GB1582757A - Method of pressing and forging metal powder - Google Patents

Description

(54) METHOD OF PRESSING AND FORGING METAL POWDER (71) We, ALUMINUM COMPANY OF AMERICA, a corporation organized and existing under the laws of the State of Pennsylvania, United States of America, of Alcoa Building, Pittsburgh, State of Pennsylvania, United States of America, do hereby declare the invention, for which we pray that a patent may be granted to us, and the method by which it is to be performed, to be particularly described in and by the following statement: This invention relates to a method of forming high density metal articles from metal powders of aluminum and its alloys.

More particularly, the invention relates to a method for direct pressing and forging of articles from preheated loose metal powder contained in a substantially closed deformable metal container.

Methods of hot forging of high density metal articles from metal powder are known in the field of powder metallurgy. In general practice metal powder flows into a die cavity where it may be pressed or compacted into an intermediate shape before it is forged into a shape of a final article. At the pressing stage to form an intermediate shape, heat may be added to aid interparticle bonding to form a compact of metal powder.

Metal powder may also be cold compacted, i.e. pressed without the addition of heat, into an intermediate shape. These compacts are sintered and repressed into another intermediate shape, or are forged into the finished shape of the worked article.

It is further known in the art of fabricating powdered metal to place metal powder in a deformable container and to compact the powder in the container to the desired density and shape by techniques such as rolling, extruding and forging of the powderfilled container. The powdered metal may be compacted into compacts which are stacked in a metallic container and the container and compacts evacuated, heated and deformed as in the forging method described in U.S. Patent 3,899,821, granted August 19, 1975. A metallic container filled with loose powder can be sealed, evacuated, heated and deformed in compacting the metal powder into an article of high density by applying a compressive force axially in a longitudinal portion of an extrusion chamber. U.S. Patent 3,631,583, granted January 4, 1972, describes such a method. Hotrolling of an evacuated, sealed, heated container filled with metal powder is shown in U.S. Patent 3,866,303, granted February 18, 1975. Thus the prior art practices include cold compacting and sintering, cold compacting and hot repressing, or hot forging of powder in sealed containers. Such methods add to the complexity of forging operations in that effort and apparatus are needed to evacuate the air from the powderfilled container, to seal the container, to compact the powder to an intermediate shape and to reheat the powdered material.

It is desirable, therefore, to provide a less complicated method of forging metal powder that eliminates the steps of compacting to an intermediate shape and sintering while providing a forged article having improved mechanical properties and metallurgical characteristics.

In accordance with the present invention there is provided a method for forming high density metal articles from metal powders of aluminum and its alloys, which comprises placing an amount of loose metal powder in à deformable container, heating the powder within the container, and forging said container with the metal powder therein to produce a metal article having the desired density and shape, the metal powder being initially placed in an open-ended readily deformable container having the general shape of the article to be forged, the amount of powder being more than sufficient metal needed to forge the article to said desired density, the powder being heated to a substantially uniform temperature below the melting point of the powder but at least 600"F to facilitate metallurgical bonding of the powder during conditions of plastic deformation with the container substantially closed to thereby contain the powder and to allow for venting of a portion of gases evolved from heating the powder within the container but to retain in said container a sufficient portion of said gases to effectively shield the powder and provide an oxidation protective atmosphere, and compressing the container within substantially closed dies which have provision for escape of excess metal to forge an article having a density of at least 99%.

Thus the present invention provides an improved method of forging metal parts from metal powders of aluminum and its alloys which eliminates any need of degassing a closed metal container with metal powder therein, of compacting and repressing into an intermediate shape, and of removing a deformed metal container after forging. The invention, generally includes placing in a metal container of light gauge metal foil loose metal powder. The container, of the general simple shape related to the article to be forged, is substantially closed with a cover during heating to contain the powder and to shield the powder from contamination. The cover also permits the powder to generate its own protective atmosphere during preheating while permitting some gases to escape from the container. The amount of metal powder put into the container is in excess of the metal needed to forge the article to a predetermined density and is heated to a uniform temperature to facilitate metallurgical bonding. Forging of the powder-filled container into an article of at least 99% density is done within closed dies having limited relief for flash. Such an uncomplicated method provides a forged article having a homogenous composition when the container and powder are of the same composition. Cladded forged articles from metal powder are obtained when the metal contanner and cover are of an alloy that is different from the metal powder but is compatible in that it bonds with the forged metal powder to form a composite product. Composite forged articles are also obtained by placing multiple powder alloys in the metal container. Thus the method facilitates forging metal powder without the need for complex multi-action tools or intricately shaped containers and provides for forged powder metallurgy parts having improved mechanical properties and/or metallurgical characteristics over conventionally forged powder metal parts.

