GB2141236A - Nuclear magnetic logging - Google Patents

Nuclear magnetic logging Download PDF

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Publication number
GB2141236A
GB2141236A GB08413166A GB8413166A GB2141236A GB 2141236 A GB2141236 A GB 2141236A GB 08413166 A GB08413166 A GB 08413166A GB 8413166 A GB8413166 A GB 8413166A GB 2141236 A GB2141236 A GB 2141236A
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United Kingdom
Prior art keywords
probe
solenoid
magnets
gap
core
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB08413166A
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GB2141236B (en
GB8413166D0 (en
Inventor
Hugh Clow
William Spencer Percival
Peter Ernest Walters
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National Research Development Corp UK
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National Research Development Corp UK
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Publication date
Priority claimed from GB838315866A external-priority patent/GB8315866D0/en
Application filed by National Research Development Corp UK filed Critical National Research Development Corp UK
Priority to GB08413166A priority Critical patent/GB2141236B/en
Publication of GB8413166D0 publication Critical patent/GB8413166D0/en
Publication of GB2141236A publication Critical patent/GB2141236A/en
Application granted granted Critical
Publication of GB2141236B publication Critical patent/GB2141236B/en
Expired legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N24/00Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
    • G01N24/08Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance
    • G01N24/081Making measurements of geologic samples, e.g. measurements of moisture, pH, porosity, permeability, tortuosity or viscosity
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01VGEOPHYSICS; GRAVITATIONAL MEASUREMENTS; DETECTING MASSES OR OBJECTS; TAGS
    • G01V3/00Electric or magnetic prospecting or detecting; Measuring magnetic field characteristics of the earth, e.g. declination, deviation
    • G01V3/18Electric or magnetic prospecting or detecting; Measuring magnetic field characteristics of the earth, e.g. declination, deviation specially adapted for well-logging
    • G01V3/32Electric or magnetic prospecting or detecting; Measuring magnetic field characteristics of the earth, e.g. declination, deviation specially adapted for well-logging operating with electron or nuclear magnetic resonance

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  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Geology (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Remote Sensing (AREA)
  • Geophysics (AREA)
  • Geophysics And Detection Of Objects (AREA)

Abstract

An elongated probe suitable for lowering down a borehole for nuclear magnetic logging has a pair of similar cylindrical magnets 1 and 2 separated by a gap in which a solenoid 3 is symmetrically disposed. The solenoid has a core 4 of high permeability ferrimagnetic material and has a length preferably equal to half the length of the gap. The magnets 1 and 2 and solenoid 3 with its core 4 are contained within a hollow cylindrical casing 5 of non-magnetic material. The static & RF(coil) magnetic field distributions are such that after suitable filtering upwards of 95% of the NMR signal arises from points more than 10cm from the probe axis & is hence properly representative of the earth formation. Provision of the core also increases the Q of the coil & the signal to raise ratio of the signal. <IMAGE>

