GB2110106A - Distributor/collector assembly - Google Patents

Distributor/collector assembly Download PDF

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Publication number
GB2110106A
GB2110106A GB08231214A GB8231214A GB2110106A GB 2110106 A GB2110106 A GB 2110106A GB 08231214 A GB08231214 A GB 08231214A GB 8231214 A GB8231214 A GB 8231214A GB 2110106 A GB2110106 A GB 2110106A
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GB
United Kingdom
Prior art keywords
screen cylinder
distributor
support
catalyst
support discs
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB08231214A
Other versions
GB2110106B (en
Inventor
Tadayoshi Nagaoka
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nagaoka Kanaami KK
Original Assignee
Nagaoka Kanaami KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nagaoka Kanaami KK filed Critical Nagaoka Kanaami KK
Publication of GB2110106A publication Critical patent/GB2110106A/en
Application granted granted Critical
Publication of GB2110106B publication Critical patent/GB2110106B/en
Expired legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0278Feeding reactive fluids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0492Feeding reactive fluids

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

A distributor/collector assembly (10) is composed of a screen cylinder (18), a perforated tube (13) provided in the screen cylinder and support discs (17) also provided in the screen cylinder. The screen cylinder is made of cylindrically arranged support rods (11) and a wire (12) wound helically on the support rods. The perforated tube is formed with apertures for distributing or collecting fluid which flows through the wire screen. The support discs support, on one hand, the screen cylinder on the outer peripheries thereof and, on the other, the perforated tube in the opening formed in the support discs in such a manner that space is defined between the tube and the screen cylinder. The distributor/collector assembly can be buried in catalyst in a catalyst reactor and used as a distributor or collector. The assembly may comprise more than one screen cylinder, or two perforated tubes. <IMAGE>

