GB2251312A - Sensor for measuring fluid flow rate - Google Patents

Sensor for measuring fluid flow rate Download PDF

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Publication number
GB2251312A
GB2251312A GB9126769A GB9126769A GB2251312A GB 2251312 A GB2251312 A GB 2251312A GB 9126769 A GB9126769 A GB 9126769A GB 9126769 A GB9126769 A GB 9126769A GB 2251312 A GB2251312 A GB 2251312A
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GB
United Kingdom
Prior art keywords
film
silicon
silicon base
sensor
resistor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB9126769A
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GB9126769D0 (en
GB2251312B (en
Inventor
Jiri Marek
Frank Bantien
Eugen Haering
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Robert Bosch GmbH
Original Assignee
Robert Bosch GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Robert Bosch GmbH filed Critical Robert Bosch GmbH
Publication of GB9126769D0 publication Critical patent/GB9126769D0/en
Publication of GB2251312A publication Critical patent/GB2251312A/en
Application granted granted Critical
Publication of GB2251312B publication Critical patent/GB2251312B/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01PMEASURING LINEAR OR ANGULAR SPEED, ACCELERATION, DECELERATION, OR SHOCK; INDICATING PRESENCE, ABSENCE, OR DIRECTION, OF MOVEMENT
    • G01P5/00Measuring speed of fluids, e.g. of air stream; Measuring speed of bodies relative to fluids, e.g. of ship, of aircraft
    • G01P5/10Measuring speed of fluids, e.g. of air stream; Measuring speed of bodies relative to fluids, e.g. of ship, of aircraft by measuring thermal variables
    • G01P5/12Measuring speed of fluids, e.g. of air stream; Measuring speed of bodies relative to fluids, e.g. of ship, of aircraft by measuring thermal variables using variation of resistance of a heated conductor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01FMEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F1/00Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow
    • G01F1/68Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow by using thermal effects
    • G01F1/684Structural arrangements; Mounting of elements, e.g. in relation to fluid flow
    • G01F1/6845Micromachined devices

Abstract

A sensor for measuring the velocity or flow rate of a flowing medium, in particular a gas, and which is exposed to the flowing medium, has a silicon base 1 to which there is applied a sequence of thin films in which a membrane 20 is formed. Between the membrane and the silicon base there is a cavity 15. The membrane has a resistor arrangement comprising at least one heating resistor 21 and at least one temperature-dependent sensor resistor 22 formed e.g. as doped polysilicon film elements. As shown the membrane consists of a polysilicon film 10, a silicon nitride insulating film 11, and an overall passivating film 12. Various forms and methods of manufacture are described. Since the device is also pressure sensitive, a "dummy" device which is not sensitive to temperature may be included in the sensor and used to compensate for pressure variations. <IMAGE>

