GB1495442A - Process for preparing chlorinated copper phthalocyanines - Google Patents
Process for preparing chlorinated copper phthalocyaninesInfo
- Publication number
- GB1495442A GB1495442A GB3255/75A GB325575A GB1495442A GB 1495442 A GB1495442 A GB 1495442A GB 3255/75 A GB3255/75 A GB 3255/75A GB 325575 A GB325575 A GB 325575A GB 1495442 A GB1495442 A GB 1495442A
- Authority
- GB
- United Kingdom
- Prior art keywords
- weight
- sulphuric acid
- water
- copper phthalocyanine
- jan
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B47/00—Porphines; Azaporphines
- C09B47/04—Phthalocyanines abbreviation: Pc
- C09B47/08—Preparation from other phthalocyanine compounds, e.g. cobaltphthalocyanineamine complex
- C09B47/10—Obtaining compounds having halogen atoms directly bound to the phthalocyanine skeleton
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Abstract
1495442 Chlorinating copper phthalocyanines HOECHST AG 24 Jan 1975 [26 Jan 1974]3255/75 Heading C4P Unchlorinated or partially chlorinated copper phthalocyanine is reacted with chlorine under a partial pressure of at least 0À1 atmospheres gauge at temperatures up to 20 C. in fuming sulphuric acid in presence of iodine as catalyst; preferably in amounts of 0À05 to 0À5% by weight of the copper phthalocyanine. Oleum having a free sulphur trioxide content of 0À5 to 5À0% by weight is preferred and chlorination is continued until the product contains 2À5 to 6% by weight of chlorine. Water may be added to the product mixture to reduce the sulphuric acid concentration to 80-88% by weight at 20-80C. and the precipitated sulphate of chlorinated copper phthalocyanine is isolated, washed with sulphuric acid and hydrolysed in water. The product may be aftertreated by grinding or kneading in aqueous or aqueous-organic medium or by heating with water or an organic liquid. The pigments may be used to colour lacquers, printing inks, paints, paper, or natural, regenerated, semi-synthetic or synthetic polymers.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2403706A DE2403706A1 (en) | 1974-01-26 | 1974-01-26 | PROCESS FOR THE PRODUCTION OF CHLORINATED COPPER PHTHALOCYANINES |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1495442A true GB1495442A (en) | 1977-12-21 |
Family
ID=5905736
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3255/75A Expired GB1495442A (en) | 1974-01-26 | 1975-01-24 | Process for preparing chlorinated copper phthalocyanines |
Country Status (12)
| Country | Link |
|---|---|
| JP (1) | JPS5850264B2 (en) |
| AR (1) | AR202336A1 (en) |
| BE (1) | BE824816A (en) |
| BR (1) | BR7500510A (en) |
| CA (1) | CA1028693A (en) |
| CH (1) | CH606327A5 (en) |
| DE (1) | DE2403706A1 (en) |
| DK (1) | DK139756C (en) |
| FR (1) | FR2259142B1 (en) |
| GB (1) | GB1495442A (en) |
| IN (1) | IN141183B (en) |
| IT (1) | IT1031144B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5028801B2 (en) | 2004-01-13 | 2012-09-19 | 旭硝子株式会社 | Fluorinated polyether compounds |
-
1974
- 1974-01-26 DE DE2403706A patent/DE2403706A1/en not_active Withdrawn
- 1974-12-27 IN IN2870/CAL/74A patent/IN141183B/en unknown
-
1975
- 1975-01-23 CH CH79575A patent/CH606327A5/xx not_active IP Right Cessation
- 1975-01-24 BR BR510/75A patent/BR7500510A/en unknown
- 1975-01-24 JP JP50009905A patent/JPS5850264B2/en not_active Expired
- 1975-01-24 CA CA218,650A patent/CA1028693A/en not_active Expired
- 1975-01-24 DK DK23175A patent/DK139756C/en not_active IP Right Cessation
- 1975-01-24 IT IT19578/75A patent/IT1031144B/en active
- 1975-01-24 GB GB3255/75A patent/GB1495442A/en not_active Expired
- 1975-01-24 AR AR257410A patent/AR202336A1/en active
- 1975-01-27 FR FR7502387A patent/FR2259142B1/fr not_active Expired
- 1975-01-27 BE BE152736A patent/BE824816A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| FR2259142B1 (en) | 1979-08-03 |
| CH606327A5 (en) | 1978-10-31 |
| IT1031144B (en) | 1979-04-30 |
| BR7500510A (en) | 1975-11-11 |
| DK139756B (en) | 1979-04-09 |
| DK23175A (en) | 1975-09-22 |
| DE2403706A1 (en) | 1975-08-14 |
| JPS5850264B2 (en) | 1983-11-09 |
| JPS50104229A (en) | 1975-08-18 |
| BE824816A (en) | 1975-07-28 |
| AR202336A1 (en) | 1975-05-30 |
| DK139756C (en) | 1979-09-17 |
| IN141183B (en) | 1977-01-29 |
| FR2259142A1 (en) | 1975-08-22 |
| CA1028693A (en) | 1978-03-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |