GB191113018A - Method of and Apparatus for Treating Distillery Wash. - Google Patents
Method of and Apparatus for Treating Distillery Wash.Info
- Publication number
- GB191113018A GB191113018A GB191113018DA GB191113018A GB 191113018 A GB191113018 A GB 191113018A GB 191113018D A GB191113018D A GB 191113018DA GB 191113018 A GB191113018 A GB 191113018A
- Authority
- GB
- United Kingdom
- Prior art keywords
- glycerine
- solvent
- benzene
- vapours
- wash
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D19/00—Recovery of glycerol from a saponification liquor
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
- Solid Fuels And Fuel-Associated Substances (AREA)
Abstract
13,018. Meunier, G. May 30. [Addition to 12,207/11.] Glycerine, obtaining and purifying. - Relates to that portion of the parent invention dealing with the treatment of the mixture of distillers' wash or crude glycerine with carbonized cellulose to obtain glycerine and succinic acid or pure glycerine respectively. (1) A mixture of alcohol and benzene, preferably in equal parts, is used as a solvent; the glycerine may be separated from the resulting solution by adding a further quantity of benzene. (2) The residual solvent contained in the residue after the extraction of the glycerine is recovered by washing with a saturated solution of the saline constituents of the wash, or with concentrated wash freed from glycerine, or with petrol. The washing may be effected in the centrifugal apparatus in which the extraction was performed. (3) A continuously-acting plant is provided for effecting the drying of the mixture of wash and cellulose, the extraction of glycerine, and the recovery of the solvent by distillation. It comprises a drier A, an extractor B, and a solvent recuperator C, each provided with screw conveyers. The conveyers of the drier A and the recuperator C are provided with hollow steam-heated shafts, and may themselves be hollow; the conveyer of the extractor B is perforated to allow the solvent to pass through it. An agent, such as the mixture of benzene and alcohol, or benzene alone, is brought into contact with the material in the drier A in order to aid in the disengagement of the moisture at low temperatures. The vapours evolved pass to a rectifying-column a<1> in which the water is separated, the vapours of the added agent being either returned directly to the base of the drier or condensed in a condenser a<2> and returned in the liquid form. The liquid derived from the extractor B passes to a distilling-column b<1>, from which the solvent vapours pass to a condenser b<2> or directly to the extractor B. The recovery of the solvent in the recuperator B is aided by a current of steam or of benzene or other vapours. The vapours are separated from water &c. in a rectifying- column c' and are returned to the system.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT191112207X | 1910-05-21 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB191113018A true GB191113018A (en) | 1912-05-30 |
Family
ID=32476114
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB191112207D Expired GB191112207A (en) | 1910-05-21 | 1910-05-21 | Method of Treating Distillery Wash. |
GB191113018D Expired GB191113018A (en) | 1910-05-21 | 1911-05-30 | Method of and Apparatus for Treating Distillery Wash. |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB191112207D Expired GB191112207A (en) | 1910-05-21 | 1910-05-21 | Method of Treating Distillery Wash. |
Country Status (1)
Country | Link |
---|---|
GB (2) | GB191112207A (en) |
-
1910
- 1910-05-21 GB GB191112207D patent/GB191112207A/en not_active Expired
-
1911
- 1911-05-30 GB GB191113018D patent/GB191113018A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
GB191112207A (en) | 1912-05-20 |
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