Description

- 1 2231312 Sensor
Prior art
The invention is based on a sensor for measuring the velocity or flow rate of a flowing medium according to the generic type of the main claim.
PCT application WO 90/02317 describes a device for measuring a flowing quantity of air having a sensor element which is exposed to the flowing air and constructed in thick-film technology and which has a resistor arrangement comprising a film-type heating resistor and a temperaturedependent sensor film resistor, the sensor film resistor being a component of a bridge circuit. The resistor arrangement is accommodated in a bubble which is composed of ceramic material, in particular of glass ceramic, and which is formed into a dome on an insulating substrate. The thin membrane forming the bubble and the cavity between the membrane and the substrate ensure a thermal decoupling of the film resistors from the substrate.
In "Fine Grained Polysilicon and its Application to Planar Pressure Transducers", H. Guckel et al., Transducers 187, page 277 - 282, the production of a micromechanical pressure sensor, in particular the production of a "pillbox" membrane of polysilicon in thin-film technology is described.
In "Single-cryistal Silicon Pressure Sensors with 500 x Overpressure Protection" [sic), Lee Christel et al, Sensors and Actuators, A21 - A23 (1990), 84-88, a process is presented for producing a pressure sensor which has a membrane and in which a recess is etched in a f irst 24057 silicon wafer. In a further process step, a second wafer, which is made thinner in a third process step until it has the desired thickness of the sensor membrane, is bonded against the structured surface of the first wafer.
Advantages of the invention The sensor according to the invention for measuring the velocity or the flow rate of a flowing medium having the characterising features of the main claim has the advantage that it can be produced with very small overall size. As a result, measurements can also be carried out in very thin tubes. In addition, the small overall size of the sensor makes possible multiple arrangements, so that the measurement uncertainty can be reduced by redundancy and the reliability can be increased. For this purpose, for example, the measurement signals of a plurality of devices can be averaged. Multiple arrangements of sensor elements can also advantageously be used to determine the movement profile of a flowing medium. The very small overall size of the sensor which is exposed to the flowing medium also has a very advantageous effect since the sensor affects the flow of the medium only insignificantly and the medium is virtually not swirled. The micromechanical implementation of the sensor according to the invention is also moderate in price since silicon is used as base material and many devices can be produced on one wafer. The production of the membrane by micromechanical surf ace technology is particularly inexpensive and makes possible a substantially stress-free structure of the sensor element. In addition, the integration of the evaluation electronics on the sensor itself is possible. It is particularly advantageous that the membrane can be produced very thinly in thin-film technology, typically 1 to 2 jam thick, so that the resistor arrangement composed of sensor resistor and heating resistor produced on the membrane can be thermally decoupled very well from the silicon base.. This effect is further promoted by the use is 24057 of materials with low thermal conductivity, such as polysilicon, silicon nitride, silicon oxynitride and silicon oxide as membrane.
The measures listed in the subordinate claims make possible advantageous further developments of the sensor provided in the main claim. It is particularly advantageous if the spacing between membrane and silicon base is as large as possible. This can be achieved in that a silicon membrane is formed into a dome on the silicon base over auxiliary films which are later removed again, or, alternatively, by further additionally structuring the silicon base in its depth. A further advantageous measure for avoiding interfering effects, in particular as a result of the action of pressure on the sensor, is to etch the silicon base completely through, so that there is a pressure equalisation on both sides of the membrane. Another possibility for avoiding a measurement signal distortion due to pressure effects is to arrange a further membrane on the sensor element which is equipped with a temperature-independent sensor resistor exclusively for measuring pressure.

Claims (1)