Description

SPECIFICATION Distributor/collector assembly This invention relates to a distributor/collector assembly suitable for use as a distributor (or collector) in a column type of catalyst reactor, deodorizing apparatus or the like device.
The conventional column catalyst reactor includes, as shown in Fig. 1, a number of catalyst support grids 2 provided in a reactor column 1. Catalyst layers 3 are disposed on these catalyst support grids 2 and distributors 4 are suspended in the space above the catalyst layers 3 to distribute fluid (liquid or gas) over the catalyst layers 3 (for convenience of explanation, description of the distributors 4 will be made hereinafter as distributing liquid). The liquid is dripped through numerous apertures formed in the distributors 4 over the catalyst layers 3 and is subjected to a desired reaction through the catalyst layers 3 and then the liquid after reaction is taken out of the reactor column 1 through an outlet la.
As will be understood from the above, the conventional catalyst reactor 1 is of such a construction that the distributors 4 are provided separately from the catalyst support grids 2. Such construction, however, requires a large number of the catalyst support grids 2 if there are many catalyst layers 3 which results in a high manufacturing cost. Besides, if the number of the catalyst layers 3 increases, space required for providing the distributors 4 increases as well resulting in requirement of a huge reactor column with a substantial portion of its inside space being not utilized for packing catalyst. Moreover, mounting of the prior art distributors 4 in the reactor column 1 requires precision of the highest degree for the liquid must be evenly distributed from the distributors 4 and the labor cost spent for the mounting of the distributors 4 amounts to a considerable sum.
It is, therefore, an object of the present invention to provide a distributor which has eliminated the above described disadvantages of the prior art distributor in the column type catalyst reactor. According to the invention, a novel buried type distributor having both a fluid distribution (or collection) function and a catalyst retention function is provided.By disposing this distributor in the catalyst layer in a buried state, the catalyst support grids which have been indispensable in the conventional reactor column are obviated, the labor cost for mounting the distributors in the reactor column is saved for the mounting position of the distributor according to the invention does not require such a high degree of precision as in the case of the prior art distributor, and moreover, the efficiency of space utilization in the reactor column is greatly improved for the catalyst does not have to be separated in plural layers even if the distributors are pro vided in plural stages.
In disposing a distributor in catalyst in a buried state, there arises the problem that while the buried distributor must have a suffi ciently rugged construction to bear a heavy load imposed by the catalyst, the construction must not allow occurrence of a turbulent flow or drift of the liquid which is to be evenly distributed. There also arises the problem, particularly in the catalyst reactor wherein catalyst is circulated in a system including the reactor, that the distributor must be of a construction which will not allow clogging of the the catalyst in openings from which the liquid is to be distributed.
The above described problems can be com pletely overcome by the distributor/collector assembly according to the invention which comprises a screen cylinder composed of a plurality of elongated support rods arranged cylindrically with a suitable distance between adjacent rods and a wire screen member wound helically on said cylindrically arranged support rods, a tube disposed in said screen cylinder and formed with a multiplicity of apertures for distributing or collecting fluid which flows through said wire screen member of said careen cylinder, and a plurality of support discs provided in said screen cylinder with a suitable distance therebetween in such a manncr that said support rods of said screen cylinder are supported on the outer periphery of said support discs, each of said support discs being formed with an opening for being fitted with said tube and supporting said tube in said screen cylinder in such a manner that space is defined between said tube and said wire screen member of said screen cylinder.
Preferred embodiments of the invention will now be described with reference to the ac companying drawings.
In the acccompanying drawings, Figure 1 is a vertical sectional view of a I prior art column type catalyst reactor; Figure 2 is a perspective view showing an embodiment of the distributor/collector as sembly according to the invention in a state in which a part of the screen cylinder is removed for the convenience of illustration; Figure 3(a) is a front vertical section of an example of a column type catalyst reactor in which the distributor/collector assembly ac cording to the invention is provided; Figure 3(b) is a cross sectional view of the catalyst reactor taken along lines A-A in Fig.
3(a); Figure 3(c) is a vertical sectional view of the catalyst reactor taken along lines B-B in Fig.
3(a); Figure 4 is a view showing a state in which liquid is diffused from the distributor 21 shown in Figs. 3(a)-3(c); and Figures 5, 6, 7 and 8 are perspective views showing, showing, a part thereof being also removed, other embodiments of the distributor assembly according to the invention.
Fig. 2 shows a basic embodiment of the distributor/collector assembly according to the invention generally designated by a reference numeral 1 0. A reference numeral 1 8 designates a screen cylinder composed of elongated support rods 11 and a wire screen member 1 2. The support rods 11 are arranged cylindrically with a suitable distance between adjacent rods. The wire screen member 1 2 is of a wedge shape cross section and is wound helically on the cylindrically arranged support rods 11 with a suitable pitch.
Slits 1 2a are formed between respective adjacent wire portions. The width of each slit 1 2 is determined depending upon the size of a catalyst particle.
A plurality of support discs 1 7 are provided in the screen cylinder 1 8 with a suitable distance between adjacent support discs 1 7 in the axial direction of the screen cylinder 1 8.
The support discs 1 7 are disposed in such a manner that the support rods 11 cf the screen cylinder 1 8 are supported on the outer periphery of the respective support discs 17. Each of the support discs 1 7 is formed with a central opening 17a.
A tube 1 3 is fitted in the central openings 1 7a of the support discs 1 7. The support discs 1 7 therefore supports the tube 1 3 in such a manner that space is defined between the tube 1 3 and the wire screen member 1 2 of the screen cylinder 1 8. The tube 1 3 is formed with a multiplicity of small apertures 1 3a for distributing or collecting fluid which flows through the slits 1 2a of the wire screen member 1 2. The support discs 1 7 in this example are further formed with openings 1 7b which are formed equidistantly in the disc portion about the central opening 1 7a for communicating spaces in the screen cylinder 18 which are separated from one another by the support discs 1 7.
It will be appreciated from the above description that the combination of the screen cylinder 18, the perforated tube 1 3 and the support discs 1 3 provides a unique structure in which the support discs 1 7 perform the dual functions of (1) supporting the screen cylinder 18 against load applied inwardly from outside thus serving as reinforcing elements for the screen cylinder 18 and (2) supporting the tube 1 3 in the center of the screen cylinder 1 8 without requiring any other supporting devices.
