GB1560984A - Process for preparing phosphate salts - Google Patents
Process for preparing phosphate salts Download PDFInfo
- Publication number
- GB1560984A GB1560984A GB32642/75A GB3264275A GB1560984A GB 1560984 A GB1560984 A GB 1560984A GB 32642/75 A GB32642/75 A GB 32642/75A GB 3264275 A GB3264275 A GB 3264275A GB 1560984 A GB1560984 A GB 1560984A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acid
- phosphoric acid
- solution
- solvent
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 125000002467 phosphate group Chemical class [H]OP(=O)(O[H])O[*] 0.000 title 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 179
- 239000002253 acid Substances 0.000 claims description 90
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 80
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 73
- 239000002904 solvent Substances 0.000 claims description 71
- 239000000243 solution Substances 0.000 claims description 52
- 239000008346 aqueous phase Substances 0.000 claims description 40
- 238000000034 method Methods 0.000 claims description 37
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 34
- 239000007864 aqueous solution Substances 0.000 claims description 27
- 239000011734 sodium Substances 0.000 claims description 27
- 239000012074 organic phase Substances 0.000 claims description 26
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical group CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 claims description 25
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 claims description 25
- 239000012071 phase Substances 0.000 claims description 23
- 125000004432 carbon atom Chemical group C* 0.000 claims description 22
- 229910019142 PO4 Inorganic materials 0.000 claims description 21
- 235000021317 phosphate Nutrition 0.000 claims description 21
- 150000001875 compounds Chemical class 0.000 claims description 20
- 239000003960 organic solvent Substances 0.000 claims description 20
- 239000012535 impurity Substances 0.000 claims description 19
- 239000010452 phosphate Substances 0.000 claims description 19
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 18
- 229910021529 ammonia Inorganic materials 0.000 claims description 17
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 16
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 16
- 229910052700 potassium Inorganic materials 0.000 claims description 16
- 239000011591 potassium Substances 0.000 claims description 16
- 238000006386 neutralization reaction Methods 0.000 claims description 15
- 229910052751 metal Inorganic materials 0.000 claims description 14
- 239000002184 metal Substances 0.000 claims description 14
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 14
- 229910052708 sodium Inorganic materials 0.000 claims description 14
- 238000006243 chemical reaction Methods 0.000 claims description 13
- NBIIXXVUZAFLBC-UHFFFAOYSA-M dihydrogenphosphate Chemical compound OP(O)([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-M 0.000 claims description 13
- 150000002576 ketones Chemical class 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 13
- 150000001768 cations Chemical class 0.000 claims description 10
- 150000003839 salts Chemical class 0.000 claims description 10
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 8
- 125000000217 alkyl group Chemical group 0.000 claims description 7
- 150000001983 dialkylethers Chemical group 0.000 claims description 7
- 238000002425 crystallisation Methods 0.000 claims description 6
- 230000008025 crystallization Effects 0.000 claims description 6
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 claims description 4
- 150000007514 bases Chemical class 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 3
- 238000009835 boiling Methods 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 239000007791 liquid phase Substances 0.000 claims description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-L Phosphate ion(2-) Chemical compound OP([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-L 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 31