The metal container employed by the invention is of a readily deformable simple shape generally in the configuration of, or related to, the detailed shape of an article to be forged. By simple shape is meant that the container has the outward appearance of the shape of the article to be forged, e.g. rectangular, triangular or cylindrical, without the detailed features and configurations of the shape of the forged article.

Such a form of the container will be sufficient if it contains the metal powder in a manner as to assure filling of a forged article during pressing and forging. A readily deformable container is one that has sufficient strength to maintain its shape to contain the powder while placing and heating of the powder in the container and during any transferring of the powder-filled container into a die cavity or elsewhere. Preferably, the metal container has an open-end for receiving metal powder and is made of a light gauge metal foil, such as aluminum and its alloys, of a gauge thickness generally between 00005 to 0040 inch depending upon the structural requirements as determined by the weight and shape of the article to be forged. Conceivably the container thickness could be as thick as 0125 inch for extremely large forgings.

The composition of the metal container may be the same as the metal powder or may differ. The invention thus provides a unique opportunity to produce clad products and parts composed of multiple powder alloys. The invention also provides an advantage in that the powder forged parts may have increased mechanical properties due to the plastic deformation and flow of both the metal powder and the metal container during the pressing and forging step. A finished forged product of a powder-filled container of the invention having the same composition as the powder, results in a homogenous forged article of uniform alloy composition having improved mechanical properties over a forged article produces by conventional powder metallurgy techniques.

A composite forged article is provided when the composition of the metal container differs from but is compatible with the composition of the metal powder. An alloy compatible with the metal powder is one that bonds with the metal powder during forging to provide a composite forged article, clad with an alloy of the metal container. If the metal container and cover are to be removed after forging by subsequent machining or by caustic etching, the metal container and cover need not be compatible and bond with the powder. Furthermore, powders of various compositions and characteristics can be selectively placed in the metal container to produce a forged article having unique and special properties in desired locations of the article. The finished forged shape of a forged article is the final worked shape of powder metal resulting from the pressing and forging operation and having over 99% density.

The forged article may and most often does require machining before its end use. It may also include both additional forging or other working to change its shape without significantly affecting the density and some machining before its end use.

A cover is provided for substantially closing an open-end of the metal container. The cover must be in place during the heating of the powder-filled container to obtain maximum properties and is preferably of a light gauge metal foil of the same composition as the powder or metal container.

The cover, however, can be of any composition and may be removed just prior to forging. One purpose of the cover is to keep the metal powder from blowing out of the container due to activity caused by any moisture on the powder particles and air between the particles during the preheat cycle. The cover also shields the powder from the furnace environment or any fan circulated furnace atmosphere during heating. Substantially closing the container confines the powder in its own evolved atmosphere protecting it against oxidation, but still provides ventilation of the container to permit some of the evolved gases to escape. Ventilation may be provided by loosely attaching the cover to the container so as to permit gases to escape or by providing holes in the cover or by other means.

A purpose of maintaining a cover over the open-end of the container while in the die cavity and during forging is to protect the metal powder from contamination by absorption and adsorption of lubricants within a die cavity.

A die cavity for pressing and forging the metal powder is of the closed die type, preferably heated and lubricated. The lubricant is one selected to suit die and forging temperatures, to aid in the plastic flow and to provide release of the finished forged article. Commercially available and typical forging lubricants may be used. Operating temperatures of the die must be compatible with the alloy being fabricated, the geometry of the article, and the forgoing rate achieved with the forging equipment being used. The design of the die cavity should limit the escape of loose powder or plastics flow of excess metal from the cavity until the forging pressure exceeds that required to fill the cavity and produce metallurgical bonding of the powder. The dies also preferably have provision for escape of the excess metal, commonly known as flash.