  1. In Claims 13 to 17, advantageous processes are proposed for producing a
    sensor according to the invention. The sensor membrane can advantageously be produced by applying polysilicon films to structured silicon oxide auxiliary films and then removing the auxiliary films. An electrically insulating film to which the resistor arrangement is applied is then deposited on the polysilicon membrane. It is essential that this film structure is as stress-free as possible. The structured silicon oxide auxiliary films can advantageously be produced either by thermal oxidation of the masked surface of the silicon base or, alternatively, by depositing silicon oxide from a silane/oxygen atmosphere and then structuring the silicon oxide film. A further advantageous process for producing the sensor element is to etch a recess into the surface of a first silicon base and to deposit, on the surface of a second silicon base, a silicon oxide film,
    24057 against which the first silicon base with its structured surface is bonded. In a subsequent process step, the entire second silicon base is then etched away except for a small residual thickness which corresponds to the resistor thickness, so that the silicon oxide film forms a film of the sensor membrane. The resistor arrangement is then formed from the thin silicon film. An insulating protective film is furthermore finally deposited over the membrane with the resistor arrangement. In this process it is also possible to first introduce a recess into the surface of the second silicon base, deposit a first electrically insulating film over this structured surface of the second silicon base and apply the resistor arrangement, for example in the form of polysilicon films to said film in the region of the recess and finally to deposit a silicon oxide film thereover. After bonding the first silicon base with the structured surface against the second silicon base via the silicon oxide film, the entire second silicon base is again etched away, the silicon oxide film, the resistor arrangement and the insulating film serving as protective film forming the membrane.
    Drawing Exemplary embodiments of the invention are shown in the drawing and explained in greater detail in the description below.
    Figures la to le show various process steps in the construction of a sensor element according to the invention, Figure 2 shows a section through a sensor element, Figures 3a to 3c show process steps for constructing a sensor element according to the invention by a second process, Figures 4a and 4b show different process steps corresponding to a third process and Figure 5 shows a section through a pressure-equalised sensor element.
    is 24057 Description of the exemplary embodiments In Figure la, 1 denotes a silicon base to which a structured silicon oxide film 5 has been applied. The structured silicon oxide f ilm 5 can be produced either by suitable masking of the surf ace of the silicon base 1 and subsequent thermal oxidation of the points of the surf ace of the silicon base 1 not covered by the masking or by an oxidation of the entire surface and subsequent photolithographic structuring of the oxide. In the case of thermal oxidation, the silicon oxide film 5 is produced from the silicon of the silicon base 1 and atmospheric oxygen. Said silicon oxide film partially extends into the surface of the silicon base 1. A further possibility for producing a structured silicon oxide film is to deposit a silicon oxide film on the surface of the silicon base 1 from a silane/oxygen atmosphere and then to structure it in a photomasking process.
    Figure lb shows the silicon base 1 with the structured silicon oxide film 5 which serves as auxiliary film and over which a polysilicon film 10 has been deposited. Etch channels 6 are introduced into the polysilicon film 10 in the region of the auxiliary film 5, and this is shown in Figure 1c. Figure ld shows the structure after the silicon oxide auxiliary film 5 has been etched out under the polysilicon film 10 through the etch channels 6, so that a cavity 15 has been produced between the polysilicon film 10 and the silicon base 1. An insulating film 11, preferably of silicon nitride, which also seals the etch channels 6 is deposited over this structure.
    Figure le shows the final structure of the sensor element. Arranged on the insulating film 11 in the region of the cavity 15 are a heating resistor 21 and a temperature-dependent sensor resistor 22. The resistors 21 and 22 can advantageously be produced in the form of doped polysilicon films. As a protection against external effects and against contamination, a passivating film 12 has been deposited over the entire arrangement. Suitable - 6 24057 passivating films 12 are, in particular, silicon nitride or silicon oxynitride films.
    Depending on the nature of the structured silicon oxide film, i.e. depending on whether it is a thermal oxide or an oxide film deposited from a silane/oxygen atmosphere, the process shown in Figures la to d produces membranes 20 corresponding to Figure le or Figure 2. The silicon base 1 in Figure le is not structured; the cavity 15 between the membrane 20 and the silicon base 1 is produced because the membrane 20 is formed into a dome in t he manner of a bubble on the silicon base 1, as it is produced if an oxide film deposited from a silane-oxygen atmosphere is used. The silicon base 1 in Figure 2 has a recess across which the membrane 20 is stretched, so that the cavity 15 is produced by sealing the recess in the silicon base 1. This structure can be produced if thermal oxide is used. In the sensor structure corresponding to Figure 2, it is advantageous that the sensor surface is relatively flat.