Description

SPECIFICATION Nuclear magnetic logging Nuclear magnetic logging is a borehole technique in which information relating to a fluid (such as water or oil) in a geological formation is derived by performing nuclear magnetic resonance (NMR) experiments with a probe located in a borehole extending through the formation. The relevant nuclei are normally protons, and the measured parameters in respect of the fluid may include spin density and the relaxation times commonly denoted T1 and T2.Hitherto it has been the usual practice in nuclear magnetic logging to arrange for the polarising field H1 which excites the NMR to be a steady field generated by a constant current flowing through a coil in the probe, and to utilise the earth's magnetic field as the field Ho about which the nuclear spins precess during signal acquisition; this arrangement of course differs from the one used in conventional NMR spectrometers, in which the field Ho is generated by a magnet system and the field H1 is generated by a high frequency alternating current flowing through a coil.
Although offering the advantage over other borehole logging techniques of obtaining signals directly from an extractable fluid, nuclear magnetic logging has not so far been put to widespread use. A major problem encountered with the technique is that of ensuring that the desired NMR signals are not swamped by signals arising either from fluid in the borehole or from fluid in a disturbed region of rock immediately surrounding the borehole (which region will not usually be typical of the bulk of the formation). This selectivity problem is accentuated for the field arrangement normally used because with that arrangement the sensitivity falls off rapidly with distance from the axis of the borehole. Previous attempts to deal with this problem have involved the use of specially doped fluid in the borehole, but this is undesirable when logging water wells.It would in any event be preferable for the probe itself to be of a form inherently capable of affording a high degree of the desired spatial selectivity.
The present invention seeks to meet this requirement by providing a probe for use in nuclear magnetic logging, the probe being of elongated form suitable for lowering down a borehole with its longitudinal axis extending vertically, and incorporating a pair of similar cylindrical permanent magnets disposed with their axes substantially coincident with said longitudinal axis and separated by a gap extending between like poles of the two magnets, a solenoid disposed about the centre of in said gap coaxial with the magnets, and a core of magnetic material disposed within the solenoid.
Preferably the solenoid is disposed symmetrically in said gap. Preferably also the core of the solenoid is of a high permeability ferrimagnetic material.
In use of such a probe the field H1 is generated by a high frequency current flowing through the solenoid, which may also suitably serve to pick up the NMR signals; it will normally be appropriate to utilise conventional pulsed NMR techniques. The field Ho generated by the magnets and shaped by the core within the solenoid exhibits an inhomogeneous form such that appropriate spatial selectivity can be achieved by frequency discrimination, suitably by filtering the received NMR signals prior to detection; the basis for this is of course the fundamentai equation F = PyH/2rr, relating resonance frequency F to magnetic field H ("being the gyromagnetic ratio for the relevant nuclei).The provision of the core within the solenoid is also significant in enabling a satisfactory signal to noise ratio to be achieved.
The invention will be further described and explained with reference to the accompanying drawings, in which Figure lisa diagram illustrating the layout of the essential components of one probe in accordance with the invention; and Figures 2fa) to 2(d) are explanatory diagrams.
Referring to Figure 1, the probe includes a pair of similar permanent magnets 1 and 2 fabricated from a material of the type incorporating a cobaltsamarium alloy with a polymeric binder. The magnets 1 and 2 are of cylindrical form of length about 50 cm and diameter about five cm, and are disposed coaxially with like poles facing each other and separated by a gap of length about 50 cm. Symmetrically disposed within this gap and coaxial with the magnets 1 and 2 is a solenoid 3 having a length of about 25 cm and an external diameter of the magnets 1 and 2. The solenoid 3 consists of a copper winding formed on a core 4 of a high permeability ferrimagnetic material, for example constituted by a rod of manganese-zinc ferrite material.In a complete probe the components 1 to 4 are mounted coaxially within the cylindrical casing of non-magnetic material, which is indicated in outline at 5 and which has an external diameter of about 7 cm; the casing 5 may also house at least part of the electronic circuitry (not shown) required to carry out the NMR experiments.
The casing 5 is suspended at one end from one end of a cable (indicated in outline at 6) by means of which the probe can be lowered down a borehole with the longitudinal axis of the casing 5 extending vertically; the cable 6 incorporates conductors via which energising and/or signal currents can be passed between the probe and the part of the logging equipment located at the surface.
In explaining the design of the probe illustrated in Figure 1, it is convenient to denote the longitudinal axis of the probe as the Z-axis and to define the plane Z = 0 as that plane perpendicular to the Z-axis which bisects the gap between the magnets 1 and 2.
In respect of the requirement for spatial selectivity it is assumed that it is desired to discriminate as far as possible against any NMR signals arising from points less than say 10 cm from the Z-axis. It is appropriate firstly to consider an arrangement simi larto that shown in Figure 1 but with the core4 omitted; because of the symmetry of the arrangement about the plane Z = 0, at any point in this plane the field Ho generated by the magnets is directed wholly radially while the field H1 generated by the solenoid is directed parallel to the Z-axis and hence perpendicular to the field Ho. Figure 2(a) illustrates for this arrangement how the strength of the field Ho varies with distance R from the Z-axis for points in the plane Z = 0; the maximum value of the field occurs for a value of R equal to G/2Z-, where G is the length ofthe gap between the magnets. So far as points in the plane Z = 0 are concerned, the spatial selectivity requirement can be met by restricting the detected NMR signals to a band of resonance frequencies corresponding to values ofthefield Ho lying between the lines A and B in Figure 2(a); for protons this band will be approximately 56-67 kHz.It is however necessary to consider also points away from the plane Z = 0, and in Figure 2(b) the shaded area represents (for positive values of Z) the area in any plane passing through the Z-axis for which the proton resonance frequency will lie within the quoted frequency band; there is of course a similar area for negative values of Z and the volume of effective sensitivity can be obtained by rotation of these two areas about the Z-axis. As will be seen from Figure 2(b), the spatial selectivity is far from ideal for the arrangement being considered, since some 20% of the detected NMR signals would arise from points within 10 cm of the Z-axis. Moreover, calculations indicate that for such an arrangement the signal to noise ratio would be impracticably low.
The effect of the inclusion of the core 4 can be appreciated from Figures 2(c) and 2(d), which are diagrams respectively similar to Figures 2(a) and 2(b) but relating to the probe illustrated in Figure 1.
In this case the lines C and D in Figure 2(c) and the boundaries of the shaded area in Figure 2(d) corres pond respectively to proton resonance frequencies of 41.8 and 46.2 kHz; by filtering the received NMR signals with a filter having a pass band matching these values it should be possible to ensure that upwards of 95% of the detected signals emanate from points more than 10 cm from the Z-axis and hence properly representative of the formations under investigation. Moreover due to the effect of the high permeability core increasing the Q factor of the coil it is estimated that the signal to noise ratio should be several times higher for the probe illustrated in Figure 1 than for the similar arrangement with the core 4 omitted. In particular the signal to noise ratio should be high enough to enable accurate measurements of proton spin density (and hence free fluid index) to be obtained with a signal averaging time of three or four seconds, which would for example enable a vertical resolution of about 25 cm to be achieved within a reasonable logging rate of about four metres/minute. The probe can of course also be used for making measurements of one or other of the relaxation times T1 and T2, but in this case it is envisaged that the probe would be maintained stationary with the vertical resolution being about 15 cm.

Claims (6)

1. A probe for use in nuclear magnetic logging, the probe being of elongated form suitable for lowering down a borehole with its longitudinal axis extending vertically, and incorporating a pair of similar cylindrical permanent magnets disposed with their axes substantially coincident with said longitudinal axis and separated bya gap extending between like poles of the two magnets, a solenoid disposed about the centre of said gap coaxial with the magnets, and a core of magnetic material disposed within the solenoid.
2. The probe as claimed in Claim 1 in which the solenoid is disposed symmetrically in said gap.
3. The probe as claimed in either one of the preceding claims in which the length of the solenoid is approximately equal to half the length of the gap between the magnets.
4. The probe as claimed in any one of the preceding claims in which the core is of a high permeability ferrimagnetic material.
5. The probe as claimed in any one of the preceding claims in which the magnets are fabricated from material incorporating a cobalt/samarium alloy.
6. A probe for use in nuclear magnetic logging substantially as described herein with reference to the accompanying drawings.
GB08413166A 1983-06-09 1984-05-23 Nuclear magnetic logging Expired GB2141236B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB08413166A GB2141236B (en) 1983-06-09 1984-05-23 Nuclear magnetic logging

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB838315866A GB8315866D0 (en) 1983-06-09 1983-06-09 Nuclear magnetic logging
GB08413166A GB2141236B (en) 1983-06-09 1984-05-23 Nuclear magnetic logging

Publications (3)

Publication Number Publication Date
GB8413166D0 GB8413166D0 (en) 1984-06-27
GB2141236A true GB2141236A (en) 1984-12-12
GB2141236B GB2141236B (en) 1986-12-10

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Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2150303A (en) * 1983-11-25 1985-06-26 Picker Int Ltd Nuclear magnetic resonance methods and apparatus
DE3614154A1 (en) * 1985-05-03 1986-11-06 British Technology Group Ltd., London NMR DEVICE WITH A SWITCHABLE ATTENUATOR
EP0237323A2 (en) * 1986-03-11 1987-09-16 Numar Corporation nuclear magnetic resonance sensing apparatus and techniques
US4714881A (en) * 1986-07-15 1987-12-22 Mobil Oil Corporation Nuclear magnetic resonance borehole logging tool
US4933638A (en) * 1986-08-27 1990-06-12 Schlumber Technology Corp. Borehole measurement of NMR characteristics of earth formations, and interpretations thereof
US5055788A (en) * 1986-08-27 1991-10-08 Schlumberger Technology Corporation Borehole measurement of NMR characteristics of earth formations
WO1992007279A1 (en) * 1990-10-11 1992-04-30 Oxford Instruments Limited Magnetic field generating assembly
US5212447A (en) * 1990-12-03 1993-05-18 Numar Corporation Apparatus and technique for nmr diffusion measurement
US5376884A (en) * 1993-04-01 1994-12-27 Schlumberger Technology Corporation Nuclear magnetic resonance measuring apparatus
EP0774671A1 (en) * 1995-11-15 1997-05-21 Oxford Instruments (Uk) Limited Magnetic field generating assembly
US5712566A (en) * 1996-02-23 1998-01-27 Western Atlas International, Inc. Nuclear magnetic resonance apparatus and method
FR2770304A1 (en) * 1997-10-29 1999-04-30 Western Atlas Int Inc Permanent magnet structure and composition for bore hole NMR investigations
US6326785B1 (en) 2000-07-18 2001-12-04 Baker Hughes, Inc. Nuclear magnetic resonance tool with magnetostrictive noise compensation
WO2002001256A1 (en) 2000-06-28 2002-01-03 Baker Hughes Incorporated An nmr probe and method using powdered soft magnetic material
US6844727B2 (en) 2000-06-28 2005-01-18 Baker Hughes Incorporated Method and apparatus of reducing ringing in a nuclear magnetic resonance probe
US7235970B2 (en) 2000-06-28 2007-06-26 Baker Hughes Incorporated Antenna core material for use in MWD resistivity measurements and NMR measurements