Reverting to Fig. 2, a branch tube 1 4 is connected to the tube 1 3 which in turn is connected through a coupling 1 6 to a pipe 1 5 of a system in which the cylindrical screen assembly is used. The ends of the screen cylinder 18 and the tube 1 7 are respectively closed by suitable closing members.
For making the distributor/collector assembly 10, the support discs 1 7 are first fitted with the perforated tube 13, the support rods 11 are welded with a suitable interval therebetween to the support discs 1 7 by, e.g., spot welding, and finally the wire screen member 2 is wound on the support rods 11 with a predetermined pitch and welded thereon by, e.g., spot welding. Alternatively, the wire screen member 1 2 may be pressed to the support rods 11 by utilizing elasticity of the wire screen member 1 2. In this case, the welding of the wire screen member 1 2 to the support rods 11 may be omitted.
An example of using the assembly 10 in the column type catalyst reactor is shown in Figs. 3(a)-3(c). In this example, distributors 21 comprising a plurality of the assemblies 10 are disposed in upper and lower stages in a single layer of catalyst 25 packed in a column 20. Each of the distributors 21 includes the asssemblies 10 arranged in parallel across the pipe 1 5 and connected to the pipe 1 5 through the branch tube 14 and the coupling 16. Each of the assemblies 10 is closed at both ends thereof by closing members 23 and mounted on a flange 20a secured to the inner wall of the column 20. A single layer of catalyst support grids 22 are provided in the lower portion of the column 20.The catalyst 25 is filled into the column from an inlet 20c of the column 20 until the distributors 21 in the respective stages are completely buried in the catalyst.
The liquid to be reacted is caused to flow through the pipe 1 5 into the perforated tube 1 3 of each assembly 10 and diffused into the catalyst 25 through the apertures 1 3a of the tube 1 3. This state is shown in Fig. 4. As will be seen from this figure, since there is space defined between the tube 1 3 and the wire screen member 12, the liquid is diffused more evenly over a wider range of the catalyst layer than in the case where the tube 1 3 is buried in the catalyst layer in direct contact with the catalyst.It is also an advantage of the assembly of the present invention that the slits 1 2a of the wire screen member 1 2 are uniformly provided and there is no substantial barrier that will obstruct the diffusion of the liquid through the slits 1 2a in all directions so that no turbulence or drift of the liquid takes place in the distribution.
The liquid diffused into the catalyst 25 flows down in the catalyst layer and the expected reaction takes place during this flowing down of the liquid. The liquid, having completed the reaction, is received in the catalyst support grids 22 and taken out of the column 20 through openings 22a of the grids 22 and an outlet 20d of the column 20.
In the illustrated example, only one catalyst layer is provided and, since separation of the catalyst layer is unnecessary, the space inside of the column 20 can be utilized for filling of the catalyst to a maximum extent so that a maximum space efficiency can be realized.
Moreover, since only one layer of the catalyst support grids suffices, the cost for the provision of the catalyst support grids can be saved. In the illustrated example, two stages of the distributors 21 are provided. It will be apparent, however, that the above described advantages will become more prominent if there are an increased number of stages of the distributors 21.
The distributor/collector assembly according to the invention can be used only as a distributor but also as a collector. For example, the distributor 21 in the lower stage in the column shown in Figs. 3(a)-3(c) may be used as the collector for collecting the liquid which has flown down after completing reaction into the tube 1 3 through the slits 1 2a and taking out the liquid out of the column 20 through the pipe 1 5. In this case, the catalyst support grids 22 are not required and the outlet 20d of the column is closed. It is also possible to use the distributor/collector assemblies of the respective stages as the distributors for a certain period of time and, after completion of reaction, use the same assemblies as the collectors to collect the liquid completion of the reaction.
The arrangement of the distributor/collector assemblies is not limited to the horizontal disposition as shown in Figs. 3(a)-3(c) but the assemblies may be disposed vertically, or obliquely and crosswisely or in a staggered arrangement.
Modified embodiments of the cylindrical screen assemblies according to the invention are shown in Figs. 5, 6, 7 and 8. Throughout these embodiments, the same component parts as in the embodiment shown in Fig. 2 are designated by the same reference numerals and detailed description thereof will be omitted.
In the embodiment shown in Fig. 5, a pair of support beams 30 are fitted in slits 1 7c of the support discs 1 7 to connect these support discs 1 7 together and thereby to increase the strength of the distributor/collector assembly 10.
In the embodiment shown in Fig. 6, beams of a relatively large width are used as support beams 31A and 31 B. A substantial portion of each of the beams 31 A and 31 B extends outside of the outer periphery of the support discs 1 7. The screen cylinder 1 8 is divided into two portions along a plane including its axis and the respective divided portions are welded to the support beams 31 A and 31 B on opposite sides thereof.
In the embodiment shown in Fig. 7, the space inside of the screen cylinder 1 8 is separated into two parts by a support beam 32 and two tubes 13-1 and 13-2 are provided in the respective parts.
In the embodiment of Fig. 8, wire screens 12-1 and 12-2 are provided concentrically with the screen cylinder 1 8. Different kinds of catalysts are filled in the space between the inner wall surface of the column 20 and the outer wire screen 1 2-1, the space between the outer wire screen 1 2-1 and the inner wire screen 1 2-2 and the space between the inner screen 12-2 and the screen cylinder 18. The assembly is used as a vertical type distributor.
The liquid ejected from the apertures 1 3a of the tube 1 3 is diffused through the screen cylinder 18, the inner wire screen 1 2-2 and the outer wire screen 12-1 and reactions are carried out while the liquid flows through the different catalyst layers.
The screen cylinder 1 8 in the above described embodiments are all of a circular cross section. The configuration of the screen cylinder 1 8 is not limited to this but may be of an elliptic, octagonal, hexagonal or the like cross section. The configuration of the support discs 1 7 can also be varied depending upon the configuration of the screen cylinder 1 8. The wire screen member 1 2 should preferably be of a wedge-shape cross section but wires of other cross section may be used if they are capable of effectively preventing clogging of the slits 1 2a by catalyst particles.
In the above described embodiments, the distributor/collector assembly 10 is utilized as the distributor or collector in the catalyst reactor. The distributor/collector assembly 10 can be utilized as a distributor or collector for various uses in other chemical processes such, for example, as a deodorizing apparatus.