    In Figure 3a, 1 denotes a.first silicon base into whose surface a recess 16 has been introduced. A silicon oxide film 18 has been deposited on the surface of a second silicon base 2. The arrow indicates that the second silicon base 2 is bonded to the structured surf ace of the f irst silicon base 1. This takes place via the silicon oxide film 18. After bonding, the entire silicon base 2 is removed in an etching process except for a thin silicon film 30. Into the latter a heating resistor 21 and a temperature-dependent sensor resistor 22 are then introduced by doping. as shown in Figure 3b. The silicon f ilm. 30 is then etched away with the exception of the resistors 21 and 22. Alternatively, the resistors 21 and 22 can also be introduced into the silicon base 2 for this purpose before bonding. Figure 3c shows the structure of the sensor element produced in this process. The recess in the first silicon base 1 is sealed by the silicon oxide film 18 which originates from the second silicon base 2, so that a cavity 15 is produced. The 24057 resistors 21 and 22 which are not removed during the etching process are arranged on the silicon oxide film 18. The entire sensor surface is covered with a passivating film 12 which serves as protective film against external effects, in particular contamination or attack by aggressive media. In this structure, the membrane 20 is essentially formed by the silicon oxide film 18. The resistors 21 and 22 are composed in this case of doped single-crystal silicon.
    In Figures 4a and b, a process is described which is similar to the process for constructing the sensor element shown in Figures 3a to 3c. A recess 16 is again introduced into a first silicon base 1. Passivating film 12, preferably a silicon nitride, silicon oxide or even a silicon oxynitride film, is deposited on the surface of a second silicon base 2. Resistors 22 and 21 in the form of doped polysilicon films are then deposited on the second silicon base 2. Finally, a silicon oxide film 18 is applied to the prepared surface of the second silicon base 2. The second silicon base 2 is now bonded against the first silicon base 1 exactly as in the process described above, so that the recess 16 in the first silicon base 1 is sealed to form a cavity 15. In a subsequent etching step, the entire silicon base 2 is etched away. In this process it is no. longer necessary to apply a further passivating film to the sensor element surface since the passivating film 12 takes over the function of a protective film. In addition, this sensor has an unstructured surface, and this reduces the deposition of particles and the swirling of the medium.
    Since the sensor elements shown in Figures 1 to 4 also act as pressure sensors, it is expedient to arrange next to the actual sensor element a further sensor element which is constructed in the same manner as the actual sensor element, but has only at least one temperature-independent sensor resistor so that it only determines the pressure but not any temperature effects. This correction parameter for the pressure can be 24057 subtracted from the signal of the actual sensor element whose resistors are temperature-dependent.
    Figure 5 shows the structure of a sensor element whose membrane 20 does not adjoin a sealed cavity. The silicon base 1 has a rear-side etching 17 which completely penetrates the silicon base 1 so that a pressure equalisation exists between the two sides of the sensor element. This structure suppresses interfering effects due to pressure differences.
    - 9 Claims 1. Sensor for measuring the velocity or flow rate of a f lowing medium, in particular a gas, having a sensor element, exposed to the flowing medium, with a membrane which has a resistor arrangement comprising at least one heating resistor and at least one temperature-dependent sensor resistor, the at least one sensor resistor being a component of an evaluation circuit, characterised in that the sensor element has a silicon base (1), in that a sequence of thin films (10. 11, 12; 18, 12) in which the membrane (20) is constructed is applied to the silicon base (1), and in that a cavity (15) exists between the mem brane (20) and the silicon base (1).
    2. Sensor according to Claim 1, characterised in that the at least one heating resistor (21) and the at least one sensor resistor (22) are arranged next to each other on a film (11; 18) and in that said film (11; 18) is composed of electrically insulating material.
    Sensor according to Claim 1. characterised in that the at least one heating resistor and the at least one sensor resistor are arranged above each other on two different films and in that between the at least one heating resistor and the at least one sensor resistor there is at least one film of electrically insulating material.
    4. Sensor according to Claim 1, characterised in that the heating resistor and sensor resistor are identi- Sensor according to one of the preceding claims, - 10 24057 characterised in that at least one f ilm (12) of electrically insulating material which completely covers the resistors (21, 22) is applied to the films (11; 18) on which the at least one heating resistor (21) and/or the at least one sensor resistor (22) are arranged.
    6. Sensor according to one of the preceding claims, characterised - in that the resistors (21, 22) are composed of doped single-crystal silicon or of doped polysilicon.