Cited By (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4642568A (en) * 1983-11-25 1987-02-10 Picker International Limited Nuclear magnetic resonance methods and apparatus
GB2150303A (en) * 1983-11-25 1985-06-26 Picker Int Ltd Nuclear magnetic resonance methods and apparatus
US4701711A (en) * 1985-05-03 1987-10-20 National Research Development Corporation Nuclear magnetic resonance apparatus with switched attenuator
FR2581490A1 (en) * 1985-05-03 1986-11-07 Nat Res Dev METHOD AND APPARATUS FOR PULSE FORMATION FOR NUCLEAR MAGNETIC RESONANCE APPARATUS
FR2587564A1 (en) * 1985-05-03 1987-03-20 Nat Res Dev NUCLEAR MAGNETIC RESONANCE APPARATUS WITH SWITCHED ATTENUATOR AND RESONANT CIRCUIT
DE3614154A1 (en) * 1985-05-03 1986-11-06 British Technology Group Ltd., London NMR DEVICE WITH A SWITCHABLE ATTENUATOR
US4706030A (en) * 1985-05-03 1987-11-10 National Research Development Corporation Waveform generator for nuclear magnetic resonance apparatus
EP0237323A2 (en) * 1986-03-11 1987-09-16 Numar Corporation nuclear magnetic resonance sensing apparatus and techniques
US4710713A (en) * 1986-03-11 1987-12-01 Numar Corporation Nuclear magnetic resonance sensing apparatus and techniques
EP0237323A3 (en) * 1986-03-11 1990-04-11 Numar Corporation Nuclear magnetic resonance sensing apparatus & techniques
US4714881A (en) * 1986-07-15 1987-12-22 Mobil Oil Corporation Nuclear magnetic resonance borehole logging tool
US4933638A (en) * 1986-08-27 1990-06-12 Schlumber Technology Corp. Borehole measurement of NMR characteristics of earth formations, and interpretations thereof
US5055788A (en) * 1986-08-27 1991-10-08 Schlumberger Technology Corporation Borehole measurement of NMR characteristics of earth formations
US5055787A (en) * 1986-08-27 1991-10-08 Schlumberger Technology Corporation Borehole measurement of NMR characteristics of earth formations
WO1992007279A1 (en) * 1990-10-11 1992-04-30 Oxford Instruments Limited Magnetic field generating assembly
US5212447A (en) * 1990-12-03 1993-05-18 Numar Corporation Apparatus and technique for nmr diffusion measurement
US5376884A (en) * 1993-04-01 1994-12-27 Schlumberger Technology Corporation Nuclear magnetic resonance measuring apparatus
US5486761A (en) * 1993-04-01 1996-01-23 Schlumberger Technology Corporation Nuclear magnetic resonance measuring apparatus
EP0774671A1 (en) * 1995-11-15 1997-05-21 Oxford Instruments (Uk) Limited Magnetic field generating assembly
US5739687A (en) * 1995-11-15 1998-04-14 Oxford Instruments (Uk) Limited Magnetic field generating assembly
US5712566A (en) * 1996-02-23 1998-01-27 Western Atlas International, Inc. Nuclear magnetic resonance apparatus and method
US6069479A (en) * 1996-11-04 2000-05-30 Western Atlas International, Inc. Permanent magnet material composition and structure for eddy current suppression in a nuclear magnetic resonance sensing apparatus
FR2770304A1 (en) * 1997-10-29 1999-04-30 Western Atlas Int Inc Permanent magnet structure and composition for bore hole NMR investigations
WO2002001256A1 (en) 2000-06-28 2002-01-03 Baker Hughes Incorporated An nmr probe and method using powdered soft magnetic material
US6452388B1 (en) 2000-06-28 2002-09-17 Baker Hughes Incorporated Method and apparatus of using soft non-ferritic magnetic material in a nuclear magnetic resonance probe
US6844727B2 (en) 2000-06-28 2005-01-18 Baker Hughes Incorporated Method and apparatus of reducing ringing in a nuclear magnetic resonance probe
US7084625B2 (en) 2000-06-28 2006-08-01 Baker Hughes Incorporated Method and apparatus of reducing ringing in a nuclear magnetic resonance probe
US7235970B2 (en) 2000-06-28 2007-06-26 Baker Hughes Incorporated Antenna core material for use in MWD resistivity measurements and NMR measurements
US6326785B1 (en) 2000-07-18 2001-12-04 Baker Hughes, Inc. Nuclear magnetic resonance tool with magnetostrictive noise compensation

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Publication number Publication date
GB2141236B (en) 1986-12-10
GB8413166D0 (en) 1984-06-27

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Legal Events

Date Code Title Description
732 Registration of transactions, instruments or events in the register (sect. 32/1977)
PE20 Patent expired after termination of 20 years

Effective date: 20040522