Claims (5)

1. A distributor/collector assembly comprising: a screen cylinder composed of a plurality of elongated support rods arranged cylindrically with a suitable distance between adjacent rods and a wire screen member wound helically on said cylindrically arranged support rods; a tube disposed in said screen cylinder and formed with a multiplicity of apertures for distributing or collecting fluid which flows through said wire screen member of said screen cylinder; and a plurality of support discs provided in said screen cylinder with a suitable distance therebetween in such a manner that said support rods of said screen cylinder are supported on the outer periphery of said support discs, each of said support discs being formed with an opening for being fitted with said tube and supporting said tube in said screen cylinder in such a manner that space is defined between said tube and said wire screen member of said screen cylinder.
2. A distributor/collector assembly as defined in Claim 1 wherein said support discs are formed with a pair of slits in diametrically opposed positions in said support discs and which further comprises a pair of support beams which are fitted in said slits of said support discs to connect said support discs together.
3. A distributor/collector assembly as defined in Claim 1 wherein said support discs are formed with a plurality of said openings and a plurality of said tubes are fitted in said openings.
4. A distributor/collector assembly as defined in any of Claims 1, 2 and 3 wherein said support discs are formed with openings for communicating spaces defined between said support discs and said screen cylinder.
5. A distributor/collector assembly subtantially as herein described with reference to Fig. 2,5,6,7 or 8 of the accompanying drawings.
GB08231214A 1981-11-06 1982-11-01 Distributor/collector assembly Expired GB2110106B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP56177901A JPS5932178B2 (en) 1981-11-06 1981-11-06 Multi-hole tube-encased screen tube

Publications (2)

Publication Number Publication Date
GB2110106A true GB2110106A (en) 1983-06-15
GB2110106B GB2110106B (en) 1985-04-24

Family

ID=16039037

Family Applications (1)

Application Number Title Priority Date Filing Date
GB08231214A Expired GB2110106B (en) 1981-11-06 1982-11-01 Distributor/collector assembly

Country Status (11)

Country Link
JP (1) JPS5932178B2 (en)
KR (1) KR880001995B1 (en)
AR (1) AR228692A1 (en)
AU (1) AU537473B2 (en)
BE (1) BE894919A (en)
BR (1) BR8206427A (en)
CA (1) CA1201876A (en)
DE (1) DE3240987C2 (en)
FR (1) FR2515982B1 (en)
GB (1) GB2110106B (en)
IT (1) IT1218329B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101147852B (en) * 2006-09-20 2010-09-01 中国石油化工股份有限公司 Multistage insulation fixed bed reactor

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102006060509A1 (en) * 2006-12-19 2008-06-26 Basf Se Reactor for continuous oxide hydrogenation of feed gas flow of saturated hydrocarbons on moving catalyst bed, comprises four reactor sections, which are separated from each other and split into sub-sections by alternating deflector plates
DE102006060507A1 (en) * 2006-12-19 2008-06-26 Basf Se Reactor for carrying out a reaction between two fluid educts on a catalyst bed with premixing of the fluid educts in a mixing device
TW200936245A (en) * 2007-10-30 2009-09-01 Basf Se Horizontal reactor for reacting a fluid feed stream with a fluid oxidant stream in the presence of a solid catalyst
FR2974739B1 (en) * 2011-05-03 2016-03-11 Commissariat Energie Atomique SOLID REACTOR MODULE / HEAT PUMP COMPRISING GAS DIFFUSERS WITH REDUCED SHUTDOWN HAZARDS

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT139112B (en) * 1931-10-17 1934-10-25 Houdry Process Corp Device for distributing a medium in a contact mass filling a reaction device.
FR1529137A (en) * 1966-10-28 1968-06-14 Exxon Research Engineering Co Fluid flow distributor
US3592613A (en) * 1968-12-30 1971-07-13 Universal Oil Prod Co Apparatus for fluid distribution in a fluid-solids contacting chamber
GB2065492B (en) * 1979-12-21 1983-10-19 Uop Inc Fluid distributor for fixed-bed catalytic reaction zones

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101147852B (en) * 2006-09-20 2010-09-01 中国石油化工股份有限公司 Multistage insulation fixed bed reactor

Also Published As

Publication number Publication date
KR880001995B1 (en) 1988-10-11
BR8206427A (en) 1983-09-27
BE894919A (en) 1983-03-01
AU9006282A (en) 1983-05-26
DE3240987A1 (en) 1983-07-14
FR2515982A1 (en) 1983-05-13
JPS5879537A (en) 1983-05-13
AR228692A1 (en) 1983-03-30
KR840002257A (en) 1984-06-25
FR2515982B1 (en) 1987-04-30
JPS5932178B2 (en) 1984-08-07
IT8224109A0 (en) 1982-11-05
GB2110106B (en) 1985-04-24
CA1201876A (en) 1986-03-18
DE3240987C2 (en) 1985-09-19
IT1218329B (en) 1990-04-12
AU537473B2 (en) 1984-06-28

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Date Code Title Description
PE20 Patent expired after termination of 20 years

Effective date: 20021031