    7. Sensor according to one of the preceding claims, characterised in that the films of electrically insulating material are preferably composed of silicon nitride, silicon oxynitride or silicon oxide and said films are deposited in a low-stress manner.
    Sensor according to one of the preceding claims, characterised is in that a polysilicon film (10) is formed into a dome in bubble fashion on the silicon base (1), in that a first electrically insulating film (11) is applied to the polysilicon film (10) and in that the resistor arrangement is applied to 25 the first electrically insulating film (11).
    10.
    terised 0. Sensor according to one of Claims 1 to 7, charac- terised in that the silicon base (1) has a recess (16), in that a polysilicon film (10) which seals off the recess (16) is applied to the silicon base (1), in that a first electrically insulating film (11) is applied to the silicon film (10), and in that the resistor arrangement is applied to the first electrically insulating film (11). g-nR-- accordinn to one of Claims 1 to 7 charac- in that the silicon base (1) has a recess (16), in that a first electrically insulating film (18), 11 - 24057 preferably a silicon oxide film, which seals off the recess (16) is applied to the silicon base (1), and in that the resistor arrangement is applied to the first electrically insulating film (18).
    11. Sensor according to one of the preceding claims, characterised in that the silicon base (1) has a rear-side opening (17) so that the silicon base (1) is completely pierced in the region of the membrane (20).
    12. Sensor according to one of the preceding claims, characterised in that a further sensor element having a membrane is present which is exposed to the flowing medium, the membrane of the further sensor element having at least one temperature- independent sensor resistor for determining pressure.
    Process for producing a sensor according to Claim 8 or 9, characterised in that an S'02 film (5) structured in plinth fashion is introduced into a surface andlor applied to a surface of the silicon base (1), 13.
    in that a polysilicon film (10) is deposited on the surface of the silicon base (1) over the S'02 film (5) structured in plinth fashion.
    in that etch channels (6) are introduced into the polysilicon film (10) in the region of the S'02 film (5) structured in plinth fashion, in that the polysilicon film (10) is underetched through the etch channels (6) by etching away the SiO, film (5) formed in plinth fashion, in that a first electrically insulating film (11) is deposited on the polysilicon film (10), in that the resistor arrangement is applied to the first electrically insulating film (11) and in that at least one electrically insulating passivating film (12) which completely covers the resistor arrangement is applied to the first elec trically insulating film (11).
    - 12 is 24057 14. Process according to Claim 13, characterised in that the structured S'02 f "ra (5) is produced by depositing S'02 in a silane/oxygen atmosphere.
    Process according to Claim 13, characterised in that the structured S'02 film (5) is produced by thermal oxidation of the masked surface of the silicon base (1).
    16. Process for producing a sensor according to Claim or 11. characterised in that a recess (16, 17) is preferably etched into at least one surface of a first silicon base (1), in that an insulating film (18), preferably an S'02 film, is deposited on a surface of a second silicon base (2), in that the first silicon base (1) is bonded against the second silicon base (2) via the insulating film (18), in that the entire second silicon base (2) is then etched away with the exception of a thin silicon film (30) in that at least one heating resistor (21) and at least one sensor resistor (22) is [sic] introduced into the thin silicon film (30) by doping, in that the thin silicon f ilm (30) is etched away except for the at least one heating resistor (21) and the at least one sensor resistor (22) and in that at least one electrically insulating passivating film (12) which completely covers the resistors (21, 22) is applied to the S'02 film (18) 17. Process for producing a sensor according to Claim or 11, characterised in that a recess (16, 17) is preferably etched into at least one surface of a first silicon base (1), in that a first electrically insulating film (12) is deposited on a surface of a second silicon base (2), in that a resistor arrangement, preferably of polysilicon, is applied to the first electrically 24057 18.
    insulating film (12), in that a further electrically insulating film (18), preferably an S'02 film, is deposited on the first electrically insulating film (12) and over the resistor arrangement, in that the first silicon base (1) with a structured surface is bonded against the second silicon base (2) via the 1 S'02 film (18) and in that the entire second silicon base (2) is then etched away.
    Any of the sensors substantially as herein described with reference to the accompanying drawings.
    19. Any of the processes for producing a sensor substantially as herein described with reference to the accompanying drawings.
GB9126769A 1990-12-22 1991-12-17 Sensor Expired - Fee Related GB2251312B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19904041578 DE4041578C2 (en) 1990-12-22 1990-12-22 Method for producing a sensor for measuring the speed or the flow rate of a flowing medium