- 239000010410 layer Substances 0.000 description 13
- 235000011121 sodium hydroxide Nutrition 0.000 description 10
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 description 9
- 238000000605 extraction Methods 0.000 description 8
- 230000005484 gravity Effects 0.000 description 8
- 125000004437 phosphorous atom Chemical group 0.000 description 8
- 229960003975 potassium Drugs 0.000 description 8
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 description 7
- -1 di-isopropyl ether Chemical compound 0.000 description 7
- 229910052739 hydrogen Inorganic materials 0.000 description 7
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 description 7
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 description 6
- 229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 description 6
- 235000019837 monoammonium phosphate Nutrition 0.000 description 6
- 229910000403 monosodium phosphate Inorganic materials 0.000 description 6
- 235000019799 monosodium phosphate Nutrition 0.000 description 6
- XNLICIUVMPYHGG-UHFFFAOYSA-N pentan-2-one Chemical compound CCCC(C)=O XNLICIUVMPYHGG-UHFFFAOYSA-N 0.000 description 6
- FDPIMTJIUBPUKL-UHFFFAOYSA-N pentan-3-one Chemical compound CCC(=O)CC FDPIMTJIUBPUKL-UHFFFAOYSA-N 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 5
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 5
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical class [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 241000894007 species Species 0.000 description 4
- 239000001117 sulphuric acid Substances 0.000 description 4
- 235000011149 sulphuric acid Nutrition 0.000 description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- MSXVEPNJUHWQHW-UHFFFAOYSA-N 2-methylbutan-2-ol Chemical compound CCC(C)(C)O MSXVEPNJUHWQHW-UHFFFAOYSA-N 0.000 description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- PHTQWCKDNZKARW-UHFFFAOYSA-N isoamylol Chemical compound CC(C)CCO PHTQWCKDNZKARW-UHFFFAOYSA-N 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000012044 organic layer Substances 0.000 description 3
- 239000001488 sodium phosphate Substances 0.000 description 3
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 description 3
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 3
- JWZZKOKVBUJMES-UHFFFAOYSA-N (+-)-Isoprenaline Chemical compound CC(C)NCC(O)C1=CC=C(O)C(O)=C1 JWZZKOKVBUJMES-UHFFFAOYSA-N 0.000 description 2
- BBMCTIGTTCKYKF-UHFFFAOYSA-N 1-heptanol Chemical compound CCCCCCCO BBMCTIGTTCKYKF-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 description 2
- 239000001506 calcium phosphate Substances 0.000 description 2
- 229910000389 calcium phosphate Inorganic materials 0.000 description 2
- 235000011010 calcium phosphates Nutrition 0.000 description 2
- BGTOWKSIORTVQH-UHFFFAOYSA-N cyclopentanone Chemical compound O=C1CCCC1 BGTOWKSIORTVQH-UHFFFAOYSA-N 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- FKRCODPIKNYEAC-UHFFFAOYSA-N ethyl propionate Chemical compound CCOC(=O)CC FKRCODPIKNYEAC-UHFFFAOYSA-N 0.000 description 2
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 description 2
- AMQJEAYHLZJPGS-UHFFFAOYSA-N n-butyl carbinol Natural products CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 235000011118 potassium hydroxide Nutrition 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000011435 rock Substances 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 2
- 229910000406 trisodium phosphate Inorganic materials 0.000 description 2
- 235000019801 trisodium phosphate Nutrition 0.000 description 2
- RPAJSBKBKSSMLJ-DFWYDOINSA-N (2s)-2-aminopentanedioic acid;hydrochloride Chemical class Cl.OC(=O)[C@@H](N)CCC(O)=O RPAJSBKBKSSMLJ-DFWYDOINSA-N 0.000 description 1
- PTTPXKJBFFKCEK-UHFFFAOYSA-N 2-Methyl-4-heptanone Chemical compound CC(C)CC(=O)CC(C)C PTTPXKJBFFKCEK-UHFFFAOYSA-N 0.000 description 1
- NCHAZMIREBYOAP-UHFFFAOYSA-N C(CC)C(=O)CCC.C(C)(=O)O Chemical compound C(CC)C(=O)CCC.C(C)(=O)O NCHAZMIREBYOAP-UHFFFAOYSA-N 0.000 description 1
- 208000035871 PIK3CA-related overgrowth syndrome Diseases 0.000 description 1
- 244000000188 Vaccinium ovalifolium Species 0.000 description 1
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- KDFQYGBJUYYWDJ-UHFFFAOYSA-N azane;sodium Chemical compound N.[Na] KDFQYGBJUYYWDJ-UHFFFAOYSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 235000011180 diphosphates Nutrition 0.000 description 1
- ZPWVASYFFYYZEW-UHFFFAOYSA-L dipotassium hydrogen phosphate Chemical compound [K+].[K+].OP([O-])([O-])=O ZPWVASYFFYYZEW-UHFFFAOYSA-L 0.000 description 1
- POLCUAVZOMRGSN-UHFFFAOYSA-N dipropyl ether Chemical compound CCCOCCC POLCUAVZOMRGSN-UHFFFAOYSA-N 0.000 description 1
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000010440 gypsum Substances 0.000 description 1
- 229910052602 gypsum Inorganic materials 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Substances CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 1
- JMMWKPVZQRWMSS-UHFFFAOYSA-N isopropanol acetate Natural products CC(C)OC(C)=O JMMWKPVZQRWMSS-UHFFFAOYSA-N 0.000 description 1
- 229940011051 isopropyl acetate Drugs 0.000 description 1
- GWYFCOCPABKNJV-UHFFFAOYSA-N isovaleric acid Chemical compound CC(C)CC(O)=O GWYFCOCPABKNJV-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910001463 metal phosphate Inorganic materials 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- YKYONYBAUNKHLG-UHFFFAOYSA-N n-Propyl acetate Natural products CCCOC(C)=O YKYONYBAUNKHLG-UHFFFAOYSA-N 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 238000010587 phase diagram Methods 0.000 description 1
- PJGSXYOJTGTZAV-UHFFFAOYSA-N pinacolone Chemical compound CC(=O)C(C)(C)C PJGSXYOJTGTZAV-UHFFFAOYSA-N 0.000 description 1
- QVLTXCYWHPZMCA-UHFFFAOYSA-N po4-po4 Chemical compound OP(O)(O)=O.OP(O)(O)=O QVLTXCYWHPZMCA-UHFFFAOYSA-N 0.000 description 1
- 235000015497 potassium bicarbonate Nutrition 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 235000011181 potassium carbonates Nutrition 0.000 description 1
- 150000003112 potassium compounds Chemical class 0.000 description 1
- 229940086066 potassium hydrogencarbonate Drugs 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 229940090181 propyl acetate Drugs 0.000 description 1
- 239000013557 residual solvent Substances 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 235000015424 sodium Nutrition 0.000 description 1
- 150000003388 sodium compounds Chemical class 0.000 description 1
- 229910000162 sodium phosphate Inorganic materials 0.000 description 1
- 235000011008 sodium phosphates Nutrition 0.000 description 1
- 235000019832 sodium triphosphate Nutrition 0.000 description 1
- UPDATVKGFTVGQJ-UHFFFAOYSA-N sodium;azane Chemical compound N.[Na+] UPDATVKGFTVGQJ-UHFFFAOYSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N valeric acid Chemical compound CCCCC(O)=O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/46—Preparation involving solvent-solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/28—Ammonium phosphates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/38—Condensed phosphates
- C01B25/40—Polyphosphates
- C01B25/405—Polyphosphates of ammonium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
Priority Applications (13)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB32642/75A GB1560984A (en) | 1975-08-05 | 1975-08-05 | Process for preparing phosphate salts |
| ZA764512A ZA764512B (en) | 1975-08-05 | 1976-07-27 | Process for preparing phosphate salts |
| US05/709,632 US4112118A (en) | 1975-08-05 | 1976-07-29 | Process for preparing phosphate salts |
| CA258,176A CA1094287A (en) | 1975-08-05 | 1976-07-30 | Process for preparing phosphate salts |
| AU16425/76A AU507838B2 (en) | 1975-08-05 | 1976-07-30 | Method of making phosohate salts |
| IL50195A IL50195A (en) | 1975-08-05 | 1976-08-03 | Process for preparing phosphate salts |
