GB2355715B - Synthesis of 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) and diamino-2,4,6-trinitrobenzene (DATB) - Google Patents

Synthesis of 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) and diamino-2,4,6-trinitrobenzene (DATB)

Info

Publication number
GB2355715B
GB2355715B GB0026075A GB0026075A GB2355715B GB 2355715 B GB2355715 B GB 2355715B GB 0026075 A GB0026075 A GB 0026075A GB 0026075 A GB0026075 A GB 0026075A GB 2355715 B GB2355715 B GB 2355715B
Authority
GB
United Kingdom
Prior art keywords
trinitrobenzene
datb
tatb
triamino
diamino
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
GB0026075A
Other versions
GB0026075D0 (en
GB2355715A (en
Inventor
Anthony John Bellamy
Peter Golding
Simon James Ward
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
UK Secretary of State for Defence
Original Assignee
UK Secretary of State for Defence
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by UK Secretary of State for Defence filed Critical UK Secretary of State for Defence
Publication of GB0026075D0 publication Critical patent/GB0026075D0/en
Publication of GB2355715A publication Critical patent/GB2355715A/en
Application granted granted Critical
Publication of GB2355715B publication Critical patent/GB2355715B/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/04Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
    • C07C209/14Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
    • C07C209/18Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to carbon atoms of six-membered aromatic rings or from amines having nitrogen atoms bound to carbon atoms of six-membered aromatic rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06Preparation of nitro compounds
    • C07C201/08Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06Preparation of nitro compounds
    • C07C201/12Preparation of nitro compounds by reactions not involving the formation of nitro groups
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
GB0026075A 1999-10-26 2000-10-25 Synthesis of 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) and diamino-2,4,6-trinitrobenzene (DATB) Expired - Fee Related GB2355715B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB9925147A GB2355713A (en) 1999-10-26 1999-10-26 Synthesis of Diamino-orTriamino- 2,4,6-trinitrobenzene

Publications (3)

Publication Number Publication Date
GB0026075D0 GB0026075D0 (en) 2000-12-13
GB2355715A GB2355715A (en) 2001-05-02
GB2355715B true GB2355715B (en) 2004-03-17

Family

ID=10863280

Family Applications (2)

Application Number Title Priority Date Filing Date
GB9925147A Withdrawn GB2355713A (en) 1999-10-26 1999-10-26 Synthesis of Diamino-orTriamino- 2,4,6-trinitrobenzene
GB0026075A Expired - Fee Related GB2355715B (en) 1999-10-26 2000-10-25 Synthesis of 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) and diamino-2,4,6-trinitrobenzene (DATB)

Family Applications Before (1)

Application Number Title Priority Date Filing Date
GB9925147A Withdrawn GB2355713A (en) 1999-10-26 1999-10-26 Synthesis of Diamino-orTriamino- 2,4,6-trinitrobenzene

Country Status (1)

Country Link
GB (2) GB2355713A (en)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7057073B2 (en) 2003-08-04 2006-06-06 Regents Of The University Of California Synthesis of trinitrophloroglucinol and triaminotrinitrobenzene (TATB)
US8030521B2 (en) 2007-05-07 2011-10-04 Alliant Techsystems Inc. Methods of producing 1,3,5-triamino-2,4,6-trinitrobenzene
US7910776B2 (en) 2009-06-15 2011-03-22 Alliant Techsystems Inc. Methods of producing 1,3,5-triamino-2,4,6-trinitrobenzene
US7763753B1 (en) 2009-06-15 2010-07-27 Alliant Techsystems Inc. Methods for the production of 1,3,5-triamino-2,4,6-trinitrobenzene
US7737308B1 (en) 2009-06-15 2010-06-15 Alliant Techsystems Inc. Methods for nitrating compounds
CN102500292B (en) * 2011-10-13 2014-04-09 北京理工大学 Preparation method of amino-containing energetic material graded microspheres
CN104237405B (en) * 2014-09-05 2015-12-09 北京理工大学 The method of TATB synthetic intermediate and product in liquid chromatogram measuring waste water
CN104926660B (en) * 2015-05-29 2016-10-05 中国科学院青岛生物能源与过程研究所 The green synthesis method of a kind of trinitrophloroglucinol and application
CN104987293B (en) * 2015-07-22 2017-05-31 中国科学院青岛生物能源与过程研究所 A kind of green nitration method of phenolic compound and application
CN115108915A (en) * 2022-06-17 2022-09-27 四川九原程新材料有限公司 Preparation method of 1,3, 5-triethoxy-2, 4, 6-trinitrobenzene
CN116621714A (en) * 2023-05-19 2023-08-22 西南科技大学 Internal standard for detecting purity of TATB and detection method thereof

Also Published As

Publication number Publication date
GB9925147D0 (en) 1999-12-22
GB0026075D0 (en) 2000-12-13
GB2355713A (en) 2001-05-02
GB2355715A (en) 2001-05-02

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Legal Events

Date Code Title Description
PCNP Patent ceased through non-payment of renewal fee

Effective date: 20061025