Publications (3)

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GB9126769D0 GB9126769D0 (en) 1992-02-12
GB2251312A true GB2251312A (en) 1992-07-01
GB2251312B GB2251312B (en) 1995-02-08

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DE (1) DE4041578C2 (en)
GB (1) GB2251312B (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0696725A1 (en) * 1994-08-12 1996-02-14 Tokyo Gas Co., Ltd. Thermal micro flow sensor and production method thereof
WO1998050763A1 (en) * 1997-05-07 1998-11-12 Ncsr 'demokritos' Integrated gas flow sensor based on porous silicon micromachining
EP1009974A1 (en) * 1998-07-01 2000-06-21 Memsys, Incorporated Solid state microanemometer
WO2008095747A1 (en) * 2007-02-07 2008-08-14 Continental Automotive Gmbh Method for producing a layered component
EP2085754A3 (en) * 2008-01-29 2011-06-15 Hitachi Ltd. Flow sensor with metal film resistor

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DE4233153C2 (en) * 1992-10-02 1995-08-17 Lang Apparatebau Gmbh Calorimetric flow meter and process for its manufacture
JP2002131106A (en) * 2000-10-24 2002-05-09 Hitachi Ltd Microheater and thermal air flowmeter
DE10119192C2 (en) * 2001-04-19 2003-07-10 Paal Gmbh Machine for baling and strapping
DE10121394A1 (en) * 2001-05-02 2002-11-07 Bosch Gmbh Robert Semiconductor component, in particular a micromechanical pressure sensor
US6983653B2 (en) * 2002-12-13 2006-01-10 Denso Corporation Flow sensor having thin film portion and method for manufacturing the same
JP2007286007A (en) * 2006-04-20 2007-11-01 Denso Corp Method of producing thermal type flow sensor
JP2010230312A (en) * 2009-03-25 2010-10-14 Fujikura Ltd Semiconductor sensor manufacturing method and semiconductor sensor
DE102011110882A1 (en) * 2011-08-17 2013-02-21 Sensus Spectrum Llc Thermal flow sensor

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US4501144A (en) * 1982-09-30 1985-02-26 Honeywell Inc. Flow sensor
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WO1989005963A1 (en) * 1987-12-23 1989-06-29 Siemens Aktiengesellschaft Silicon-based mass airflow sensor
US4867842A (en) * 1982-09-30 1989-09-19 Honeywell Inc. Method of making slotted diaphragm semiconductor devices

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JPS60236024A (en) * 1984-05-09 1985-11-22 Nippon Soken Inc Direct heating type air flow rate sensor
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US4501144A (en) * 1982-09-30 1985-02-26 Honeywell Inc. Flow sensor
US4867842A (en) * 1982-09-30 1989-09-19 Honeywell Inc. Method of making slotted diaphragm semiconductor devices
EP0319871A1 (en) * 1987-12-07 1989-06-14 Honeywell Inc. Thin film orthogonal microsensor for air flow and method for its fabrication
WO1989005963A1 (en) * 1987-12-23 1989-06-29 Siemens Aktiengesellschaft Silicon-based mass airflow sensor

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0696725A1 (en) * 1994-08-12 1996-02-14 Tokyo Gas Co., Ltd. Thermal micro flow sensor and production method thereof
WO1998050763A1 (en) * 1997-05-07 1998-11-12 Ncsr 'demokritos' Integrated gas flow sensor based on porous silicon micromachining
EP1009974A1 (en) * 1998-07-01 2000-06-21 Memsys, Incorporated Solid state microanemometer
EP1009974A4 (en) * 1998-07-01 2005-04-06 Memsys Inc Solid state microanemometer
WO2008095747A1 (en) * 2007-02-07 2008-08-14 Continental Automotive Gmbh Method for producing a layered component
EP2085754A3 (en) * 2008-01-29 2011-06-15 Hitachi Ltd. Flow sensor with metal film resistor

Also Published As

Publication number Publication date
GB9126769D0 (en) 1992-02-12
JPH04269628A (en) 1992-09-25
DE4041578C2 (en) 1997-07-17
DE4041578A1 (en) 1992-07-02
GB2251312B (en) 1995-02-08

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Effective date: 20061217