GB1413565A - Apparatus for producing organometallic compounds and method of preparing organolithium compounds in said apparatus - Google Patents

Apparatus for producing organometallic compounds and method of preparing organolithium compounds in said apparatus

Info

Publication number
GB1413565A
GB1413565A GB617473A GB617473A GB1413565A GB 1413565 A GB1413565 A GB 1413565A GB 617473 A GB617473 A GB 617473A GB 617473 A GB617473 A GB 617473A GB 1413565 A GB1413565 A GB 1413565A
Authority
GB
United Kingdom
Prior art keywords
compounds
spinneret
organometallic compounds
alkali metal
alkyl halides
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB617473A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
VORON VNII SINT CHESKOGO KAUCH
Original Assignee
VORON VNII SINT CHESKOGO KAUCH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to DE19732304124 priority Critical patent/DE2304124C3/en
Priority claimed from DE19732304124 external-priority patent/DE2304124C3/en
Application filed by VORON VNII SINT CHESKOGO KAUCH filed Critical VORON VNII SINT CHESKOGO KAUCH
Priority to GB617473A priority patent/GB1413565A/en
Priority to CA163,599A priority patent/CA1007832A/en
Priority to NL7303211.A priority patent/NL156703B/en
Priority to FR7308377A priority patent/FR2220534B1/fr
Priority to JP3584773A priority patent/JPS5629673B2/ja
Priority to DD170203A priority patent/DD106815A1/xx
Publication of GB1413565A publication Critical patent/GB1413565A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F1/00—Compounds containing elements of Groups 1 or 11 of the Periodic Table
    • C07F1/02—Lithium compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/81—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis the stirrers having central axial inflow and substantially radial outflow
    • B01F27/811—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis the stirrers having central axial inflow and substantially radial outflow with the inflow from one side only, e.g. stirrers placed on the bottom of the receptacle, or used as a bottom discharge pump
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/86—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis co-operating with deflectors or baffles fixed to the receptacle
    • B01F27/861—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis co-operating with deflectors or baffles fixed to the receptacle the baffles being of cylindrical shape, e.g. a mixing chamber surrounding the stirrer, the baffle being displaced axially to form an interior mixing chamber
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90—Heating or cooling systems
    • B01F35/92—Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1875—Stationary reactors having moving elements inside resulting in a loop-type movement internally, i.e. the mixture circulating inside the vessel such that the upwards stream is separated physically from the downwards stream(s)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F1/00—Compounds containing elements of Groups 1 or 11 of the Periodic Table
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90—Heating or cooling systems
    • B01F2035/99—Heating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00085—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/185—Details relating to the spatial orientation of the reactor vertical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1413565 Apparatus for preparing organometallic compounds VORONEZHSKY FILIAL VSESOJUZNOGO NAUCHNO ISSLEDOVATELSKOGO INSTITUTA SINTETICHES KOGO KAUCHUKA IMENI AKADEMIKA SV LEBEDEVA 8 Feb 1973 6174/73 Heading B1F [Also in Division C2] An apparatus for preparing organometallic compounds from alkali metals and alkyl halides or polynuclear compounds comprises hermetic reactor 1, heating jackets 3 and 15, extrusion press 5 comprising piston 6 for extruding alkali metal through spinneret 9, rotating cutter blades 11 for comminuting the alkali metal strands from spinneret 9, and a stirring means 12 which may be of the turbine type or toothed impeller type. Organolithium compounds are prepared in the above reactor by reacting metallic lithium with alkyl halides or polynuclear compounds in a hydrocarbon solvent under an inert gas blanket at 0-60‹C.
GB617473A 1973-01-29 1973-02-08 Apparatus for producing organometallic compounds and method of preparing organolithium compounds in said apparatus Expired GB1413565A (en)

Priority Applications (7)

Application Number Priority Date Filing Date Title
DE19732304124 DE2304124C3 (en) 1973-01-29 Reactor for the production of organic alkali compounds and process for the production of organolithium compounds
GB617473A GB1413565A (en) 1973-01-29 1973-02-08 Apparatus for producing organometallic compounds and method of preparing organolithium compounds in said apparatus
CA163,599A CA1007832A (en) 1973-01-29 1973-02-13 Apparatus for producing organometallic compounds and method of preparing organolithium compounds in said apparatus
NL7303211.A NL156703B (en) 1973-01-29 1973-03-07 DEVICE FOR PREPARING ORGANOMETAL COMPOUNDS.
FR7308377A FR2220534B1 (en) 1973-01-29 1973-03-08
JP3584773A JPS5629673B2 (en) 1973-01-29 1973-03-30
DD170203A DD106815A1 (en) 1973-01-29 1973-04-16

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
DE19732304124 DE2304124C3 (en) 1973-01-29 Reactor for the production of organic alkali compounds and process for the production of organolithium compounds
GB617473A GB1413565A (en) 1973-01-29 1973-02-08 Apparatus for producing organometallic compounds and method of preparing organolithium compounds in said apparatus
CA163,599A CA1007832A (en) 1973-01-29 1973-02-13 Apparatus for producing organometallic compounds and method of preparing organolithium compounds in said apparatus
FR7308377A FR2220534B1 (en) 1973-01-29 1973-03-08
JP3584773A JPS5629673B2 (en) 1973-01-29 1973-03-30
DD170203A DD106815A1 (en) 1973-01-29 1973-04-16

Publications (1)

Publication Number Publication Date
GB1413565A true GB1413565A (en) 1975-11-12

Family

ID=27543249

Family Applications (1)

Application Number Title Priority Date Filing Date
GB617473A Expired GB1413565A (en) 1973-01-29 1973-02-08 Apparatus for producing organometallic compounds and method of preparing organolithium compounds in said apparatus

Country Status (6)

Country Link
JP (1) JPS5629673B2 (en)
CA (1) CA1007832A (en)
DD (1) DD106815A1 (en)
FR (1) FR2220534B1 (en)
GB (1) GB1413565A (en)
NL (1) NL156703B (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996011052A1 (en) * 1994-10-07 1996-04-18 Bayer Aktiengesellschaft Sludge phase reactor and its use
CN1062502C (en) * 1996-11-18 2001-02-28 北京燕山石油化工公司研究院 Apparatus and method for preparing alkali metal suspension and organic alkali metal compound solution
EP1926549A1 (en) * 2005-09-21 2008-06-04 Stratco, Inc. Asphalt reactor and blending system
CN112871120A (en) * 2021-02-04 2021-06-01 中国特种设备检测研究院 High-pressure reaction kettle
CN115055076A (en) * 2022-08-19 2022-09-16 乐比(广州)健康产业有限公司 Even mixing equipment for preparing mosquito bite relieving composition
CN115212744A (en) * 2022-08-04 2022-10-21 江苏方达正塬电子材料科技有限公司 High-viscosity colloidal material pretreatment device
CN116284060A (en) * 2023-05-22 2023-06-23 研峰科技(北京)有限公司 Safe production process of organic lithium reagent butyl lithium

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5340507A (en) * 1991-07-26 1994-08-23 Fmc Corporation Catalyzed hydrocarbyllithium process
GB0022016D0 (en) * 2000-09-08 2000-10-25 Aea Technology Plc Chemical process plant
CN108043352A (en) * 2017-12-26 2018-05-18 徐州孝科编织有限公司 A kind of chemical reaction kettle
CN108786692A (en) * 2018-04-08 2018-11-13 张新雨 A kind of hydrogen production reaction kettle of improvement

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996011052A1 (en) * 1994-10-07 1996-04-18 Bayer Aktiengesellschaft Sludge phase reactor and its use
CN1062502C (en) * 1996-11-18 2001-02-28 北京燕山石油化工公司研究院 Apparatus and method for preparing alkali metal suspension and organic alkali metal compound solution
EP1926549A1 (en) * 2005-09-21 2008-06-04 Stratco, Inc. Asphalt reactor and blending system
EP1926549A4 (en) * 2005-09-21 2013-03-06 Stratco Inc Asphalt reactor and blending system
CN112871120A (en) * 2021-02-04 2021-06-01 中国特种设备检测研究院 High-pressure reaction kettle
CN115212744A (en) * 2022-08-04 2022-10-21 江苏方达正塬电子材料科技有限公司 High-viscosity colloidal material pretreatment device
CN115055076A (en) * 2022-08-19 2022-09-16 乐比(广州)健康产业有限公司 Even mixing equipment for preparing mosquito bite relieving composition
CN115055076B (en) * 2022-08-19 2022-10-25 乐比(广州)健康产业有限公司 Even mixing equipment for preparing mosquito bite relieving composition
CN116284060A (en) * 2023-05-22 2023-06-23 研峰科技(北京)有限公司 Safe production process of organic lithium reagent butyl lithium

Also Published As

Publication number Publication date
FR2220534B1 (en) 1977-08-12
NL7303211A (en) 1974-09-10
DD106815A1 (en) 1974-07-05
NL156703B (en) 1978-05-16
CA1007832A (en) 1977-04-05
DE2304124A1 (en) 1974-08-15
DE2304124B2 (en) 1976-03-04
JPS49126626A (en) 1974-12-04
JPS5629673B2 (en) 1981-07-09
FR2220534A1 (en) 1974-10-04

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PCNP Patent ceased through non-payment of renewal fee