| MX165780A MX143793A (es) | 1975-08-05 | 1976-08-04 | Metodo mejorado para preparar sales de fosfato a partir de acido fosforico |
| FR7623879A FR2320262A1 (fr) | 1975-08-05 | 1976-08-04 | Procede de preparation de phosphates a partir d'acide phosphorique |
| IT68947/76A IT1069532B (it) | 1975-08-05 | 1976-08-04 | Procedimento per la preparazione di sali fosfatici |
| BE169537A BE844860A (fr) | 1975-08-05 | 1976-08-04 | Procede de preparation de sels de phosphate |
| DE19762635165 DE2635165A1 (de) | 1975-08-05 | 1976-08-05 | Verfahren zur herstellung von phosphaten |
| JP51092854A JPS5220397A (en) | 1975-08-05 | 1976-08-05 | Process for preparing phosphate |
| NL7608701A NL7608701A (nl) | 1975-08-05 | 1976-08-05 | Werkwijze voor de bereiding van fosfaten. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB32642/75A GB1560984A (en) | 1975-08-05 | 1975-08-05 | Process for preparing phosphate salts |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1560984A true GB1560984A (en) | 1980-02-13 |
Family
ID=10341815
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB32642/75A Expired GB1560984A (en) | 1975-08-05 | 1975-08-05 | Process for preparing phosphate salts |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US4112118A (cg-RX-API-DMAC7.html) |
| JP (1) | JPS5220397A (cg-RX-API-DMAC7.html) |
| AU (1) | AU507838B2 (cg-RX-API-DMAC7.html) |
| BE (1) | BE844860A (cg-RX-API-DMAC7.html) |
| CA (1) | CA1094287A (cg-RX-API-DMAC7.html) |
| DE (1) | DE2635165A1 (cg-RX-API-DMAC7.html) |
| FR (1) | FR2320262A1 (cg-RX-API-DMAC7.html) |
| GB (1) | GB1560984A (cg-RX-API-DMAC7.html) |
| IL (1) | IL50195A (cg-RX-API-DMAC7.html) |
| IT (1) | IT1069532B (cg-RX-API-DMAC7.html) |
| MX (1) | MX143793A (cg-RX-API-DMAC7.html) |
| NL (1) | NL7608701A (cg-RX-API-DMAC7.html) |
| ZA (1) | ZA764512B (cg-RX-API-DMAC7.html) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4224294A (en) * | 1979-01-15 | 1980-09-23 | Stauffer Chemical Company | Preparation of sodium orthophosphate mixtures |
| FR2447348A1 (fr) * | 1979-01-24 | 1980-08-22 | Rhone Poulenc Ind | Procede de purification d'un acide phosphorique impur |
| US4285920A (en) * | 1979-11-08 | 1981-08-25 | Stauffer Chemical Company | Solvent extraction process for preparing purified phosphoric acid and sodium phosphate salts |
| US4265867A (en) * | 1980-06-20 | 1981-05-05 | Arcanum Corporation | Preparation of dicalcium phosphate |
| DE3413020A1 (de) * | 1984-04-06 | 1985-10-17 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung einer alkaliphosphatloesung |
| US4751066A (en) * | 1986-05-08 | 1988-06-14 | Fmc Corporation | Process for preparing alkali metal phosphate |
| RU2166476C2 (ru) * | 1998-12-04 | 2001-05-10 | Зайцев Борис Николаевич | Способ очистки экстракционной фосфорной кислоты |
| RU2191745C1 (ru) * | 2001-04-25 | 2002-10-27 | Зайцев Борис Николаевич | Способ очистки экстракционной фосфорной кислоты |
| RU2208576C1 (ru) * | 2002-05-14 | 2003-07-20 | Открытое акционерное общество "Научно-исследовательский институт по удобрениям и инсектофунгицидам им. проф. Я.В.Самойлова" | Способ восстановления органического экстрагента в производстве очищенной фосфорной кислоты |
| US8658117B2 (en) | 2009-05-27 | 2014-02-25 | Easymining Sweden Ab | Production of ammonium phosphates |
| SE536607C2 (sv) | 2012-06-21 | 2014-03-25 | Easymining Sweden Ab | Framställning av ammoniumfosfater |
| EP4165001A4 (en) | 2020-06-12 | 2025-11-05 | Easymining Sweden Ab | PRODUCTION OF POTASSIUM PHOSPHATES |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1929443A (en) * | 1930-08-26 | 1933-10-10 | American Agricultural Chem Co | Process for obtaining alkali metal phosphates |
| GB974610A (en) * | 1962-05-24 | 1964-11-04 | Canadian Ind | Purification of phosphoric acid |
| DE2029564C3 (de) * | 1970-06-16 | 1978-06-22 | Giulini Chemie Gmbh, 6700 Ludwigshafen | Verfahren zur Herstellung von reinen Alkaliphosphaten aus Rohphosphorsäure |
| ZA732725B (en) * | 1972-04-26 | 1974-11-27 | Albright & Wilson | Purification of phosphoric acid |
| GB1464536A (cg-RX-API-DMAC7.html) * | 1973-02-07 | 1977-02-16 | ||
| US4018869A (en) * | 1973-06-06 | 1977-04-19 | Chemische Fabrik Budenheim Rudolf A. Oetker | Process for the extractive purification of phosphoric acid containing cationic impurities |
| US4024225A (en) * | 1973-11-02 | 1977-05-17 | United States Steel Corporation | Method of making high purity alkali metal phosphates from wet-process phosphoric acid |
-
1975
- 1975-08-05 GB GB32642/75A patent/GB1560984A/en not_active Expired
-
1976
- 1976-07-27 ZA ZA764512A patent/ZA764512B/xx unknown
- 1976-07-29 US US05/709,632 patent/US4112118A/en not_active Expired - Lifetime
- 1976-07-30 AU AU16425/76A patent/AU507838B2/en not_active Expired
- 1976-07-30 CA CA258,176A patent/CA1094287A/en not_active Expired
- 1976-08-03 IL IL50195A patent/IL50195A/xx unknown
- 1976-08-04 IT IT68947/76A patent/IT1069532B/it active
- 1976-08-04 FR FR7623879A patent/FR2320262A1/fr active Granted
- 1976-08-04 BE BE169537A patent/BE844860A/xx unknown
- 1976-08-04 MX MX165780A patent/MX143793A/es unknown
- 1976-08-05 NL NL7608701A patent/NL7608701A/xx not_active Application Discontinuation
- 1976-08-05 DE DE19762635165 patent/DE2635165A1/de not_active Withdrawn
- 1976-08-05 JP JP51092854A patent/JPS5220397A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| AU1642576A (en) | 1978-02-02 |
| DE2635165A1 (de) | 1977-02-24 |
| JPS5220397A (en) | 1977-02-16 |
| US4112118A (en) | 1978-09-05 |
| AU507838B2 (en) | 1980-02-28 |
| ZA764512B (en) | 1977-07-27 |
| FR2320262A1 (fr) | 1977-03-04 |
| FR2320262B1 (cg-RX-API-DMAC7.html) | 1979-05-25 |
| NL7608701A (nl) | 1977-02-08 |
| CA1094287A (en) | 1981-01-27 |
| IL50195A0 (en) | 1976-10-31 |
| MX143793A (es) | 1981-07-16 |
| IL50195A (en) | 1979-07-25 |
| IT1069532B (it) | 1985-03-25 |
| BE844860A (fr) | 1977-02-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US2885265A (en) | Process for producing substantially pure orthophosphoric acid | |
| US4112118A (en) | Process for preparing phosphate salts | |
| US4836995A (en) | Process for the manufacture of monopotassium phosphate | |
| BR112014032059B1 (pt) | Produção de fosfatos de amônio | |
| US4236911A (en) | Purification and conversion of phosphoric acid to ammonium phosphates | |
| CA1095218A (en) | Purification of phosphoric acid | |
| US4225568A (en) | Process for the purification of an impure phosphoric acid | |
| US4132540A (en) | Process for removing solvent from the raffinate of extracted phosphoric acid and for preparing phosphate salts | |
| US4222994A (en) | Solvent extraction purification of wet-processed phosphoric acid | |
| US3554729A (en) | Manufacture of low chloride potassium phosphate fertilizer | |
| FI59077B (fi) | Foerfarande foer rening av vaotprocessfosforsyra | |
| US4781905A (en) | Process for producing phosphoric acid and/or phosphates from wet-process phosphoric acid and an extractant therein | |
| US1857470A (en) | Process for obtaining orthophosphoric acid and/or conversion products thereof | |
| IL45043A (en) | Purification of phosphoric acid by means of organic solvents | |
| US3428418A (en) | Ammonium nitrate stabilization | |
| GB1038486A (en) | A process for the preparation of alkali metal aluminium acid orthophosphates | |
| US2396115A (en) | Production of mono-calcium citrate | |
| US3348910A (en) | Process for the manufacture of magnesium ammonium phosphate monohydrate | |
| US4200620A (en) | Decontamination of wet-processed phosphoric acid | |
| US4132765A (en) | Recovery of fluoride values | |
| IL42065A (en) | Purification of phosphoric acid | |
| US3947499A (en) | Phosphoric acid purification | |
| US4196180A (en) | Purification of phosphoric acid by means of organic solvents | |
| US3525585A (en) | Process of preparing water-soluble phosphates | |
| US3661513A (en) | Manufacture of alkali metal phosphates |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |