GB2459570A - Hardcoating bore and seat face of gate valve - Google Patents
Hardcoating bore and seat face of gate valve Download PDFInfo
- Publication number
- GB2459570A GB2459570A GB0907490A GB0907490A GB2459570A GB 2459570 A GB2459570 A GB 2459570A GB 0907490 A GB0907490 A GB 0907490A GB 0907490 A GB0907490 A GB 0907490A GB 2459570 A GB2459570 A GB 2459570A
- Authority
- GB
- United Kingdom
- Prior art keywords
- coating
- bore
- seat
- valve
- gate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000576 coating method Methods 0.000 abstract description 48
- 239000011248 coating agent Substances 0.000 abstract description 44
- 238000000034 method Methods 0.000 abstract description 17
- 239000007921 spray Substances 0.000 abstract description 14
- 238000000151 deposition Methods 0.000 abstract description 2
- UONOETXJSWQNOL-UHFFFAOYSA-N tungsten carbide Chemical compound [W+]#[C-] UONOETXJSWQNOL-UHFFFAOYSA-N 0.000 abstract description 2
- 239000007789 gas Substances 0.000 description 9
- 230000008569 process Effects 0.000 description 5
- 230000007704 transition Effects 0.000 description 4
- 241001274197 Scatophagus argus Species 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000005137 deposition process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000010926 purge Methods 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 241000272168 Laridae Species 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- -1 for example Substances 0.000 description 1
- 239000002737 fuel gas Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000005552 hardfacing Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 238000005304 joining Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16K—VALVES; TAPS; COCKS; ACTUATING-FLOATS; DEVICES FOR VENTING OR AERATING
- F16K3/00—Gate valves or sliding valves, i.e. cut-off apparatus with closing members having a sliding movement along the seat for opening and closing
- F16K3/02—Gate valves or sliding valves, i.e. cut-off apparatus with closing members having a sliding movement along the seat for opening and closing with flat sealing faces; Packings therefor
- F16K3/0227—Packings
- F16K3/0236—Packings the packing being of a non-resilient material, e.g. ceramic, metal
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16K—VALVES; TAPS; COCKS; ACTUATING-FLOATS; DEVICES FOR VENTING OR AERATING
- F16K25/00—Details relating to contact between valve members and seats
- F16K25/005—Particular materials for seats or closure elements
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16K—VALVES; TAPS; COCKS; ACTUATING-FLOATS; DEVICES FOR VENTING OR AERATING
- F16K25/00—Details relating to contact between valve members and seats
- F16K25/04—Arrangements for preventing erosion, not otherwise provided for
Landscapes
- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Ceramic Engineering (AREA)
- Coating By Spraying Or Casting (AREA)
- Valve-Gear Or Valve Arrangements (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Spray Control Apparatus (AREA)
- Fuel-Injection Apparatus (AREA)
Abstract
A method of treating a valve with a coating 32, such as tungsten carbide, includes depositing the coating with a spray stream 45 that is oriented perpendicular to the surface being treated. The method comprises applying the coating of uniform thickness onto lateral surface 18 of a valve seat 16, a portion of the valve seat bore 22, and the chamfered edge between the valve seat lateral surface 18 and the valve seat bore 22. The valve seat bore 22 can include an annular recess 55 formed to receive a layer of coating.
Description
PROCESS FOR IIAR1)FACING OF BORE AND
SEAT FACE INTERSECTION ON GATE VALVE
CROSS REFERENCE TO RELATED APPLiCATIONS
[0001] This application claims priority to and the benefit of copendirig U.S. Provisional Application 5cr. No. 61/049,571, filed May 1st, 2008, the frill disclosure of which is hereby incorporated by reference herein.
1. Field of Invention
[9002] This invention relates in general to gate valves used in the oil and gas industry, and in particular to a process for coating the inner rim of a gate valve seat.
2. Description of Related Art
100031 Referring to FIGS. 1 and 2, a standard gate valve 10 as used in the oil and gas production industry according to the prior art is illustrated. Valve 10 has a body 12 with a generally flow passage 14 extending there through. A pair of ring-shaped seats 16 rest in recesses formed in body 12. Seats 16 each have a front face 18 and a back face 19 and contain an annular bore 20.
The bore 20 has a wail 22 with an inside diameter that is approximately equal to the flow passage 14 inside diameter. A chamfered edge or curved surface is formed on each seat 16 where the front face 18 joins the inner wall 22. Each seat 16 has an outer rim 25 at the junction of front face 18. A gate 26 is positioned between the seats 16. Gate 26 has a solid portion 28 with a hole shown registering with the bore 20 allowing flow through the valve 10. The hole 30 has an inside diameter that is approximately equal to the inside diameter of the bore 20 in the seats 16.
[0004] The gate 26 is movable relative to the front faces 18 of the seats 16. Shown iii FRI. 2, the gate 26 has moved with respect to its position in FIG. 1, taking the hole 30 out of registration with the bore 20 to close the valve. When the valve 10 is in the closed position, the gate 26 and the seat front faces 18 are in contact and held closely together to prevent fluid leakage. Over time; as the gate 26 moves repeatedly between the open and closed positions, wear and friction occur at the areas of contact between the solid portion 28 and the front faces 18. These wear surfaces can be treated by applying a coating 32 or "hardfacJng," for example tungsten carbide to the contacting surfaces of at least one of the gate 26 uxl the seats 16.
[0005J Depicted in FIG. 3 is a valve 10 having a coating 32 applied to the seat front face 18 downstream o the gate 26. Damage is most prevalent along the front Face 18 and wall 22 boundary because the gate 26 elastically bows into the seat bore 20 under a pressure load. When the gate 26 is moved to open the valve, the deflected portion of the gate 26 applies concentrated forces onto the scat 16 which can result in damage.
[0006] TypicaJly, a theimal spray or vapor gas deposition processes have been used to apply the coating 32 to the seat 16. A thermal spray gull 34 according to the prior art is illustrated in FIG. 4 applying a coating to a valve seat 16. A robotic arm 36 is attached to the gun 34 and programmed to direct the movement of the gun 34. A fine metallic powder, for example, a member of the ttingsten carbide-cobalt family, is introduced into the barrel of the gun at an entry point 38. Oxygen and thel gas, for example, propane, propylene, hydrogen, or some hydrocarbon, are fed into the harrel of the gun at entry points 40 and 42. Purge gas may be introduced into the barrel at entry point 46. The fuel gas is ignited, and the resulting hot, high-pressure gas heats the powder and forces it out of the nozzle 44 olthe gun barrel as a beam 45 for use as coating 32. The coating 32 may be dispensed through the nozzle 44 in the form of a continuous stream, or alternatively, it may be dispensed. in intermittent pulses, with nitrogen gas used to purge the barrel after each pulse.
[0007] To apply coating 32 to a valve seat 16, as illustrated hi FIGS. 4 and 5, the seat 16 is affixed to a base 4C The robotic arm 36 positions the spray gun 34 so that the nozzle 44 is directed towards the front face 18 of the scat 16. There is preferably a fixed distance between the end of the nozzle 44 and the front face 18 of the seat 16 in order to produce a beam 45 with optimum strength and a coating 32 with optimum bond integrity. The coating 32 is applied to the front face 18 of the seat 16 along the radius 50 of the seat 16 along axis A. The gun 34 points a beam 45 initially at the outer rim 25 of the seat 16 on a point on axis A, and then moves the beam to apply coating 32 from the outer rim 25 of the seat 16 to the inner rim 24 of the seat 16.
Beam 45 remains perpendicular to Plane A at all times. Once the gun 34 reaches the bore 20, it reverses course and retraces its path along A to apply coating 32 from the bore 20 of the seal 16 to the outer rim 25 of the seat 16. As shown, the beam 45 contacts the seat 16 normal to the front face 18.
[0008] Referring now to FIG. 5, the seat 16 is rotated about axis B while coaling 32 is applied to the front face 18 of the seat 16 back and forth between bore 20 and outer rim 25. Obtaining a constant coating 32 thickness can be achieved by timing seat 16 rotation and the gun 34 emissions rate. When the gun 34 sprays coating 32 near the bore 20, some overspray may enter the bore 20 hut it is kept minimal by perpendicular path of the beam 45 to plane A. Moreover, the minimal overspray does not significantly attach itself as coating 32 to the inner wall 22 of the bore 20+ 100091 Enlarged for clarity in FJG. 6, depicted in a side sectional view is a closed valve 20 with its gate 26 wedged by fluid pressure (represented by arrows) against a seat 16. The fluid pressure bows the gate 26 in its middle concentrating force along an inteiface 21 between the front face 18 and the bore wall 22. The bowing is exaggerated in FIG. 6. Present coating processes leave a reduced thickness feathered end 33 at the interfëce 21. Thus bardfacing 32 along the interface 21 is vulnerable to fracturing due to the concentrated stress combined with the decreased thickness hardface coating at the feathered end 33.
SUMMARY OF INVENTION
[0010] Disclosed herein is a method of treating a valve seat having a bore, a seat face, and a chamfered edge joining the bore and seat face. In one example the method includes forming a counter bore from the seat face into the bore that defines a recess, and directing a metal coating spray stream at chamfered edge, so that a metal coating is applied on the chamfered edge, the seat face, and into the recess.
[0011] The prcscnt disclosure also include a valve that includes a valve body, an axial passage formed through the body, a valve gate having an aperture selectively registcrablc with the passage, an annular valve seat having a lateral side in contact with the valve gate and a bore registered with the passage, a chamfered edge on the valve seat spanning from a seat face into the bore, and a metal coating on the seat side, the chamfered surface, and along the bore wall past tile chamfered edge.
BRIEF DESCRIPTION OF TilE DRAWINGS
[0012] FIG. I is a sectional view of a typical gate valve according to the prior art with the gate in an open position.
[00131 FIG. 2 is a sectional view of the gate valve of FIG. 1 with the gate in a closed position.
[0014] FIG 3 is an enlarged view of the downstream side of the gate valve of FIG. I with a prior art coating applied to the top surface of the valve seat.
[0015] FIG. 4 is a side view of a themial spray gun and robotic arm for applying coating to a valve seat of the gate valve of FIG. 1 in a prior art method.
[0016] FIG. 5 is a top view of a valve seat of the gate valve of FIG. 3.
[0017] FIG. 6 is an enlarged side view of the valve seat of the gate valve of FIG. 3.
[0018] FIG. 7 provides a side view of a thermal spray gun and robotic arm for applying coating to a valve seat ola gate valve according to an embodiment of the present disclosure.
[0019] FIG. 8 is an enlarged side view of the valve seat of a gate valve as coating is being applied according to an embodiment of the present disclosure.
[0020] FIG. 9 schematically illustrates a side sectional view of a valve treated as disclosed herein included with a production tree with a wirelirie through the valve.
I)ETAIIJED DESCRIPTION OF INVENTION
[00211 Disclosed herein is a process for treating a downhole component. In an example the component parts may also be treated. The thermal spray gun 34 (FIG. 4) orientation can be advantageously changed during the coating process to apply a coating 32 having a uniform composition and thickness that bonds to the article being treated, including eurvcd surfaces on the article. In one example, a valve seat 16 can be treated by coating one of its lateral faces, i.e. inner or outer face 18, 19, as well as the bore inner wall 22 of the valve seat 1 6 (FIG. 3).
[0022] Refei-ring now to FiG. 7, depicted in a side vicw is an example of a thermal spray gun 34 coating a valve portion. In the example illustrated, the beam 45 is angled oblique, rather than normal, to the plane A containing the inner Face 18. A controller 37, shown in conununication with the arm 36, can be included and programmed to control the robotic ant 36. The arm 36 is shown tilting the gun 34 with respect to the plane A as the beam 45 is directed at the seat 16 from the nozzle 44. The arm 36 can manipulate the gun 34 so that the nozzle 44 moves back and forth between the seat 16 outer rim and its bore 20 without changing the oblique angle to the plane A. This can be accomplished by maintaining the gun 34 tilt constant while moving it along the path.
Alternatively, the controller 37 may swivel the gun 34 so its tilt angle changes as the nozzle 44 moves along a path. Coaling 32 can be applied directly along the scat outer rim 25, the bore inner wall 22, and/or other areas of the seat 16. Optionally, the robotic ann 36 and spray gun 34 can be held stationary and instead, the base 48 securing the seat 16 may be tilted. In an alternative embodiment, the process may be used to provide a coating 32 to other components of the valve 10, for example, certain areas of the solid portion 28 of the gate 26.
[0023] An enlarged view of the coating process of FIG. 7 is shos in a partial sectional side view in FIG. 8. In this example coaLing 32 is being applied along the boundary 27 between the front face 18 and the bore inner wall 22 where the boundary 27 is on a chamfered edge 29. The chamfered edge 29 includes a curved surface on its outer periphery with a radius R. In the example of FIG. 8, the beam 45 is oriented substantially normal to the chamfered edge 29 at nra! around the boundary 27. For the purposes of discussion herein, substantially normal to the chamfered edge 29 (including any other curved surface) can mean substantially perpendicular to a tangent line 53 shown where a curved surface is being contacted by the beam 45. When normal to the line 53, the beam 45 may also coincide with the line representing the surface radius R and thus may also point at the origin 0 of the radius R. In one example of use, the boundary 27 may be roughly at the mid-point of the chamfered edge 29. In this example, material being deposited on the chamfered edge 29 at the boundary 27 flows respectively along the front face 18 and towards the bore inner wall 22 to ibrrn the coating 32.
100241 In another example of use, the coating process includes adjusting the beam 45 angle (either stepwise or continuously) with respect to the plane A so that the beam 45 remains normal to the chamfered edge 29 at or around the boundary 27, irrespective of where on its curved surface the beam 45 contacts the chamfered edge 29. Thus the orientation of the gun 34 can change as it directs the beam 45 on the chamfered edge 29 along both sides of the boundary 27 between the bore wall 22 and inner surface 18. The orientation change can be performed manually or by the controller.
[0025] Tn the valve 10 embodiment of FIG. 8, a counter bore 54 is provided at an end of the bore adjacent the face 18. A transition 55 on the bore wall 22 defines an end of the counter bore 54. The transition 55 is shown disposed where the bore wall 22 is cylindrical and no longer tapered or conical. The coating 32 of hardfaeing (shown in dashed outline) applied to the seat 16 extends to the transition 55, having an outer surface shown generally coplanar with the bore wall 22. Strategically locating the transition 55 a distance inward from the plane A provides a sufficient space to receive the hardfacing without it flowing onto the bore inner wall 22 and protruding into the bore 20.
100261 After being applied, the coating 32 may be ground to provide a curved surface with a radius R. Optionally, the radius R can extend from the same origin 0 as the curved surface radius R. Grinding can also smooth the surface and so that the coating 32 has a unitbrm desired thickness and contact stress capacity for maximum resistance and sealing capability. As illustrated in FJG. 8, the coating 32 thickness is substantially the same along the front face 18 and the counter bore 54.
[0027j The application of coating 32 using a spray gun 34 with multiple degrees of movement according to the present invention increases the likelihood that a significant layer of coating 32 of uniform composition, thickness and bond integrity will attach and form along the front face 18.
Additionally, any coating 32 that is applied along the counter bore 54 will provide added support for the section of the coating 32 at the curved surface along the wall 22 and face 18 boundary that is tapered off and has reduced thickness and integrity. Thus valves treated with the present method can withstand greater loading and more loading cycles.
[0028] Shown in a schematic view in FIG. 9 is an example of a valve 74 with components, such as a valve gate, coated as described above. The valve 74 is disposed in a line 72 attached to a wellhead assembly 70. The wellhead assembly 70, which can be subsea or on land, is disposed over a well 76 bored through a formation 78. A wireline 80 is inserted through the line 72 and valve 74. The coating on the valve gate and valve seat increases their strength and cutting ability so the valve 74 can be closed onto and more easily sever the wirelinc 80 (including slickline, and/or tubing) with less susceptibility to damage than untreated valves.
[0029J The method described herein can coat a surface or object using a thermal spray or cold spray process, including any other method or technique for applying and/or depositing material onto a surface. Additionally, a vapor gas deposition process can be employed with the present method. In an example, the seat 16 is heated to high temperature in a vapor chamber and controlled amounts of tungsten and carbon gases released into the chamber. The gases contact the seat 16 and form a thin layer of coating 32 on the surface of the seat 16. Since no spraying is involved, the coating thickness will be substantially uniform on the front face 18, inner wall 22, and the chamfered edge 29 along where the face 18 and wall 22 join. The coating 32 can then be ground to a desired thickness.
[0030] The present method described herein, therefore, is well adapted to carry out and attain the ends and advantages mentioned, as well as others inherent therein. While a presently preferred embodiment has been given for purposes of disclosure, numerous changes exist in the details of procedures for accomplishing the desired results. These and other similar modifications will readily suggest themselves to those skilled in the art, and are intended to be encompassed within the spirit of the present invention disclosed herein and the scope of the appended claims.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US4957108P | 2008-05-01 | 2008-05-01 |
Publications (3)
Publication Number | Publication Date |
---|---|
GB0907490D0 GB0907490D0 (en) | 2009-06-10 |
GB2459570A true GB2459570A (en) | 2009-11-04 |
GB2459570B GB2459570B (en) | 2010-07-07 |
Family
ID=40792082
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB0907490A Active GB2459570B (en) | 2008-05-01 | 2009-05-01 | Process for hardfacing of bore and seat face intersection on gate valve |
Country Status (3)
Country | Link |
---|---|
GB (1) | GB2459570B (en) |
MY (1) | MY149053A (en) |
SG (2) | SG172725A1 (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2484191A (en) * | 2010-09-30 | 2012-04-04 | Vetco Gray Inc | Gate valve seal |
CN102840348A (en) * | 2011-06-20 | 2012-12-26 | 韦特柯格雷公司 | Gate valve seat and seat ring |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2282869A (en) * | 1993-10-15 | 1995-04-19 | Vetco Gray Inc Abb | Gate valve |
GB2352494A (en) * | 1999-07-15 | 2001-01-31 | Vetco Gray Inc Abb | Shear gate valve |
-
2009
- 2009-05-01 GB GB0907490A patent/GB2459570B/en active Active
- 2009-05-04 SG SG2011045614A patent/SG172725A1/en unknown
- 2009-05-04 MY MYPI20091799A patent/MY149053A/en unknown
- 2009-05-04 SG SG200903011-5A patent/SG156606A1/en unknown
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2282869A (en) * | 1993-10-15 | 1995-04-19 | Vetco Gray Inc Abb | Gate valve |
GB2352494A (en) * | 1999-07-15 | 2001-01-31 | Vetco Gray Inc Abb | Shear gate valve |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2484191A (en) * | 2010-09-30 | 2012-04-04 | Vetco Gray Inc | Gate valve seal |
CN102840348A (en) * | 2011-06-20 | 2012-12-26 | 韦特柯格雷公司 | Gate valve seat and seat ring |
GB2492217A (en) * | 2011-06-20 | 2012-12-26 | Vetco Gray Inc | Gate valve seat hard coating |
US8689886B2 (en) | 2011-06-20 | 2014-04-08 | Vetco Gray Inc. | Gate valve seat and seat ring |
CN102840348B (en) * | 2011-06-20 | 2016-09-21 | 韦特柯格雷公司 | Gate valve seat and seat ring |
Also Published As
Publication number | Publication date |
---|---|
SG172725A1 (en) | 2011-07-28 |
SG156606A1 (en) | 2009-11-26 |
GB2459570B (en) | 2010-07-07 |
GB0907490D0 (en) | 2009-06-10 |
MY149053A (en) | 2013-07-15 |
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