GB1489699A - Process for the production of 1,3-dialkyl and di-(alkoxyalkyl)ureas - Google Patents
Process for the production of 1,3-dialkyl and di-(alkoxyalkyl)ureasInfo
- Publication number
- GB1489699A GB1489699A GB843175A GB843175A GB1489699A GB 1489699 A GB1489699 A GB 1489699A GB 843175 A GB843175 A GB 843175A GB 843175 A GB843175 A GB 843175A GB 1489699 A GB1489699 A GB 1489699A
- Authority
- GB
- United Kingdom
- Prior art keywords
- melt
- urea
- dialkyl
- alkyl group
- ureas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/18—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas
- C07C273/1854—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas by reactions not involving the formation of the N-C(O)-N- moiety
- C07C273/1863—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas by reactions not involving the formation of the N-C(O)-N- moiety from urea
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1489699 Substituted ureas JOHANN A WULFING 28 Feb 1975 [7 March 1974] 8431/75 Heading C2C Substituted ureas of the formula wherein R is an alkyl group or alkoxy alkyl group, are obtained by reacting together monoalkylamine or monoalkoxyalkylamine hydrochlorides (R-NH 2 -HCl) with urea, by heating with stirring a solvent-free mixture of the amine hydrochloride and urea, to melt the mixture, and then further heating the melt to 135‹ to 145‹ C. and on completion of the reaction, cooling the melt to a temperature of at least 100‹ C., adding water thereto and subsequently removing the dialkyl or dialkoxyalkyl urea formed by filtration under suction or extraction with a water-immiscible organic solvent.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19742411009 DE2411009B2 (en) | 1974-03-07 | 1974-03-07 | Process for the preparation of 1,3-dialkylureas |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1489699A true GB1489699A (en) | 1977-10-26 |
Family
ID=5909412
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB843175A Expired GB1489699A (en) | 1974-03-07 | 1975-02-28 | Process for the production of 1,3-dialkyl and di-(alkoxyalkyl)ureas |
Country Status (7)
Country | Link |
---|---|
AT (1) | AT343127B (en) |
BE (1) | BE826437A (en) |
CH (1) | CH592613A5 (en) |
DE (1) | DE2411009B2 (en) |
FR (1) | FR2263233B1 (en) |
GB (1) | GB1489699A (en) |
NL (1) | NL7502673A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2279347A (en) * | 1993-06-22 | 1995-01-04 | Roger Liddle Jefferson | Urea derivatives and their use in treating water |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2844962A1 (en) * | 1978-10-16 | 1980-04-30 | Basf Ag | METHOD FOR PRODUCING SYMMETRIC 1,3-DISUBSTITUTED UREAS |
AT394715B (en) * | 1990-08-14 | 1992-06-10 | Chemie Linz Gmbh | METHOD FOR N-ALKYLATING UREAS |
US5985968A (en) * | 1997-11-17 | 1999-11-16 | Air Products And Chemicals, Inc. | Surface tension reduction with N,N-dialkyl ureas |
-
1974
- 1974-03-07 DE DE19742411009 patent/DE2411009B2/en active Granted
-
1975
- 1975-01-16 CH CH51375A patent/CH592613A5/xx not_active IP Right Cessation
- 1975-02-28 GB GB843175A patent/GB1489699A/en not_active Expired
- 1975-03-04 AT AT165475A patent/AT343127B/en not_active IP Right Cessation
- 1975-03-05 FR FR7506855A patent/FR2263233B1/fr not_active Expired
- 1975-03-06 NL NL7502673A patent/NL7502673A/en not_active Application Discontinuation
- 1975-03-07 BE BE154135A patent/BE826437A/en not_active IP Right Cessation
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2279347A (en) * | 1993-06-22 | 1995-01-04 | Roger Liddle Jefferson | Urea derivatives and their use in treating water |
Also Published As
Publication number | Publication date |
---|---|
FR2263233B1 (en) | 1980-02-08 |
AT343127B (en) | 1978-05-10 |
NL7502673A (en) | 1975-09-09 |
FR2263233A1 (en) | 1975-10-03 |
BE826437A (en) | 1975-06-30 |
DE2411009B2 (en) | 1976-01-08 |
DE2411009A1 (en) | 1975-09-11 |
ATA165475A (en) | 1977-09-15 |
CH592613A5 (en) | 1977-10-31 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PCNP | Patent ceased through non-payment of renewal fee |