wherein the second reflector or refractor means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the optically defined detection zone in to the second detector means.
According to a fourth aspect of the present invention there is provided a method for the for the detection of a fluid-borne particle in an optically defined detection zone, the method comprising: i) providing an apparatus having; a scattering chamber, a first reflector or refractor means, a second reflector or refractor means, a first detector means, and a second detector means; ii) providing a sample of fluid in the form of a flow through the optically defined detection zone; iii) directing a beam of radiation that illuminates the optically defined detection zone with uniform intensity of radiation; and iv) deriving data from the radiation detected by the first and second detection means; wherein the first reflector or refractor means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the optically defined detection zone into the first detector means and wherein the second reflector or refractor means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the optically defined detection zone in to the second detector means.
According to a fifth aspect of the present invention there is provided a method for the for the detection of a fluid-borne particle in an optically defined detection zone, the method comprising: i) providing an apparatus as claimed in any of claims 1 to 15 ii) providing a sample of fluid in the form of a flow through the optically defined detection zone; iii) directing a beam of radiation that illuminates the optically defined detection zone with uniform intensity of radiation; and iv) deriving data from the radiation detected by the first and second detection means.
The present invention seeks to provide a method of aerosol monitoring (having single particle sensitivity) which requires no air-pump or particle filter, and which is mechanically very simple, thus offering the prospect of manufacture using a small number of injection-moulded plastic parts. The air-movement may be achieved using a small electrical fan (far lower current consumption than a rotary-vane or diaphragm air-pump), by exploiting the natural movement of the ambient air (e.g.: wind, convection flow, etc.), or by simply moving the sensor unit itself through the air by hand or by attaching to a moving vehicle (car, train, aircraft, etc).
The present invention is based on the principle of optically defining a detection zone rather than mechanically defining the zone as in conventional OPCs. As mentioned above, OPCs confine the sample airflow to a narrow column, typically -1mm in diameter, which is directed through a narrow ribbon-shaped laser beam such that the intersection between the beam and the airflow -the detection zone -is sufficiently small that it very rarely contains more than a single particle even when measuring high-concentration aerosols. Avoiding particle coincidences' where two or more particles occupy the detection zone at any instant is crucial to obtaining unbiased aerosol size and concentration data.
In the present Invention, the sample air does not pass through a narrow inlet tube as in conventional OPCs, but instead passes through a far wider space that may or may not have cylindrical tube-like geometry. The particles carried by the air moving though this space are not constrained to move in single file by any mechanical tube or other device. The single-particle detection zone is instead defined by suitable optical components.
Brief Description of the Drawings
A preferred embodiment of the present invention will now be more particularly described, by way of example only, with reference to the accompanying drawings, wherein: Figure 1 shows a cross-sectional view of the particle detection apparatus according to a first embodiment; Figure 2 shows a side perspective view of the particle detection apparatus inside the scattering chamber; Figure 3 shows a graphical display of the first and second detector responses of a particle passing through the first and second zones of the optical detection zone; and Figure 4 shows a cross-sectional view of the particle detection apparatus according to a second embodiment.
Description of the Preferred Embodiments
A preferred embodiment of the present invention is shown in Figure 1. In this embodiment, a small low-power electrical fan 1 causes particle-laden ambient air 2 to move through a scattering chamber 3 at a desired rate. The fan, in one alternative, is of a type commonly used to cool computer microprocessors, requiring a current of only a few milliamps; far less than the tens-of-milliamp currents required by conventional OPC air-pumps. The scattering chamber 3 has end-caps 4 that do not restrict the airflow but act as light baffles to prevent entry of ambient daylight or room-light. An alternative arrangement can be seen in Figure 4.
A beam of radiation from a continuous-wave laser 5 traverses the inside of the scattering chamber. The beam of radiation is configured using lenses and other optical components 6 to have a narrow elliptical cross-section with the major axis of the beam of radiation lying perpendicular to the direction of the air flow in the scattering chamber.
Depending on the particulate concentration in the air, the beam of radiation may illuminate many particles simultaneously that all happen to be traversing at different points along the beam path. Finally, the beam of radiation exits the scattering chamber 3 and is absorbed in some form of beam-dump 7.
Above and below the beam of radiation on the opposite side of the scattering chamber 3 to the beam entry point are positioned first and second optical mirrors 8a, 8b having concave spherical surfaces. The first and second optical mirrors 8a, 8b are of the same size and are of the same curvature. Light scattered by a particle passing through a small region of the beam of radiation will be reflected by the first mirror 8a back across the scattering chamber and through apertures 9, and reflected by mirror 8b across to aperture 10, finally to fall onto respective first and second optical detectors 11, 12. The apertures 9, 10 are critical to the operation in one embodiment of the invention as they optically define the required detection zone as shown in Figure 2.
The first aperture 9 has a diameter such than when projected back via the mirror and onto the beam of radiation forms an elliptical field-of-view 14. This field-of-view is smaller than the width of the beam of radiation so as to minimise the effects of intensity variations across the beam of radiation resulting from the Gaussian beam intensity profile common in such laser beams. Any particle passing through this field-of-view will cause light to fall onto the detector 11. In itself, the resulting detector signal can be used to register the presence of a particle. However, it cannot be used to size the particle because of so-called edge effects', i.e: light scattered by a particle passing through the edge of the field-of-view will suffer some vignetting of the rays collected by the mirror, resulting in a lower signal on the detector 11 and the under-sizing of the particle. The second mirror-aperture assembly overcomes this.
The second aperture 10 is smaller than the first so as to project a field-of-view 16 that lies entirely within the first field-of-view 14, as in Figure 2. This field-of-view is sufficiently small that the maximum intensity variation across it resulting from the, normally, Gaussian beam intensity profile is acceptable, typically <5%. It is only particles passing through this well-defined region of space of the smaller field-of-view 16 that will be deemed valid' particles in particle counting and sizing determination.
Typically for normal ground level applications (i.e. in the vicinity of the ground at low altitudes rather than at high altitudes) the first aperture 9 is around 400pm and the second aperture lOis between 200 and 250im.
In operation, therefore, a particle traversing the beam along trajectory A will not be seen' by either optical detector 11 or 12. A particle on trajectory B will be detected by detector 11 but not by detector 12, and will therefore be ignored. A particle on trajectory C, however, will be detected simultaneously by both detector 11 and detector 12, and will be recorded as a single valid particle, as illustrated in Figure 3. Edge effects caused by a particle traversing the edge of field-of-view 16 are unimportant as the signal used to infer particle size is not that from detector 12, which will suffer edge effects, but instead that from detector 11, which since the particle is well away from its boundary, will not suffer edge effects. Typically for normal ground level applications the particles being detected are in the size range of around 0.5 to 1 0im in diameter.
The concentration of particles in the aerosol may be computed using the product of the air velocity through the laser beam and the cross-sectional area of field-of-view 16.
This velocity may be determined from a knowledge of the beam-depth, being the minor axis of its elliptical beam cross-section, and the time-of-flight of the particle through the beam, as measured from the duration of the electrical signal from detector 11.
Typically for normal ground level applications the minor axis of the elliptical cross-section of the beam of radiation is around 100im and the major axis is around 2mm.
The maximum measurable particulate concentration will be reached when the probability of more than one particle being within field-of-view 16 reaches an unacceptable level, typically -2% maximum, or when there is a particle within field-of- view 16 at the same instant as a particle outside of field-of-view 16 but within field-of-view 14. The beam depth and detector fields-of-view are selected such that this would not occur for concentrations less than typically several thousand particles per millilitre of air.
The apparatus as described offers several advantages over conventional OPCs; * Mechanical simplicity. The absence of internal pipework, filters, and tubing common in conventional OPC units means that the invention could be fabricated at a low manufacturing cost, especially if specialist plastic injection moulded parts (including mirrored surfaces) were employed. In such a case, the scattering chamber 3 comprises two semi-cylindrical parts, the first part with integral first and second mirrored surfaces 8a, 8b and the second part with first and second precision apertures 9 and 10. The integral first and second mirrored surfaces 8a, 8b are formed by injection moulding the scattering chamber 3 with integral first and second concave surfaces which are then provided with a coating of a reflective material.
* The air fan 1 would be capable of moving large volumes of air, required in efficient ambient monitoring, with very low power consumption, since it would be operating against minimal pressure drop. This could significantly extend the battery life of a standalone or hand-held unit compared to that in a conventional OPC with comparable sample air flow-rate. Indeed, the fan would not be necessary at all in some cases. For example, where the airflow through the sensor unit was generated by movement of the unit itself through the air, such as waving' a hand-held unit at arm's length, in which case, the end-caps 3 would be replaced by a low flow impedance light block such as counter-aligned opaque louvers 17, as in the embodiment shown in Figure 4. Such a no moving parts' implementation of the invention would be not only be even cheaper to manufacture than the fan-assisted version of the invention but would also offer improved reliability, it having no moving parts to wear out.
* In addition as no pump is required, the scattering chamber 3 does not need to be air-tight. In conventional OPC devices where a pump is required to suck the air through the narrow mechanically defined detection zone, the scattering chamber 3 needs to be air-tight. The scattering chamber needs to be air-tight, because the air pressure or vacuum drop required to cause the air to flow through the narrow mechanically defined detection zone is significant. In the present invention there is no air pressure or vacuum drop needed as the scattering chamber 3 is large and the detection zone is defined optically rather than mechanically the air-tightness is not critical. This means that the scattering chamber 3 can be formed from a plastics material rather than a metal material. This allows for a cheaper and lighter apparatus to be constructed.
* Further in addition, if a fan is employed the fan is located below the detection zone such that any particles depositing on the fan blades have already been detected.
* The apparatus would require no periodic replacement of internal filter units, making it more suitable than conventional OPCs in remote or hostile monitoring environments where manual filter replacement is undesirable on grounds of inaccessibility or safety hazard.
In an alternative embodiment of the present invention instead of the radiation scattered by a particle being reflected by the first and second mirrors through respective first and second apertures and into the respective first and second detectors, the scattering chamber 3 is provided with first and second apertures through which radiation exits the scattering chamber 3 which is then focussed into respective first and second detectors by the use of respective first and second lenses. In this embodiment, again, the first and second apertures are of different sizes and correlate to form inner and outer zones of an optical detection zone.

Claims (21)

  1. CLAIMS: 1. An apparatus for the detection of a fluid-borne particle in an optically defined detection zone, the apparatus comprising: i) a scattering chamber; ii) a means for providing a sample of fluid, containing the fluid-borne particle, in the form of a flow through the optically defined detection zone; iii) a means for generating a beam of radiation through the optically defined detection zone; iv) a first reflector or refractor means; v) a second reflector or refractor means; vi) a first detector means; vii) a second detector means; and viii) a means for deriving data from the radiation detected by the first and 0) second detection means (\J wherein the first reflector or refractor means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the 0) 20 optically defined detection zone into the first detector means and wherein the second 0 reflector or refractor means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the optically defined detection zone in to the second detector means.
  2. 2. An apparatus as claimed in claim 1 wherein the optically defined detection zone comprises a first zone and a second zone wherein the second zone is smaller than the first zone and wherein the second zone is located wholly inside the first zone.
  3. 3. An apparatus as claimed in claim 2 wherein the first zone is defined by a first aperture located between the first reflector or refractor means and the first detector means and wherein the second zone is defined by a second aperture located between the second reflector or refractor means and the second detector means.
  4. 4. An apparatus as claimed in claim 3 wherein the second aperture is smaller than the first aperture.
  5. 5. An apparatus as claimed in any preceding claim, wherein the apparatus further comprises focussing means adapted to focus the beam of radiation such that the beam of radiation has an elliptical cross-section.
  6. 6. An apparatus as claimed in Claim 5, wherein the major axis of the elliptical cross-section is orthogonal/perpendicular to the direction of fluid flow.
  7. 7. An apparatus as claimed in any preceding claim wherein the beam of radiation is generated using a diode laser.
  8. 8. An apparatus as claimed in any preceding claim wherein the means for providing a sample of fluid in the form of a flow through the optically defined detection zone comprises an open ended tube of a diameter larger than the optically defined detection zone in the scattering chamber through which fluid can freely flow.
  9. 9. An apparatus as claimed in any preceding claim wherein the means for Q providing a sample of fluid in the form of a flow through the optically defined detection (\J zone comprises a fan.
  10. 10. An apparatus as claimed in any preceding claim wherein the first and second Q reflector or refractor means comprise mirrors.
  11. 11. An apparatus as claimed in claim 10, wherein the mirrors comprise concave mirrors.
  12. 12. An apparatus as claimed in any preceding claim wherein the first and second reflector or refractor means are arranged above and below the beam of radiation.
  13. 13. An apparatus as claimed in Claim 12 when dependent on Claim 5, wherein the first and second reflector or refractor means are arranged above and below the plane containing the major axis of the cross-section of the beam of radiation.
  14. 14. An apparatus as claimed in any preceding claim wherein the first and second reflector means are integrally formed in the scattering chamber.
  15. 15. An apparatus as claimed in any preceding claim wherein the scattering chamber is formed from an injection moulded plastics material.
  16. 16. An apparatus as claimed in any preceding claim wherein a first and second concave surface are formed integrally within the scattering chamber.
  17. 17. An apparatus as claimed in claim 16, wherein the first and second concave surfaces are provided with a reflective material to form the first and second reflector or refractor means.
  18. 18. A method for the for the detection of a fluid-borne particle in an optically defined detection zone, the method comprising: i) providing a sample of fluid, containing the fluid-borne particle, in the form of a flow through the optically defined detection zone; ii) directing a beam of radiation that illuminates the optically defined O*) detection zone with uniform intensity of radiation; and Q iii) detecting radiation scattered by the fluid-borne particle as it passes through the beam of radiation in the optically defined detection zone.
  19. 19. A method for the for the detection of a fluid-borne particle in an optically defined Q detection zone, the method comprising: i) providing an apparatus having; a scattering chamber, a first reflector or refractor means, a second reflector or refractor means, a first detector means, and a second detector means; ii) providing a sample of fluid in the form of a flow through the optically defined detection zone; iii) directing a beam of radiation that illuminates the optically defined detection zone with uniform intensity of radiation; and iv) deriving data from the radiation detected by the first and second detection means; wherein the first reflector or refractor means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the optically defined detection zone into the first detector means and wherein the second reflector or refractor means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the optically defined detection zone in to the second detector means.
  20. 20. A method for the for the detection of a fluid-borne particle in an optically defined detection zone, the method comprising: i) providing an apparatus as claimed in any of claims 1 to 15 ii) providing a sample of fluid in the form of a flow through the optically defined detection zone; iii) directing a beam of radiation that illuminates the optically defined detection zone with uniform intensity of radiation; and iv) deriving data from the radiation detected by the first and second detection means.
  21. 21. An apparatus or method substantially as hereinbefore described with reference to any suitable combination of the accompanying figures. a) (\J a) 20Amendments to the claims have been filed as follows CLAIMS: 1. An apparatus for the detection of a fluid-borne particle in an optically defined detection zone, the apparatus comprising: i) a scattering chamber; ii) a means for providing a sample of fluid, containing the fluid-borne particle, in the form of a flow through the optically defined detection zone; iii) a means for generating a beam of radiation through the optically defined detection zone; iv) a first reflector means; v) a second reflector means; vi) a first detector means; vii) a second detector means; and viii) a means for deriving data from the radiation detected by the first and second detection means wherein the first reflector means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the optically defined detection zone into the first detector means and wherein the second reflector means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the optically defined detection zone in to the second detector means and wherein the optically defined detection zone comprises a first zone and a second zone wherein the second zone is smaller than the first zone and wherein the second zone is located wholly inside the first zone.2. An apparatus as claimed in claim 1 wherein the first zone is defined by a first aperture located between the first reflector means and the first detector means and wherein the second zone is defined by a second aperture located between the second *ê..* 30 reflector means and the second detector means. * ** * S **: 3. An apparatus as claimed in claim 2 wherein the second aperture is smaller than the first aperture.4. An apparatus as claimed in any preceding claim, wherein the apparatus further comprises focussing means adapted to focus the beam of radiation such that the beam of radiation has an elliptical cross-section.5. An apparatus as claimed in Claim 4, wherein the major axis of the elliptical cross-section is orthogonal/perpendicular to the direction of fluid flow.6. An apparatus as claimed in any preceding claim wherein the beam of radiation is generated using a diode laser.7. An apparatus as claimed in any preceding claim wherein the means for providing a sample of fluid in the form of a flow through the optically defined detection zone comprises an open ended tube of a diameter larger than the optically defined detection zone in the scattering chamber through which fluid can freely flow.8. An apparatus as claimed in any preceding claim wherein the means for providing a sample of fluid in the form of a flow through the optically defined detection zone comprises a fan.9. An apparatus as claimed in any preceding claim wherein the first and second reflector means comprise mirrors.10. An apparatus as claimed in claim 9, wherein the mirrors comprise concave mirrors. * S11. An apparatus as claimed in any preceding claim wherein the first and second *S*...* * reflector means are arranged above and below the beam of radiation. *S..12. An apparatus as claimed in Claim 11 when dependent on Claim 4, wherein the **5...* 30 first and second reflector means are arranged above and below the plane containing the major axis of the cross-section of the beam of radiation. * *5 S. ** *: 13. An apparatus as claimed in any preceding claim wherein the first and second reflector means are integrally formed in the scattering chamber.S14. An apparatus as claimed in any preceding claim wherein the scattering chamber is formed from an injection moulded plastics material.15. An apparatus as claimed in any preceding claim wherein a first and second concave surface are formed integrally within the scattering chamber.16. An apparatus as claimed in claim 15, wherein the first and second concave surfaces are provided with a reflective material to form the first and second reflector means.18. A method for the for the detection of a fluid-borne particle in an optically defined detection zone, the method comprising: i) providing an apparatus having; a scattering chamber, a first reflector means, a second reflector means, a first detector means, and a second detector means; ii) providing a sample of fluid in the form of a flow through the optically defined detection zone; iii) directing a beam of radiation that illuminates the optically defined detection zone with uniform intensity of radiation; and iv) deriving data from the radiation detected by the first and second detection means; wherein the first reflector means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of radiation in the optically defined detection zone into the first detector means and wherein the second reflector means is adapted to direct radiation scattered from the fluid borne particle passing through the beam of **S...* * radiation in the optically defined detection zone in to the second detector means and **. wherein the optically defined detection zone comprises a first zone and a second zone * * IS..wherein the second zone is smaller than the first zone and wherein the second zone is IIS...* 30 located wholly inside the first zone. * S. * S * *.20. A method for the for the detection of a fluid-borne particle in an optically defined detection zone, the method comprising: i) providing an apparatus as claimed in any of claims 1 to 15 ii) providing a sample of fluid in the form of a flow through the optically defined detection zone; iii) directing a beam of radiation that illuminates the optically defined detection zone with uniform intensity of radiation; and iv) deriving data from the radiation detected by the first and second detection means.21. An apparatus or method substantially as hereinbefore described with reference to any suitable combination of the accompanying figures. * * **.*S * * * *..* * I...S*SSs.. * S * ** * * * * Ss ** * * *S * *.
GB0917444A 2009-10-06 2009-10-06 A low cost apparatus and method for the detection of a fluid- borne particle Active GB2474235B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB0917444A GB2474235B (en) 2009-10-06 2009-10-06 A low cost apparatus and method for the detection of a fluid- borne particle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB0917444A GB2474235B (en) 2009-10-06 2009-10-06 A low cost apparatus and method for the detection of a fluid- borne particle

Publications (3)

Publication Number Publication Date
GB0917444D0 GB0917444D0 (en) 2009-11-18
GB2474235A true GB2474235A (en) 2011-04-13
GB2474235B GB2474235B (en) 2013-09-25

Family

ID=41393882

Family Applications (1)

Application Number Title Priority Date Filing Date
GB0917444A Active GB2474235B (en) 2009-10-06 2009-10-06 A low cost apparatus and method for the detection of a fluid- borne particle

Country Status (1)

Country Link
GB (1) GB2474235B (en)

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102012201423A1 (en) 2012-02-01 2013-08-01 Siemens Aktiengesellschaft Arrangement for the detection of particles
CN104316444A (en) * 2014-11-11 2015-01-28 邦达诚科技(常州)有限公司 Domestic air quality detection device
WO2017102545A1 (en) * 2015-12-16 2017-06-22 Valeo Schalter Und Sensoren Gmbh Fine dust sensor for a motor vehicle, motor vehicle, and method for determining a fine dust concentration
FR3060748A1 (en) * 2016-12-20 2018-06-22 Valeo Systemes Thermiques DEVICE FOR DETECTING PARTICULATE MATTER IN AN AIR FLOW FOR A MOTOR VEHICLE
CN109668810A (en) * 2017-10-17 2019-04-23 重庆梅安森科技股份有限公司 A kind of mining dust concentration sensor
US10352844B2 (en) 2013-03-15 2019-07-16 Particles Plus, Inc. Multiple particle sensors in a particle counter
US10900894B2 (en) 2015-04-14 2021-01-26 Alphasense Limited Optical particle counter
US10983040B2 (en) 2013-03-15 2021-04-20 Particles Plus, Inc. Particle counter with integrated bootloader
US11579072B2 (en) 2013-03-15 2023-02-14 Particles Plus, Inc. Personal air quality monitoring system
US11835443B2 (en) 2014-04-30 2023-12-05 Particles Plus, Inc. Real time monitoring of particle count data
US11988591B2 (en) 2020-07-01 2024-05-21 Particles Plus, Inc. Modular optical particle counter sensor and apparatus

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4662742A (en) * 1985-05-10 1987-05-05 Becton, Dickinson And Company Scatter/fluorescene beam splitter in a flow cytometry apparatus
EP0361503A1 (en) * 1988-09-30 1990-04-04 Toa Medical Electronics Co., Ltd. Particle analyzing apparatus and method for determining nuclear shift index
US5467189A (en) * 1993-01-22 1995-11-14 Venturedyne, Ltd. Improved particle sensor and method for assaying a particle
US5870190A (en) * 1997-11-25 1999-02-09 Venturedyne, Ltd. Particle sensor and related method offering improved particle discrimination
WO2005001436A1 (en) * 2003-06-26 2005-01-06 The Secretary Of State For Defence Improvements to fluid borne particle analysers
US20050021244A1 (en) * 2002-07-17 2005-01-27 Particle Sizing Systems, Inc. Sensors and methods for high-sensitivity optical particle counting and sizing
US7113266B1 (en) * 2005-03-30 2006-09-26 Beckman Coulter, Inc. Flow cytometer for differentiating small particles in suspension
WO2008140816A1 (en) * 2007-05-12 2008-11-20 Unger Roger L Compact, low cost particle sensor
GB2456671A (en) * 2008-01-25 2009-07-29 Secr Defence Detection of shape, size and fluorescence properties of fluid borne particles

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4662742A (en) * 1985-05-10 1987-05-05 Becton, Dickinson And Company Scatter/fluorescene beam splitter in a flow cytometry apparatus
EP0361503A1 (en) * 1988-09-30 1990-04-04 Toa Medical Electronics Co., Ltd. Particle analyzing apparatus and method for determining nuclear shift index
US5467189A (en) * 1993-01-22 1995-11-14 Venturedyne, Ltd. Improved particle sensor and method for assaying a particle
US5870190A (en) * 1997-11-25 1999-02-09 Venturedyne, Ltd. Particle sensor and related method offering improved particle discrimination
US20050021244A1 (en) * 2002-07-17 2005-01-27 Particle Sizing Systems, Inc. Sensors and methods for high-sensitivity optical particle counting and sizing
WO2005001436A1 (en) * 2003-06-26 2005-01-06 The Secretary Of State For Defence Improvements to fluid borne particle analysers
US7113266B1 (en) * 2005-03-30 2006-09-26 Beckman Coulter, Inc. Flow cytometer for differentiating small particles in suspension
WO2008140816A1 (en) * 2007-05-12 2008-11-20 Unger Roger L Compact, low cost particle sensor
GB2456671A (en) * 2008-01-25 2009-07-29 Secr Defence Detection of shape, size and fluorescence properties of fluid borne particles