In the method of direct pressing and forging of hot loose metal powder, a simple metal container in the general shape of the article to be forged receives loose metal powder to about 50-60% density. The loosely filled powder is not necessarily or even usually distributed in proportion to the corresponding volume of an article to be forged, but may be unevenly placed in the container. The powder may also be lightly tamped or packed in the container. By this it is meant that the powder particles undergo no deformation and are thus still loose.

During the pressing and forging, it has been found that the metal powder and container are compacted with a result that metal material is displaced from areas containing an excess to areas originally defficient in material. Plastic deformation and shearing as well as compressive forces are thus produced. It is preferable that the amount of powder used be is excess of the metal material necessary to forge a desired article to the predetermined density. Additional deformation is therefore achieved by using an excess of material and allowing it to escape from the die cavity once the powder is compacted and forced to fill the cavity. This also assures plastic deformation and produces shearing and compressive forces during the pressing and forging operation. The shearing deformations tend to promote interparticle bonding and healing or closing of interparticle voids which are not healed by normal compressive forces. As a result of plastic deformation achieved, mechanical properties and densities are improved in relation to the properties attained by the usual practice of compacting and sintering.

Additionally, the typical mechanical properties of wrought materials, which generally are superior over powder metallurgy products, have been exceeded in at least one case using powdered aluminum alloy 6061 and the method herein described.

The metal container with the metal powder therein, maintains a cover of light gauge metal foil, preferably of the same composition as the metal container, loosely attached to the open-end of the container to substantially close the container during preheat.

The cover is not sealed on the container and it is not necessary to evacuate the container of air before closing. The substantial closing of the container permits venting of the container to allow some evolved gases to escape while a sufficient portion of the gases are retained to have an atmosphere protective against oxidation. Alternately, it is within the scope of the invention to provide venting of the container by other means during heating.

The powder-filled metal container is placed in a preheating unit for a sufficient length of time to assure uniform temperature throughout the contained powder. The cover shields the powder from the environment of the preheat unit. The preheat time necessary is dependent upon several factors including the volume amount of powder to be heated. The temperature to which the powder-filled container is heated should be sufliciently high as to facilitate bonding of the particular alloy powder under plastic deformation during forging. Such temperature should be below the melting point of the powder, should be at least 600 F and may range from 600"F to 1050"F. The preheating can be done in air, vacuum, or in any other suitable atmosphere. Furthermore, the temperature and atmosphere must be selected to provide suitable properties for the particular powder composition being pressed and forged. The cover during preheat keeps the powder from blowing out of the container due to moisture on the powder particles or air between the particles. Furthermore, it permits the evolving hydrogen from the heating powder to be partially contained within the container to act as a protective atmosphere. In the preferred embodiment, after the heating operation, the preheated powder-filled container is transferred to a forging die for fabrication. It is within the scope of the invention that the powder may be heated in the die or otherwise to avoid the need to transfer the powder-filled container. Furthermore, the cover may be removed just prior to forging.

The pressing and forging operation is preferably performed as one step in a single action closed forging die. The powdered metal must be kept above a minimum temperature required to achieve bonding and metal flow at any selected forging pressure.

The temperature is that temparture above which the bonding and plastic deformation of the metal powder is facilitated. Since bonding is dependent on both temperature and pressure, increases in temperature permit decreases in pressure, and decreases in temperature permit increases in pressure.

That temperature should be at least 600"F for typical commercially used forging pressures. In order for the metal powder and forged article to hold or exceed the minimum temperature requirement throughout the pressing and forging step, the dies can be operated at or above the minimum temperature. Preferably, the contained powder is also preheated to or above the minimum temnerature.

The dies mav be operated at a lower temperature provided that the contained powder is heated to a sufficiently high temperature that it will maintain a minimum required temperature desnite heat loss to a colder die during forging. The magnitude of an adjustment in preheat temperature to compensate for heat losses to a colder die depends upon the die temperature, the mass and heat conductivitv of the die and Dowder, the geometry and surface area of the article being forged, and the intimate contact time, i.e. dwell time, between the article and die as it governed bv the speed of the pressing and forging operation.

Unless the dies are operated at or above the minimum temperature required to achieve bonding and metal flow, the multiplicity of variables requires that optimum conditions be determined and tailored for each individual article and alloy. Preferably, and for economic reasons, the dies are preheated to or above the minimum temperature.

The preheated powder-filled container is pressed and forged into the desired shape having a predetermined density approaching 100% density without the need for an intermediate shape. Preferably, the forging is performed in one operation. The pressing and forging operation continues until all die cavities are filled, bonding of the powder particles occurs and usable engineering properties are achieved. The dwell time of the forging punch at a maximum sustained pressure may be as long as ten (10) seconds. The rate of forging is dependent upon the temperature, alloy and article to be pressed and forged. The forged article is ejected from the die and is ready for use after the removal of flash and after machining. The article may also again be forged to another shape before machining.

In order to more completely understand the invention, the following example is presented: Example A pre-alloyed powder having 75-90% -325 mesh particles containing nominally 20% Si, 45% Mn, and the remainder essentially aluminum fills a simple shaped aluminum foil container. The composition of the container is of commercial purity aluminum base alloy. The container is nominally of 0005 inch gauge and is generally triangular in shape with outside dimensions of about 8 inch X 8 inch x 8 inch x 2 1 inch high. A light gauge foil of nominally 00O075 inch gauge of the same composition as the container loosely covers the open- end of the container. It does not seal the container but substantially closes it to permit venting of some evolved gases during preheat. The powder-filled container is placed in a preheating unit and heated to a temperature of between 7001"-1000"F, preferably 800"F, in a nitrogen atmosphere for 120 minutes. In accordance with the invention, the container is transferred to a lubricated die cavity which is heated to a temperature of between 700 -750 F. At a forging pressure of 45 tons per square inch, and at a speed of 10 inches per minute, with a sustained pressure dwell time of 10 seconds, the container is pressed and forged into the desired shape. The forged article produced in accordance with the invention has a tensile strength of 55,000-50,000 p.s.i.

and vield strength of 40,000-45,000 p.s.i.

WHAT WE CLAIM IS: 1. A method for forming high density

**WARNING** end of DESC field may overlap start of CLMS **.

Claims (11)

**WARNING** start of CLMS field may overlap end of DESC **. deformation during forging. Such temperature should be below the melting point of the powder, should be at least 600 F and may range from 600"F to 1050"F. The preheating can be done in air, vacuum, or in any other suitable atmosphere. Furthermore, the temperature and atmosphere must be selected to provide suitable properties for the particular powder composition being pressed and forged. The cover during preheat keeps the powder from blowing out of the container due to moisture on the powder particles or air between the particles. Furthermore, it permits the evolving hydrogen from the heating powder to be partially contained within the container to act as a protective atmosphere. In the preferred embodiment, after the heating operation, the preheated powder-filled container is transferred to a forging die for fabrication. It is within the scope of the invention that the powder may be heated in the die or otherwise to avoid the need to transfer the powder-filled container. Furthermore, the cover may be removed just prior to forging. The pressing and forging operation is preferably performed as one step in a single action closed forging die. The powdered metal must be kept above a minimum temperature required to achieve bonding and metal flow at any selected forging pressure. The temperature is that temparture above which the bonding and plastic deformation of the metal powder is facilitated. Since bonding is dependent on both temperature and pressure, increases in temperature permit decreases in pressure, and decreases in temperature permit increases in pressure. That temperature should be at least 600"F for typical commercially used forging pressures. In order for the metal powder and forged article to hold or exceed the minimum temperature requirement throughout the pressing and forging step, the dies can be operated at or above the minimum temperature. Preferably, the contained powder is also preheated to or above the minimum temnerature. The dies mav be operated at a lower temperature provided that the contained powder is heated to a sufficiently high temperature that it will maintain a minimum required temperature desnite heat loss to a colder die during forging. The magnitude of an adjustment in preheat temperature to compensate for heat losses to a colder die depends upon the die temperature, the mass and heat conductivitv of the die and Dowder, the geometry and surface area of the article being forged, and the intimate contact time, i.e. dwell time, between the article and die as it governed bv the speed of the pressing and forging operation. Unless the dies are operated at or above the minimum temperature required to achieve bonding and metal flow, the multiplicity of variables requires that optimum conditions be determined and tailored for each individual article and alloy. Preferably, and for economic reasons, the dies are preheated to or above the minimum temperature. The preheated powder-filled container is pressed and forged into the desired shape having a predetermined density approaching 100% density without the need for an intermediate shape. Preferably, the forging is performed in one operation. The pressing and forging operation continues until all die cavities are filled, bonding of the powder particles occurs and usable engineering properties are achieved. The dwell time of the forging punch at a maximum sustained pressure may be as long as ten (10) seconds. The rate of forging is dependent upon the temperature, alloy and article to be pressed and forged. The forged article is ejected from the die and is ready for use after the removal of flash and after machining. The article may also again be forged to another shape before machining. In order to more completely understand the invention, the following example is presented: Example A pre-alloyed powder having 75-90% -325 mesh particles containing nominally 20% Si, 45% Mn, and the remainder essentially aluminum fills a simple shaped aluminum foil container. The composition of the container is of commercial purity aluminum base alloy. The container is nominally of 0005 inch gauge and is generally triangular in shape with outside dimensions of about 8 inch X 8 inch x 8 inch x 2 1 inch high. A light gauge foil of nominally 00O075 inch gauge of the same composition as the container loosely covers the open- end of the container. It does not seal the container but substantially closes it to permit venting of some evolved gases during preheat. The powder-filled container is placed in a preheating unit and heated to a temperature of between 7001"-1000"F, preferably 800"F, in a nitrogen atmosphere for 120 minutes. In accordance with the invention, the container is transferred to a lubricated die cavity which is heated to a temperature of between 700 -750 F. At a forging pressure of 45 tons per square inch, and at a speed of 10 inches per minute, with a sustained pressure dwell time of 10 seconds, the container is pressed and forged into the desired shape. The forged article produced in accordance with the invention has a tensile strength of 55,000-50,000 p.s.i. and vield strength of 40,000-45,000 p.s.i. WHAT WE CLAIM IS:

1. A method for forming high density

metal articles from metal powders of aluminum and its alloys, which comprises placing an amount of loose metal powder in a deformable container, heating the powder within the container, and forging said container with the metal powder therein to produce a metal article having the desired -density and shape, the metal powder being initially placed in an open-ended readily deformable container having the general shape of the article to be forged, the amount of powder being more than sufficient metal needed to forge the article to said desired density, the powder being heated to a substantially uniform temperature below the melting point of the powder but at least 600 F to facilitate metallurgical bonding of the powder during conditions of plastic deformation with the container substantially closed to thereby contain the powder and to allow for venting of a portion of gases evolved from heating the powder within the container but to retain in said container a sufficient portion of said gases to effectively shield the powder and provide an oxidation protective atmosphere, and compressing the container within substantially closed dies which have provision for escape of excess metal to forge an article having a density of at least 99%.

2. A method according to Claim 1, wherein said container is composed of light gauge metal foil or formed sheet of suffi- cient strength to contain the powder and maintain its shape during the steps of placing and heating of the powder in said container.

3. A method according to Claim 1 or 2, wherein said metal foil container is of a gauge thickness of between 00005 inch to 0 040 inch.

4. A method according to any one of Claims 1 to 3, wherein said container is composed of material having the same composition as said powdered metal to serve as an exterior surface of the forged article having a homogenous composition.

5. A method according to any one of Claims 1 to 3, wherein said container is composed of material which differs in composition from the metal powder and is compatible therewith to provide a cladding on the forged article.

6. A method according to any one of the preceding claims, wherein more than one metal powder is placed in selected locations in said metal container, each metal powder having different compositions and characteristics to provide a composite forged article having different mechanical properties and metallurgical characteristics at the locations.

7. A method according to any one of the preceding claims, wherein loose powdered metal is packed in said container without deforming said metal powder.

8. A method according to any one of the preceding claims, wherein said die is preheated to a temperature that is higher than said temperature sufficient to facilitate bonding of the metal powder during plastic deformation.

9. A method according to any one of the preceding claims, wherein a cover composed of material having the same composition as said container is maintained over the open end of the container during heating.

10. A method according to any one of the preceding claims, wherein forging of said container with said powder therein is performed in one compressive step.

11. A method for forming high density metal articles from metal powders of aluminum and its alloys, substantially as hereinbefore described and illustrated in the Example.