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013113679A1 (en) 2012-02-01 2013-08-08 Siemens Aktiengesellschaft Arrangement for detecting particles
DE102012201423A1 (en) 2012-02-01 2013-08-01 Siemens Aktiengesellschaft Arrangement for the detection of particles
US11519842B2 (en) 2013-03-15 2022-12-06 Particles Plus, Inc. Multiple particle sensors in a particle counter
US11913869B2 (en) 2013-03-15 2024-02-27 Particles Plus, Inc. Personal air quality monitoring system
US11579072B2 (en) 2013-03-15 2023-02-14 Particles Plus, Inc. Personal air quality monitoring system
US10352844B2 (en) 2013-03-15 2019-07-16 Particles Plus, Inc. Multiple particle sensors in a particle counter
US10983040B2 (en) 2013-03-15 2021-04-20 Particles Plus, Inc. Particle counter with integrated bootloader
US11169077B2 (en) 2013-03-15 2021-11-09 Particles Plus, Inc. Personal air quality monitoring system
US11846581B2 (en) 2014-04-30 2023-12-19 Particles Plus, Inc. Instrument networking for optical particle counters
US11835443B2 (en) 2014-04-30 2023-12-05 Particles Plus, Inc. Real time monitoring of particle count data
CN104316444A (en) * 2014-11-11 2015-01-28 邦达诚科技(常州)有限公司 Domestic air quality detection device
US10900894B2 (en) 2015-04-14 2021-01-26 Alphasense Limited Optical particle counter
WO2017102545A1 (en) * 2015-12-16 2017-06-22 Valeo Schalter Und Sensoren Gmbh Fine dust sensor for a motor vehicle, motor vehicle, and method for determining a fine dust concentration
WO2018115620A1 (en) * 2016-12-20 2018-06-28 Valeo Systemes Thermiques Device for detecting particulate matter in an airflow for a motor vehicle
FR3060748A1 (en) * 2016-12-20 2018-06-22 Valeo Systemes Thermiques DEVICE FOR DETECTING PARTICULATE MATTER IN AN AIR FLOW FOR A MOTOR VEHICLE
CN109668810A (en) * 2017-10-17 2019-04-23 重庆梅安森科技股份有限公司 A kind of mining dust concentration sensor
US11988591B2 (en) 2020-07-01 2024-05-21 Particles Plus, Inc. Modular optical particle counter sensor and apparatus

Also Published As

Publication number Publication date
GB2474235B (en) 2013-09-25
GB0917444D0 (en) 2009-11-18

Similar Documents

Publication Publication Date Title
EP2633282B1 (en) An improved low cost apparatus and method for the detection of a fluid-borne particle
GB2474235A (en) Detection of fluid-bourne particles
EP2145171B1 (en) Compact, low cost particle sensor
US9995667B2 (en) Portable device for detecting and measuring particles entrained in the air
TWI276011B (en) Improvements relating to smoke detectors particularly ducted smoke detectors
US6431014B1 (en) High accuracy aerosol impactor and monitor
US6639671B1 (en) Wide-range particle counter
USRE37353E1 (en) Particle sensor with variable-speed blower
US8534116B2 (en) Size segregated aerosol mass concentration measurement with inlet conditioners and multiple detectors
JP6126217B2 (en) Sensor and method for measuring particles in a medium
US20200011779A1 (en) Highly integrated optical particle counter (opc)
ES2790664T3 (en) System and method for converting aerosol particle optical diameters into mobility and aerodynamic diameters
JP5443787B2 (en) A device that counts fibers in the air with high accuracy
US20150355084A1 (en) Optimizing analysis and identification of particulate matter
WO2019147590A1 (en) Bioaerosol particle detector
US11360015B2 (en) Sensor for measuring the concentration of particles in air
KR20190076438A (en) Dust sensor
US20200103334A1 (en) Miniaturized optical particle detector
KR20200033619A (en) Sensor assembly for particulate matter
WO2019060984A1 (en) System, apparatus, and method for monitoring air quality
KR20180041023A (en) Dust sensor and operating method thereof
WO2012018869A1 (en) Particle counter with vertical-cavity surface-emitting laser
Kaye A low-cost apparatus and method for the detection of a fluid-borne particle.
CN108120659A (en) A kind of particle concentration detecting system and method having from zero calibration
Kaye et al. An improved low-cost apparatus and method for the detection of a fluid-borne particle

Legal Events

Date Code Title Description
732E Amendments to the register in respect of changes of name or changes affecting rights (sect. 32/1977)

Free format text: REGISTERED BETWEEN 20130815 AND 20130821

732E Amendments to the register in respect of changes of name or changes affecting rights (sect. 32/1977)

Free format text: REGISTERED BETWEEN 20171214 AND 20171222